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Information card for entry 7117930
Preview
| Coordinates | 7117930.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H78 K N5 O8 Si6 U |
|---|---|
| Calculated formula | C32 H78 K N5 O8 Si6 U |
| Title of publication | CO2 conversion to isocyanate via multiple N-Si bond cleavage at a bulky uranium(III) complex |
| Authors of publication | Clement Camp; Lucile Chatelain; Christos E. Kefalidis; Jacques Pecaut; Laurent Maron; Marinella Mazzanti |
| Journal of publication | Chem.Commun. |
| Year of publication | 2015 |
| Journal volume | 51 |
| Pages of publication | 15454 |
| a | 11.5823 ± 0.0002 Å |
| b | 17.9907 ± 0.0005 Å |
| c | 14.1292 ± 0.0003 Å |
| α | 90° |
| β | 111.687 ± 0.002° |
| γ | 90° |
| Cell volume | 2735.76 ± 0.11 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 11 |
| Hermann-Mauguin space group symbol | P 1 21/m 1 |
| Hall space group symbol | -P 2yb |
| Residual factor for all reflections | 0.0493 |
| Residual factor for significantly intense reflections | 0.0353 |
| Weighted residual factors for significantly intense reflections | 0.0673 |
| Weighted residual factors for all reflections included in the refinement | 0.0718 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.091 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 165896 (current) | 2015-10-12 | cif/ Adding structures of 7117930 via cif-deposit CGI script. |
7117930.cif |
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Users of the data should acknowledge the original authors of the
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