Crystallography Open Database

Information card for entry 7114100

Preview

Coordinates	7114100.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Tb14(OH)18(acac)24
Formula	C122 H190.6 O66 Tb14
Calculated formula	C122 H16 O66 Tb14
Title of publication	Toward constructing nanoscale hydroxo‒lanthanide clusters: syntheses and characterizations of novel tetradecanuclear hydroxo‒lanthanide clusters
Authors of publication	Wang, Ruiyao; Song, Datong; Wang, Suning
Journal of publication	Chemical Communications
Year of publication	2002
Journal issue	4
Pages of publication	368
a	21.09 ± 0.004 Å
b	21.09 ± 0.004 Å
c	21.213 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	9435 ± 3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	139
Hermann-Mauguin space group symbol	I 4/m m m
Hall space group symbol	-I 4 2
Residual factor for all reflections	0.0731
Residual factor for significantly intense reflections	0.0566
Weighted residual factors for significantly intense reflections	0.1409
Weighted residual factors for all reflections included in the refinement	0.148
Goodness-of-fit parameter for all reflections included in the refinement	1.17
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180255 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/41.	7114100.cif
116561	2014-06-13	cif/ Adding structures of 7114100 via cif-deposit CGI script.	7114100.cif