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Information card for entry 7121028
Preview
| Coordinates | 7121028.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C40 H48 Cl2 N2 Ni O2 P2 |
|---|---|
| Calculated formula | C40 H48 Cl2 N2 Ni O2 P2 |
| Title of publication | Mild electrochemical synthesis of metal phosphides with dibenzo-7-phosphanorbornadiene derivatives: mechanistic insights and application to proton reduction in water. |
| Authors of publication | Shida, Naoki; Buss, Joshua A.; Agapie, Theodor |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2018 |
| Journal volume | 54 |
| Journal issue | 7 |
| Pages of publication | 767 - 770 |
| a | 17.2751 ± 0.0011 Å |
| b | 11.6325 ± 0.0007 Å |
| c | 18.6817 ± 0.0012 Å |
| α | 90° |
| β | 90.593 ± 0.002° |
| γ | 90° |
| Cell volume | 3753.9 ± 0.4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0474 |
| Residual factor for significantly intense reflections | 0.0318 |
| Weighted residual factors for significantly intense reflections | 0.0754 |
| Weighted residual factors for all reflections included in the refinement | 0.0831 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 228400 (current) | 2019-11-17 | cif/ Updating files of 7121026, 7121027, 7121028 Original log message: Adding full bibliography for 7121026--7121028.cif. |
7121028.cif |
| 204431 | 2017-12-21 | cif/ Adding structures of 7121026, 7121027, 7121028 via cif-deposit CGI script. |
7121028.cif |
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Users of the data should acknowledge the original authors of the
structural data.