Crystallography Open Database

Information card for entry 7124851

Preview

Coordinates	7124851.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H56 B2 Li2 O6
Calculated formula	C28 H56 B2 Li2 O6
Title of publication	The copper-catalysed Suzuki-Miyaura coupling of alkylboron reagents: disproportionation of anionic (alkyl)(alkoxy)borates to anionic dialkylborates prior to transmetalation.
Authors of publication	Basnet, Prakash; Thapa, Surendra; Dickie, Diane A.; Giri, Ramesh
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	74
Pages of publication	11072 - 11075
a	8.3308 ± 0.0004 Å
b	9.3831 ± 0.0005 Å
c	10.3351 ± 0.0005 Å
α	98.43 ± 0.002°
β	106.326 ± 0.002°
γ	90.671 ± 0.002°
Cell volume	765.74 ± 0.07 Å³
Cell temperature	101 ± 2 K
Ambient diffraction temperature	101 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0576
Residual factor for significantly intense reflections	0.053
Weighted residual factors for significantly intense reflections	0.1448
Weighted residual factors for all reflections included in the refinement	0.1492
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
234287 (current)	2019-11-23	cif/ Adding structures of 7124850, 7124851 via cif-deposit CGI script.	7124851.cif