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Information card for entry 7130755
Preview
| Coordinates | 7130755.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C14 H29 B F3 N O8 |
|---|---|
| Calculated formula | C14 H29 B F3 N O8 |
| Title of publication | Monotrifluoroacetoxyborane-amines: Chemoselective reagents for challenging reductive aminations |
| Authors of publication | RAMACHANDRAN, P. Veeraraghavan Veeraghavan; Choudhary, Shivani |
| Journal of publication | Chemical Communications |
| Year of publication | 2022 |
| a | 13.3739 ± 0.0017 Å |
| b | 17.908 ± 0.002 Å |
| c | 8.4752 ± 0.0008 Å |
| α | 90° |
| β | 97.311 ± 0.004° |
| γ | 90° |
| Cell volume | 2013.3 ± 0.4 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.0943 |
| Residual factor for significantly intense reflections | 0.0473 |
| Weighted residual factors for significantly intense reflections | 0.0885 |
| Weighted residual factors for all reflections included in the refinement | 0.1053 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.008 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 278088 (current) | 2022-09-23 | cif/ Adding structures of 7130755 via cif-deposit CGI script. |
7130755.cif |
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Users of the data should acknowledge the original authors of the
structural data.