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Information card for entry 7120989
Preview
| Coordinates | 7120989.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | 1,5-bis(t-butyldimethylsiloxy)hexaisobutylbicyclo[3.3.3]pentasiloxane |
|---|---|
| Formula | C18 H42 O4 Si3.5 |
| Calculated formula | C18 H42 O4 Si3.5 |
| Title of publication | Facile synthesis and bridgehead-functionalization of bicyclo[3.3.3]pentasiloxanes |
| Authors of publication | Yokouchi, Yuki; Ishida, Shintaro; Onodera, Tsunenobu; Oikawa, Hidetoshi; Iwamoto, Takeaki |
| Journal of publication | Chemical Communications |
| Year of publication | 2018 |
| a | 19.0349 ± 0.0005 Å |
| b | 13.7423 ± 0.0003 Å |
| c | 21.0422 ± 0.0005 Å |
| α | 90° |
| β | 103.889 ± 0.001° |
| γ | 90° |
| Cell volume | 5343.4 ± 0.2 Å3 |
| Cell temperature | 223 ± 2 K |
| Ambient diffraction temperature | 223 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0945 |
| Residual factor for significantly intense reflections | 0.0703 |
| Weighted residual factors for significantly intense reflections | 0.1945 |
| Weighted residual factors for all reflections included in the refinement | 0.2335 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 204201 (current) | 2017-12-13 | cif/ Adding structures of 7120986, 7120987, 7120988, 7120989 via cif-deposit CGI script. |
7120989.cif |
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