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Information card for entry 7118463
Preview
| Coordinates | 7118463.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C14 H20 F3 N O3 |
|---|---|
| Calculated formula | C14 H20 F2.997 N O3 |
| Title of publication | The synthesis of sterically hindered amines by a direct reductive amination of ketones. |
| Authors of publication | Yagafarov, Niyaz Z.; Kolesnikov, Pavel N.; Usanov, Dmitry L.; Novikov, Valentin V.; Nelyubina, Yulia V.; Chusov, Denis |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2016 |
| Journal volume | 52 |
| Journal issue | 7 |
| Pages of publication | 1397 - 1400 |
| a | 7.7764 ± 0.0012 Å |
| b | 15.755 ± 0.002 Å |
| c | 25.521 ± 0.004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3126.8 ± 0.8 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.1015 |
| Residual factor for significantly intense reflections | 0.0734 |
| Weighted residual factors for significantly intense reflections | 0.1742 |
| Weighted residual factors for all reflections included in the refinement | 0.185 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.376 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 174475 (current) | 2016-01-15 | cif/ Adding structures of 7118463 via cif-deposit CGI script. |
7118463.cif |
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Users of the data should acknowledge the original authors of the
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