Crystallography Open Database

Information card for entry 7117476

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Structure parameters

Formula	C94.4 H105.8 Cl Li Lu N4 O5.6 P4 Pd
Calculated formula	C94.4 H105.8 Cl Li Lu N4 O5.6 P4 Pd
Title of publication	Bi- and trimetallic rare-earth-palladium complexes ligated by phosphinoamides
Authors of publication	Franziska Volcker; Felix M. Muck; Konstantinos D. Vogiatzis; Karin Fink; Peter W. Roesky
Journal of publication	Chem.Commun.
Year of publication	2015
Journal volume	51
Pages of publication	11761
a	13.414 ± 0.003 Å
b	15.386 ± 0.003 Å
c	22.048 ± 0.004 Å
α	88.38 ± 0.03°
β	80.4 ± 0.03°
γ	84.17 ± 0.03°
Cell volume	4463.2 ± 1.6 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.226
Residual factor for significantly intense reflections	0.0855
Weighted residual factors for significantly intense reflections	0.11
Weighted residual factors for all reflections included in the refinement	0.1476
Goodness-of-fit parameter for all reflections included in the refinement	0.831
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301857 (current)	2025-08-22	Add cross-references to PubChem compounds in COD range 7/11/ Each referenced PubChem compound corresponds to the full crystal structure.	7117476.cif
176429	2016-02-13	cif/ (antanas@kurmis) Replacing _cod_chemical_formula_sum_orig tag with _cod_original_formula_sum tag in multiple entries since the replaced tag is deprecated according to the COD CIF dictionary.	7117476.cif
148155	2015-07-12	cif/ Adding structures of 7117473, 7117474, 7117475, 7117476, 7117477, 7117478, 7117479 via cif-deposit CGI script.	7117476.cif