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Information card for entry 7123815
Preview
| Coordinates | 7123815.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H44 Li2 N2 Si4 |
|---|---|
| Calculated formula | C24 H44 Li2 N2 Si4 |
| Title of publication | Agostic Deformations based on Electron Delocalization in the Alkyllithium-complex [{2-(Me3Si)2CLiC5H4N}2] |
| Authors of publication | Scherer, W.; Sirsch, P.; Grosche, M.; Spiegler, M.; Mason, S. A.; Gardiner, M.G. |
| Journal of publication | Chemical Communications |
| Year of publication | 2001 |
| Journal volume | 20 |
| Pages of publication | 2072 - 2073 |
| a | 11.722 ± 0.0013 Å |
| b | 9.864 ± 0.0012 Å |
| c | 12.7517 ± 0.0015 Å |
| α | 90° |
| β | 93.479 ± 0.004° |
| γ | 90° |
| Cell volume | 1471.7 ± 0.3 Å3 |
| Cell temperature | 100 ± 1 K |
| Ambient diffraction temperature | 100 ± 1 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0519 |
| Residual factor for significantly intense reflections | 0.033 |
| Weighted residual factors for significantly intense reflections | 0.067 |
| Weighted residual factors for all reflections included in the refinement | 0.0776 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.083 |
| Diffraction radiation wavelength | 0.82306 Å |
| Diffraction radiation type | neutron |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 216931 (current) | 2019-07-10 | cif/ Adding structures of 7123815 via cif-deposit CGI script. |
7123815.cif |
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Users of the data should acknowledge the original authors of the
structural data.