Crystallography Open Database

Information card for entry 7124911

Preview

Coordinates	7124911.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H54 Br N O3 Si Zn
Calculated formula	C45 H54 Br N O3 Si Zn
Title of publication	Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
Authors of publication	Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	69
Pages of publication	10490 - 10492
a	20.9835 ± 0.001 Å
b	20.9835 ± 0.001 Å
c	37.613 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	16561.3 ± 1.7 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	7
Space group number	88
Hermann-Mauguin space group symbol	I 41/a :2
Hall space group symbol	-I 4ad
Residual factor for all reflections	0.112
Residual factor for significantly intense reflections	0.0597
Weighted residual factors for significantly intense reflections	0.1136
Weighted residual factors for all reflections included in the refinement	0.1364
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
234338 (current)	2019-11-23	cif/ Adding structures of 7124906, 7124907, 7124908, 7124909, 7124910, 7124911, 7124912, 7124913, 7124914 via cif-deposit CGI script.	7124911.cif