Crystallography Open Database

Information card for entry 7124406

Preview

Coordinates	7124406.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H59 Cl2 N2 P Ru
Calculated formula	C40 H59 Cl2 N2 P Ru
Title of publication	Direct Synthesis of Dialkylaryl-vinylsilane Derivatives: Metathesis of Dialkylaryl-iso-propenylsilane and Its Application to Tetracyclic Silacycle Dye Synthesis
Authors of publication	YOSHIOKA, Shohei; Takehara, Tsunayoshi; MATSUZAKI, Tsuyoshi; Suzuki, Takeyuki; Tsujino, Hirofumi; Uno, Tadayuki; Tsutumi, Y.; Murai, Kenichi; Fujioka, Hiromichi; Arisawa, Mitsuhiro
Journal of publication	Chemical Communications
Year of publication	2019
a	12.2448 ± 0.0002 Å
b	18.3117 ± 0.0002 Å
c	17.9788 ± 0.0003 Å
α	90°
β	104.121 ± 0.0017°
γ	90°
Cell volume	3909.45 ± 0.1 Å³
Cell temperature	123 K
Ambient diffraction temperature	123 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0457
Residual factor for significantly intense reflections	0.0346
Weighted residual factors for significantly intense reflections	0.0798
Weighted residual factors for all reflections included in the refinement	0.0847
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
220574 (current)	2019-10-31	cif/ Adding structures of 7124406 via cif-deposit CGI script.	7124406.cif