Crystallography Open Database

Information card for entry 7114954

Preview

Coordinates	7114954.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H49 Li3 N7 P3
Calculated formula	C25 H49 Li3 N7 P3
Title of publication	Cooperative cation and anion coordination by a bifunctional imidophosphorane ligand framework; syntheses and structures of [LiCl{ButNHP(μ-NBut)2PNH(2-py)}3] and [{ButNP(μ-NBut)2PN(2-py)} Li2·{Li(ButN)2P}]
Authors of publication	Bond, Andrew D.; Doyle, Emma L.; Kidd, Sara J.; Woods, Anthony D.; Wright, Dominic S.
Journal of publication	Chemical Communications
Year of publication	2001
Journal issue	8
Pages of publication	777
a	17.1197 ± 0.0005 Å
b	10.5016 ± 0.0004 Å
c	18.8343 ± 0.0004 Å
α	90°
β	98.535 ± 0.002°
γ	90°
Cell volume	3348.61 ± 0.18 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1015
Residual factor for significantly intense reflections	0.0723
Weighted residual factors for significantly intense reflections	0.1848
Weighted residual factors for all reflections included in the refinement	0.2071
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180263 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/49.	7114954.cif
118445	2014-06-30	cif/ Adding structures of 7114954, 7114955 via cif-deposit CGI script.	7114954.cif