Crystallography Open Database

Information card for entry 7118310

Preview

Coordinates	7118310.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H137 Li20 Mn9 Na5 O245 P8 W45
Calculated formula	Mn9 Na2.2 O203 P7.5 W45
Title of publication	Rearrangement of {α-P2W15} to {PW6} moieties during the assembly of transition-metal-linked polyoxometalate clusters.
Authors of publication	Martin-Sabi, Mercè; Winter, Ross Stuart; Lydon, Claire; Cameron, Jamie M.; Long, De-Liang; Cronin, Leroy
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	5
Pages of publication	919 - 921
a	14.0535 ± 0.0008 Å
b	29.6184 ± 0.0016 Å
c	31.8218 ± 0.0016 Å
α	74.118 ± 0.005°
β	81.242 ± 0.004°
γ	89.716 ± 0.004°
Cell volume	12582 ± 1.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1857
Residual factor for significantly intense reflections	0.0886
Weighted residual factors for significantly intense reflections	0.2096
Weighted residual factors for all reflections included in the refinement	0.2476
Goodness-of-fit parameter for all reflections included in the refinement	0.882
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
173520 (current)	2016-01-06	cif/ Adding structures of 7118308, 7118309, 7118310 via cif-deposit CGI script.	7118310.cif