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Information card for entry 7117409
Preview
Coordinates | 7117409.cif |
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Original paper (by DOI) | HTML |
Formula | C52 H82 N4 O10 P2 Si6 W2 |
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Calculated formula | C52 H82 N4 O10 P2 Si6 W2 |
Title of publication | Facile rotation around a silicon-phosphorus double bond enabled through coordination to tungsten |
Authors of publication | Nora C. Breit; Tibor Szilvasi; Shigeyoshi Inoue |
Journal of publication | Chem.Commun. |
Year of publication | 2015 |
Journal volume | 51 |
Pages of publication | 11272 |
a | 18.8405 ± 0.0003 Å |
b | 10.1491 ± 0.0002 Å |
c | 34.9207 ± 0.0005 Å |
α | 90° |
β | 92.318 ± 0.001° |
γ | 90° |
Cell volume | 6671.87 ± 0.19 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 7 |
Space group number | 15 |
Hermann-Mauguin space group symbol | I 1 2/a 1 |
Hall space group symbol | -I 2ya |
Residual factor for all reflections | 0.0397 |
Residual factor for significantly intense reflections | 0.0361 |
Weighted residual factors for significantly intense reflections | 0.0854 |
Weighted residual factors for all reflections included in the refinement | 0.0881 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
176428 (current) | 2016-02-13 | Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively. |
7117409.cif |
139961 | 2015-07-03 | cif/ Adding structures of 7117408, 7117409 via cif-deposit CGI script. |
7117409.cif |
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Users of the data should acknowledge the original authors of the
structural data.