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Information card for entry 7118463
Preview
Coordinates | 7118463.cif |
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Original paper (by DOI) | HTML |
Formula | C14 H20 F3 N O3 |
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Calculated formula | C14 H20 F2.997 N O3 |
Title of publication | The synthesis of sterically hindered amines by a direct reductive amination of ketones. |
Authors of publication | Yagafarov, Niyaz Z.; Kolesnikov, Pavel N.; Usanov, Dmitry L.; Novikov, Valentin V.; Nelyubina, Yulia V.; Chusov, Denis |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2016 |
Journal volume | 52 |
Journal issue | 7 |
Pages of publication | 1397 - 1400 |
a | 7.7764 ± 0.0012 Å |
b | 15.755 ± 0.002 Å |
c | 25.521 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3126.8 ± 0.8 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.1015 |
Residual factor for significantly intense reflections | 0.0734 |
Weighted residual factors for significantly intense reflections | 0.1742 |
Weighted residual factors for all reflections included in the refinement | 0.185 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.376 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
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174475 (current) | 2016-01-15 | cif/ Adding structures of 7118463 via cif-deposit CGI script. |
7118463.cif |
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