Crystallography Open Database

Information card for entry 7128937

Preview

Coordinates	7128937.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H35 Cl N4 Pt
Calculated formula	C22 H35 Cl N4 Pt
SMILES	C12N(C=CN1CCCN(C)C)C(C)=[N](c1c(cccc1C(C)C)C(C)C)[PtH]=2Cl
Title of publication	Imidazolium salts and [Pt(cod)<sub>2</sub>]: from NHC hydrido complexes to the unprecedented olefinic tetrahedral cluster [Pt<sub>4</sub>(μ-H)(cod)<sub>4</sub>]BF<sub>4</sub>.
Authors of publication	He, Fengkai; Gourlaouen, Christophe; Pang, Huan; Braunstein, Pierre
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2021
Journal volume	57
Journal issue	78
Pages of publication	10039 - 10042
a	14.6958 ± 0.0008 Å
b	13.8722 ± 0.0007 Å
c	12.7246 ± 0.0006 Å
α	90°
β	112.646 ± 0.002°
γ	90°
Cell volume	2394.1 ± 0.2 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0276
Residual factor for significantly intense reflections	0.0204
Weighted residual factors for significantly intense reflections	0.0358
Weighted residual factors for all reflections included in the refinement	0.0386
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
269604 (current)	2021-10-06	cif/ Updating files of 7128934, 7128935, 7128936, 7128937 Original log message: Adding full bibliography for 7128934--7128937.cif.	7128937.cif
268445	2021-09-04	cif/ Adding structures of 7128934, 7128935, 7128936, 7128937 via cif-deposit CGI script.	7128937.cif