Crystallography Open Database

Information card for entry 7127479

Preview

Coordinates	7127479.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C134 H204 K2 La2 N4 O13 P6
Calculated formula	C134 H204 K2 La2 N4 O13 P6
Title of publication	A transient lanthanum phosphinidene complex.
Authors of publication	Watt, Fabian A.; McCabe, Karl N.; Schoch, Roland; Maron, Laurent; Hohloch, Stephan
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	98
Pages of publication	15410 - 15413
a	14.0506 ± 0.0008 Å
b	14.3744 ± 0.0008 Å
c	18.1614 ± 0.001 Å
α	99.417 ± 0.002°
β	90.617 ± 0.002°
γ	91.294 ± 0.002°
Cell volume	3617.3 ± 0.4 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.04
Residual factor for significantly intense reflections	0.0326
Weighted residual factors for significantly intense reflections	0.0906
Weighted residual factors for all reflections included in the refinement	0.0979
Goodness-of-fit parameter for all reflections included in the refinement	1.11
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
260647 (current)	2021-01-07	cif/ Updating files of 7127476, 7127477, 7127478, 7127479 Original log message: Adding full bibliography for 7127476--7127479.cif.	7127479.cif
259379	2020-12-01	cif/ Adding structures of 7127476, 7127477, 7127478, 7127479 via cif-deposit CGI script.	7127479.cif