Crystallography Open Database

Information card for entry 7118193

Preview

Coordinates	7118193.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H24 F9 O9 P2 S3 Sb
Calculated formula	C29 H24 F9 O9 P2 S3 Sb
Title of publication	Distinction between coordination and phosphine ligand oxidation: interactions of di- and triphosphines with Pn^3+^ (Pn = P, As, Sb, Bi)
Authors of publication	Chitnis, Saurabh S.; Vos, Kevin A.; Burford, Neil; McDonald, Robert; Ferguson, Michael J.
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2016
Journal volume	52
Pages of publication	685 - 688
a	13.3718 ± 0.0004 Å
b	17.5496 ± 0.0006 Å
c	15.4871 ± 0.0005 Å
α	90°
β	102.96 ± 0.0015°
γ	90°
Cell volume	3541.8 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0481
Residual factor for significantly intense reflections	0.0416
Weighted residual factors for significantly intense reflections	0.1055
Weighted residual factors for all reflections included in the refinement	0.1119
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
209786 (current)	2018-08-16	cif/7/11/ Updating bibliography in entries 7118191-7118193, 7118471-7118473. Marking entries 7118471-7118473 as duplicates of entries 7118191-7118193.	7118193.cif
171849	2016-01-01	cif/ Adding structures of 7118191, 7118192, 7118193 via cif-deposit CGI script.	7118193.cif