Crystallography Open Database

Information card for entry 7118200

Preview

Coordinates	7118200.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H29 P
Calculated formula	C22 H29 P
Title of publication	Cyclopropane formation under frustrated Lewis pair conditions.
Authors of publication	Krupski, Sergei; Kehr, Gerald; Daniliuc, Constantin G.; Erker, Gerhard
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	13
Pages of publication	2695 - 2697
a	8.3322 ± 0.0002 Å
b	8.5865 ± 0.0003 Å
c	13.0867 ± 0.0004 Å
α	87.833 ± 0.001°
β	85.945 ± 0.001°
γ	86.322 ± 0.001°
Cell volume	931.49 ± 0.05 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0416
Residual factor for significantly intense reflections	0.0353
Weighted residual factors for significantly intense reflections	0.0884
Weighted residual factors for all reflections included in the refinement	0.0925
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
177634 (current)	2016-03-05	cif/ Updating files of 7118199, 7118200, 7118201, 7118202 Original log message: Adding full bibliography for 7118199--7118202.cif.	7118200.cif
171853	2016-01-01	cif/ Adding structures of 7118199, 7118200, 7118201, 7118202 via cif-deposit CGI script.	7118200.cif