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Information card for entry 7116286
Preview
| Coordinates | 7116286.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C26 H24 Cl3 N O2 Si |
|---|---|
| Calculated formula | C26 H24 Cl3 N O2 Si |
| Title of publication | Multi-site cyclization via initial C-H activation using a rhodium(iii) catalyst: rapid assembly of frameworks containing indoles and indolines. |
| Authors of publication | Huang, Ji-Rong; Qin, Liu; Zhu, Yu-Qin; Song, Qiang; Dong, Lin |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2015 |
| Journal volume | 51 |
| Journal issue | 14 |
| Pages of publication | 2844 |
| a | 9.6847 ± 0.0007 Å |
| b | 10.6101 ± 0.0008 Å |
| c | 12.7428 ± 0.001 Å |
| α | 82.268 ± 0.006° |
| β | 87.114 ± 0.006° |
| γ | 75.081 ± 0.007° |
| Cell volume | 1253.58 ± 0.17 Å3 |
| Cell temperature | 170 ± 2 K |
| Ambient diffraction temperature | 170 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.077 |
| Residual factor for significantly intense reflections | 0.0556 |
| Weighted residual factors for significantly intense reflections | 0.1246 |
| Weighted residual factors for all reflections included in the refinement | 0.1426 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301857 (current) | 2025-08-22 | Add cross-references to PubChem compounds in COD range 7/11/ Each referenced PubChem compound corresponds to the full crystal structure. |
7116286.cif |
| 180276 | 2016-03-26 | cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/62. |
7116286.cif |
| 130946 | 2015-02-04 | cif/ Updating files of 7116285, 7116286 Original log message: Adding full bibliography for 7116285--7116286.cif. |
7116286.cif |
| 129370 | 2015-01-06 | cif/ Adding structures of 7116285, 7116286 via cif-deposit CGI script. |
7116286.cif |
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Users of the data should acknowledge the original authors of the
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