Crystallography Open Database

Information card for entry 7118452

Preview

Coordinates	7118452.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H60 Cl6 Ga N2 P3
Calculated formula	C42 H60 Cl6 Ga N2 P3
Title of publication	[((Cl)Im(Dipp))P[double bond, length as m-dash]P(Dipp)][GaCl4]: a polarized, cationic diphosphene.
Authors of publication	Schwedtmann, Kai; Holthausen, Michael H.; Sala, Chris H.; Hennersdorf, Felix; Fröhlich, Roland; Weigand, Jan J.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	7
Pages of publication	1409 - 1412
a	13.8028 ± 0.0004 Å
b	17.4286 ± 0.0005 Å
c	21.7529 ± 0.0006 Å
α	107.609 ± 0.001°
β	98.701 ± 0.001°
γ	97.42 ± 0.001°
Cell volume	4844.6 ± 0.2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.097
Residual factor for significantly intense reflections	0.0503
Weighted residual factors for significantly intense reflections	0.1069
Weighted residual factors for all reflections included in the refinement	0.1246
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
174469 (current)	2016-01-15	cif/ Adding structures of 7118449, 7118450, 7118451, 7118452 via cif-deposit CGI script.	7118452.cif