Crystallography Open Database

Information card for entry 7114699

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Coordinates	7114699.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C97 H150 N4 Ni14.08 O31 Pt9.92
Calculated formula	C97 H150 N4 Ni14.07 O31 Pt9.921
Title of publication	New high-nuclearity Ni‒Pt carbonyl clusters: synthesis and X-ray structure of the ordered [Ni24Pt14(CO)44]4‒ and the substitutionally Ni/Pt disordered [Ni10(Ni6‒xPtx)Pt8(CO)30]4‒ (x = 1.92) tetraanions
Authors of publication	Femoni, Cristina; Carmela Iapalucci, M.; Longoni, Giuliano; Svensson, Per H.
Journal of publication	Chemical Communications
Year of publication	2001
Journal issue	18
Pages of publication	1776
a	26.7155 ± 0.0009 Å
b	15.2758 ± 0.0005 Å
c	31.9982 ± 0.0011 Å
α	90°
β	98.404 ± 0.001°
γ	90°
Cell volume	12918.3 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1257
Residual factor for significantly intense reflections	0.0458
Weighted residual factors for significantly intense reflections	0.0924
Weighted residual factors for all reflections included in the refinement	0.1162
Goodness-of-fit parameter for all reflections included in the refinement	0.888
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180260 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/46.	7114699.cif
118289	2014-06-29	cif/ Adding structures of 7114698, 7114699 via cif-deposit CGI script.	7114699.cif