Crystallography Open Database

Information card for entry 7122378

Preview

Coordinates	7122378.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Ru2Sb6 cluster
Formula	C68 H115 K2 N5 O12 Ru2 Sb6
Calculated formula	C68 H115 K2 N5 O12 Ru2 Sb6
Title of publication	The cyclo-Sb<sub>6</sub> ring in the [Sb<sub>6</sub>(RuCp*)<sub>2</sub>]<sup>2-</sup> ion.
Authors of publication	Wang, Yi; Zavalij, Peter; Eichhorn, Bryan
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	84
Pages of publication	11917 - 11920
a	13.1437 ± 0.0009 Å
b	13.96 ± 0.001 Å
c	23.484 ± 0.0016 Å
α	88.5283 ± 0.0011°
β	84.7546 ± 0.0011°
γ	79.2296 ± 0.0011°
Cell volume	4215.2 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0409
Residual factor for significantly intense reflections	0.0279
Weighted residual factors for significantly intense reflections	0.0527
Weighted residual factors for all reflections included in the refinement	0.0551
Goodness-of-fit parameter for all reflections included in the refinement	1.157
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
228478 (current)	2019-11-17	cif/ Updating files of 7122378, 7122379 Original log message: Adding full bibliography for 7122378--7122379.cif.	7122378.cif
211183	2018-09-27	cif/ Adding structures of 7122378, 7122379 via cif-deposit CGI script.	7122378.cif