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Information card for entry 7128207
Preview
| Coordinates | 7128207.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H54 Cl3 Li N4 P2 Si2 U |
|---|---|
| Calculated formula | C37 H54 Cl3 Li N4 P2 Si2 U |
| Title of publication | Fragmentation, catenation, and direct functionalisation of white phosphorus by a uranium(IV)-silyl-phosphino-carbene complex. |
| Authors of publication | Boronski, Josef T.; Seed, John A.; Wooles, Ashley J.; Liddle, Stephen T. |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2021 |
| Journal volume | 57 |
| Journal issue | 41 |
| Pages of publication | 5090 - 5093 |
| a | 12.67099 ± 0.00017 Å |
| b | 21.463 ± 0.0002 Å |
| c | 16.66143 ± 0.00017 Å |
| α | 90° |
| β | 93.0428 ± 0.0011° |
| γ | 90° |
| Cell volume | 4524.81 ± 0.09 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.047 |
| Residual factor for significantly intense reflections | 0.0453 |
| Weighted residual factors for significantly intense reflections | 0.1223 |
| Weighted residual factors for all reflections included in the refinement | 0.124 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 265854 (current) | 2021-06-05 | cif/ Updating files of 7128206, 7128207, 7128208 Original log message: Adding full bibliography for 7128206--7128208.cif. |
7128207.cif |
| 264343 | 2021-04-21 | cif/ Adding structures of 7128206, 7128207, 7128208 via cif-deposit CGI script. |
7128207.cif |
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Users of the data should acknowledge the original authors of the
structural data.