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Information card for entry 7128126
Preview
| Coordinates | 7128126.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C86 H70 Cl2 F12 N2 O2 P4 Pd2 Sb2 |
|---|---|
| Calculated formula | C86 H70 Cl2 F12 N2 O2 P4 Pd2 Sb2 |
| Title of publication | Novel approach to benzo-fused 1,2-azaphospholene involving a Pd(II)-assisted tandem P-C bond cleavage and P-N bond formation reaction. |
| Authors of publication | Kunchur, Harish S.; Radhakrishna, Latchupatula; Pandey, Madhusudan K.; Balakrishna, Maravanji S. |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2021 |
| Journal volume | 57 |
| Journal issue | 39 |
| Pages of publication | 4835 - 4838 |
| a | 12.7967 ± 0.0004 Å |
| b | 14.2667 ± 0.0004 Å |
| c | 14.5382 ± 0.0004 Å |
| α | 63.884 ± 0.002° |
| β | 64.063 ± 0.003° |
| γ | 63.623 ± 0.003° |
| Cell volume | 2036.34 ± 0.12 Å3 |
| Cell temperature | 150 K |
| Ambient diffraction temperature | 150 K |
| Number of distinct elements | 9 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0627 |
| Residual factor for significantly intense reflections | 0.0555 |
| Weighted residual factors for significantly intense reflections | 0.1422 |
| Weighted residual factors for all reflections included in the refinement | 0.1494 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.079 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 265874 (current) | 2021-06-05 | cif/ Updating files of 7128125, 7128126, 7128127, 7128128 Original log message: Adding full bibliography for 7128125--7128128.cif. |
7128126.cif |
| 263876 | 2021-04-06 | cif/ Adding structures of 7128125, 7128126, 7128127, 7128128 via cif-deposit CGI script. |
7128126.cif |
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Users of the data should acknowledge the original authors of the
structural data.