Crystallography Open Database

Information card for entry 7130346

Preview

Coordinates	7130346.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C216 H180 N6 O72 Rh12
Calculated formula	C216 H180 N6 O72 Rh12
Title of publication	Synthesis of the Two Isomers of Heteroleptic Rh12L6L’6 Metal-Organic Polyhedra by Screening of Complementary Linkers
Authors of publication	Broto-Ribas, Anna; Gutiérrez, Susana; Imaz, Inhar; Carné-Sánchez, Arnau; Gándara, Felipe; Juanhuix, Judith; Maspoch, Daniel
Journal of publication	Chemical Communications
Year of publication	2022
a	31.2593 ± 0.0003 Å
b	31.2593 ± 0.0003 Å
c	73.3075 ± 0.001 Å
α	90°
β	90°
γ	120°
Cell volume	62035.1 ± 1.2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	167
Hermann-Mauguin space group symbol	R -3 c :H
Hall space group symbol	-R 3 2"c
Residual factor for all reflections	0.0846
Residual factor for significantly intense reflections	0.0695
Weighted residual factors for significantly intense reflections	0.2399
Weighted residual factors for all reflections included in the refinement	0.2525
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.82656 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
276785 (current)	2022-07-23	cif/ Adding structures of 7130335, 7130336, 7130337, 7130338, 7130339, 7130340, 7130341, 7130342, 7130343, 7130344, 7130345, 7130346 via cif-deposit CGI script.	7130346.cif