Crystallography Open Database

Information card for entry 7113581

Preview

Coordinates	7113581.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C128.5 H184 Al4 Li8 O7 P8
Calculated formula	C128.5 H184 Al4 Li8 O7 P8
Title of publication	Synthesis and structure of [{MeAl(μ-PMes)(PMes)}2Li4]2·7thf, containing a [MeAl(μ-PMes)(PMes)]24- tetraanion (Mes = 2,4,6-Me3C6H2)
Authors of publication	García, Felipe; Haigh, Robert; McPartlin, Mary; Wright, Dominic S.
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2003
Journal issue	16
Pages of publication	2052 - 2053
a	16.1493 ± 0.0003 Å
b	15.1393 ± 0.0002 Å
c	28.7338 ± 0.0005 Å
α	90°
β	90.063 ± 0.001°
γ	90°
Cell volume	7025.1 ± 0.2 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.1067
Residual factor for significantly intense reflections	0.0867
Weighted residual factors for significantly intense reflections	0.2223
Weighted residual factors for all reflections included in the refinement	0.2342
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Duplicate of	7103846
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
210630 (current)	2018-09-09	cif/7/ Updating bibliography in entries 7103846, 7113581. Marking entry 7113581 as a duplicate in entry 7103846.	7113581.cif
176453	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7113581.cif
115142	2014-06-02	cif/ Adding structures of 7113581 via cif-deposit CGI script.	7113581.cif