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Information card for entry 7118042
Preview
| Coordinates | 7118042.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H54 N6 P4 |
|---|---|
| Calculated formula | C24 H54 N6 P4 |
| Title of publication | Steric C-N bond activation on the dimeric macrocycle [{P(μ-NR)}2(μ-NR)]2. |
| Authors of publication | Shi, Yan X.; Liang, Rong Z.; Martin, Katherine A.; Star, Daniel G.; Díaz, Jesús; Li, Xin Y.; Ganguly, Rakesh; García, Felipe |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2015 |
| Journal volume | 51 |
| Journal issue | 92 |
| Pages of publication | 16468 - 16471 |
| a | 28.4547 ± 0.0019 Å |
| b | 16.8252 ± 0.0011 Å |
| c | 9.7507 ± 0.0007 Å |
| α | 90° |
| β | 94.991 ± 0.003° |
| γ | 90° |
| Cell volume | 4650.5 ± 0.5 Å3 |
| Cell temperature | 103 ± 2 K |
| Ambient diffraction temperature | 103 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 12 |
| Hermann-Mauguin space group symbol | C 1 2/m 1 |
| Hall space group symbol | -C 2y |
| Residual factor for all reflections | 0.1354 |
| Residual factor for significantly intense reflections | 0.0895 |
| Weighted residual factors for significantly intense reflections | 0.2587 |
| Weighted residual factors for all reflections included in the refinement | 0.3082 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.099 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 170147 (current) | 2015-11-07 | cif/ Adding structures of 7118041, 7118042, 7118043, 7118044 via cif-deposit CGI script. |
7118042.cif |
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Users of the data should acknowledge the original authors of the
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