Crystallography Open Database

Information card for entry 7118308

Preview

Coordinates	7118308.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Co6 H224 Li14 Na9 O250 P5 W36
Calculated formula	Co6 Na4.53 O174.9 P5 W36
Title of publication	Rearrangement of {α-P2W15} to {PW6} moieties during the assembly of transition-metal-linked polyoxometalate clusters.
Authors of publication	Martin-Sabi, Mercè; Winter, Ross Stuart; Lydon, Claire; Cameron, Jamie M.; Long, De-Liang; Cronin, Leroy
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	5
Pages of publication	919 - 921
a	14.5199 ± 0.0004 Å
b	25.6135 ± 0.0007 Å
c	27.6975 ± 0.0008 Å
α	94.512 ± 0.002°
β	99.078 ± 0.002°
γ	93.145 ± 0.002°
Cell volume	10116.6 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1339
Residual factor for significantly intense reflections	0.0492
Weighted residual factors for significantly intense reflections	0.1068
Weighted residual factors for all reflections included in the refinement	0.121
Goodness-of-fit parameter for all reflections included in the refinement	0.802
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
173520 (current)	2016-01-06	cif/ Adding structures of 7118308, 7118309, 7118310 via cif-deposit CGI script.	7118308.cif