Crystallography Open Database

Information card for entry 7125322

Preview

Coordinates	7125322.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	cis-[PtMe2[PTB]2][NEt4]2
Formula	C66 H80 B2 N2 P2 Pt
Calculated formula	C66 H80 B2 N2 P2 Pt
Title of publication	Fusing triphenylphosphine with tetraphenylborate: introducing the 9-phosphatriptycene-10-phenylborate (PTB) anion.
Authors of publication	Drover, Marcus W.; Nagata, Koichi; Peters, Jonas C.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	57
Pages of publication	7916 - 7919
a	16.708 ± 0.0008 Å
b	22.4099 ± 0.0011 Å
c	16.7415 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	6268.4 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.1027
Residual factor for significantly intense reflections	0.0735
Weighted residual factors for significantly intense reflections	0.153
Weighted residual factors for all reflections included in the refinement	0.163
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
236762 (current)	2019-11-24	cif/ Adding structures of 7125321, 7125322, 7125323, 7125324, 7125325, 7125326, 7125327, 7125328 via cif-deposit CGI script.	7125322.cif