Crystallography Open Database

Information card for entry 7114700

Preview

Coordinates	7114700.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H26 Ag2 F16 N6 O P2 S
Calculated formula	C22 H26 Ag2 F12 N6 O P2 S
Title of publication	Synthesis and structural characterization of a silver complex of a mixed-donor N-heterocyclic carbene linked cyclophane
Authors of publication	Garrison, Jered C.; Simons, Richard S.; Kofron, William G.; Tessier, Claire A.; Youngs, Wiley J.
Journal of publication	Chemical Communications
Year of publication	2001
Journal issue	18
Pages of publication	1780
a	10.389 ± 0.002 Å
b	11.272 ± 0.002 Å
c	14.104 ± 0.003 Å
α	110.21 ± 0.03°
β	96.34 ± 0.03°
γ	102.46 ± 0.03°
Cell volume	1482.3 ± 0.7 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0617
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.1229
Weighted residual factors for all reflections included in the refinement	0.1343
Goodness-of-fit parameter for all reflections included in the refinement	0.994
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180261 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/47.	7114700.cif
118291	2014-06-29	cif/ Adding structures of 7114700 via cif-deposit CGI script.	7114700.cif