Crystallography Open Database

Information card for entry 7126642

Preview

Coordinates	7126642.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C71 H60 Cl6 Fe2 P4 Rh2
Calculated formula	C71 H60 Cl6 Fe2 P4 Rh2
Title of publication	Halogenation of A-frame μ-carbido complexes: a diamagnetic rhodium(ii) carbido complex.
Authors of publication	Barnett, Harrison J.; Hill, Anthony F.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	56
Pages of publication	7738 - 7740
a	13.1742 ± 0.0003 Å
b	26.8362 ± 0.0006 Å
c	18.2963 ± 0.0003 Å
α	90°
β	90.747 ± 0.002°
γ	90°
Cell volume	6468 ± 0.2 Å³
Cell temperature	150.01 ± 0.1 K
Ambient diffraction temperature	150.01 ± 0.1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.074
Residual factor for significantly intense reflections	0.048
Weighted residual factors for significantly intense reflections	0.0975
Weighted residual factors for all reflections included in the refinement	0.1091
Goodness-of-fit parameter for all reflections included in the refinement	1.103
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
254880 (current)	2020-08-06	cif/ Updating files of 7126642, 7126643 Original log message: Adding full bibliography for 7126642--7126643.cif.	7126642.cif
252656	2020-06-05	cif/ Adding structures of 7126642, 7126643 via cif-deposit CGI script.	7126642.cif