Crystallography Open Database

Information card for entry 7128932

Preview

Coordinates	7128932.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C162 H176 B2 N8 O7 P2 Pd4
Calculated formula	C162 H176 B2 N8 O7 P2 Pd4
Title of publication	Construction of modular Pd/Cu multimetallic chains via ligand- and anion-controlled metal-metal interactions
Authors of publication	Rivada Wheelaghan, Orestes; Deolka, Shubham; Govindarajan, Ramadoss; Khaskin, Eugene; Fayzullin, Robert R.; Pal, Shrinwantu; Khusnutdinova, Julia R.
Journal of publication	Chemical Communications
Year of publication	2021
a	14.63077 ± 0.0001 Å
b	18.4543 ± 0.0002 Å
c	27.6768 ± 0.0002 Å
α	72.6084 ± 0.0008°
β	86.4096 ± 0.0006°
γ	71.5611 ± 0.0008°
Cell volume	6760.82 ± 0.11 Å³
Cell temperature	95 ± 2 K
Ambient diffraction temperature	95 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0512
Residual factor for significantly intense reflections	0.0497
Weighted residual factors for significantly intense reflections	0.1367
Weighted residual factors for all reflections included in the refinement	0.138
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268367 (current)	2021-09-03	cif/ Adding structures of 7128926, 7128927, 7128928, 7128929, 7128930, 7128931, 7128932, 7128933 via cif-deposit CGI script.	7128932.cif