Crystallography Open Database

Information card for entry 7127406

Preview

Coordinates	7127406.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H54 Cl Ge N3 Si6
Calculated formula	C18 H54 Cl Ge N3 Si6
Title of publication	Hydrophosphination using [GeCl{N(SiMe<sub>3</sub>)<sub>2</sub>}<sub>3</sub>] as a pre-catalyst.
Authors of publication	Barrett, A. N.; Sanderson, H. J.; Mahon, M. F.; Webster, R. L.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	88
Pages of publication	13623 - 13626
a	17.85648 ± 0.00015 Å
b	17.85648 ± 0.00015 Å
c	16.97342 ± 0.00015 Å
α	90°
β	90°
γ	120°
Cell volume	4686.96 ± 0.07 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	6
Space group number	161
Hermann-Mauguin space group symbol	R 3 c :H
Hall space group symbol	R 3 -2"c
Residual factor for all reflections	0.0193
Residual factor for significantly intense reflections	0.0193
Weighted residual factors for significantly intense reflections	0.0516
Weighted residual factors for all reflections included in the refinement	0.0516
Goodness-of-fit parameter for all reflections included in the refinement	1.111
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
260635 (current)	2021-01-07	cif/ Updating files of 7127406 Original log message: Adding full bibliography for 7127406.cif.	7127406.cif
258282	2020-10-10	cif/ Adding structures of 7127406 via cif-deposit CGI script.	7127406.cif