Crystallography Open Database

Information card for entry 7116166

Preview

Coordinates	7116166.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H55.82 Cl0.18 F2 Ir2 N4
Calculated formula	C34 H55.818 Cl0.182 F2 Ir2 N4
Title of publication	Fluoride, bifluoride and trifluoromethyl complexes of iridium(I) and rhodium(I)
Authors of publication	Byron J. Truscott; Fady Nahra; Alexandra M. Z. Slawin; David B. Cordes; Steven P. Nolan
Journal of publication	Chem.Commun.
Year of publication	2015
Journal volume	51
Pages of publication	62
a	10.057 ± 0.004 Å
b	12.486 ± 0.005 Å
c	14.296 ± 0.007 Å
α	101.386 ± 0.013°
β	96.141 ± 0.01°
γ	90.28 ± 0.015°
Cell volume	1749.1 ± 1.3 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0717
Weighted residual factors for all reflections included in the refinement	0.1952
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180275 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/61.	7116166.cif
129220	2014-12-30	cif/ Adding structures of 7116165, 7116166, 7116167, 7116168, 7116169, 7116170, 7116171, 7116172 via cif-deposit CGI script.	7116166.cif