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Information card for entry 7113521
Preview
| Coordinates | 7113521.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H59 Mo N2 O5 P2 Si2 |
|---|---|
| Calculated formula | C42 H59 Mo N2 O5 P2 Si2 |
| SMILES | [Mo]12([N]([Si](C)(C)C)=P(C1P(=[N]2[Si](C)(C)C)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(C#[O])(C#[O])C#[O].O(CC)CC.O(CC)CC |
| Title of publication | A novel synthesis of metallogermacyclopropane and molybdenum bis(iminophosphorano)carbene complexes from bisgermavinylidene |
| Authors of publication | Leung, Wing-Por; So, Cheuk-Wai; Wang, Jin-Zhi; Mak, Thomas C. W. |
| Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
| Year of publication | 2003 |
| Journal issue | 2 |
| Pages of publication | 248 - 249 |
| a | 11.1278 ± 0.0011 Å |
| b | 14.2454 ± 0.0013 Å |
| c | 16.2005 ± 0.0015 Å |
| α | 98.922 ± 0.002° |
| β | 95.369 ± 0.002° |
| γ | 110.193 ± 0.002° |
| Cell volume | 2350.9 ± 0.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0499 |
| Residual factor for significantly intense reflections | 0.0429 |
| Weighted residual factors for significantly intense reflections | 0.1219 |
| Weighted residual factors for all reflections included in the refinement | 0.1282 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Duplicate of | 7103937 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 210660 (current) | 2018-09-09 | cif/7/ Updating bibliography in entries 7103936-7103937, 7113520-7113521. Marking entries 7113520-7113521 as duplicates of entries 7103936-7103937. |
7113521.cif |
| 180249 | 2016-03-26 | cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/35. |
7113521.cif |
| 115108 | 2014-06-02 | cif/ Adding structures of 7113520, 7113521 via cif-deposit CGI script. |
7113521.cif |
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