#------------------------------------------------------------------------------ #$Date: 2022-09-24 00:54:03 +0300 (Sat, 24 Sep 2022) $ #$Revision: 278130 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/13/07/7130760.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7130760 loop_ _publ_author_name 'Kim, Dooyoung' 'Gray, Thomas G.' 'Teets, Thomas S.' _publ_section_title ; Heteroleptic copper(i) charge-transfer chromophores with panchromatic absorption ; _journal_name_full 'Chemical Communications' _journal_paper_doi 10.1039/D2CC03873K _journal_year 2022 _chemical_formula_sum 'C35 H29 Cu N4' _chemical_formula_weight 569.16 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2022-06-15 deposited with the CCDC. 2022-09-14 downloaded from the CCDC. ; _cell_angle_alpha 102.097(5) _cell_angle_beta 99.622(5) _cell_angle_gamma 92.954(5) _cell_formula_units_Z 4 _cell_length_a 12.103(5) _cell_length_b 12.437(5) _cell_length_c 19.039(8) _cell_measurement_reflns_used 6664 _cell_measurement_temperature 123(2) _cell_measurement_theta_max 26.53 _cell_measurement_theta_min 2.21 _cell_volume 2752(2) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 123(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0485 _diffrn_reflns_av_unetI/netI 0.0573 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 38905 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.484 _diffrn_reflns_theta_min 1.112 _exptl_absorpt_coefficient_mu 0.826 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6880 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour black _exptl_crystal_density_diffrn 1.374 _exptl_crystal_description Blocks _exptl_crystal_F_000 1184 _exptl_crystal_size_max 0.280 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.337 _refine_diff_density_min -0.617 _refine_diff_density_rms 0.066 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.034 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 725 _refine_ls_number_reflns 12587 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.034 _refine_ls_R_factor_all 0.0702 _refine_ls_R_factor_gt 0.0416 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0471P)^2^+0.3218P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0969 _refine_ls_wR_factor_ref 0.1100 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8744 _reflns_number_total 12587 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2cc03873k6.cif _cod_data_source_block 4 _cod_original_cell_volume 2751(2) _cod_database_code 7130760 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.802 _shelx_estimated_absorpt_t_max 0.984 _shelx_res_file ; TITL dk4_a.res in P-1 dk4.res created by SHELXL-2018/3 at 16:04:25 on 10-Dec-2020 REM Old TITL dk4 in P-1 REM SHELXT solution in P-1: R1 0.123, Rweak 0.003, Alpha 0.041 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C70 N8 Cu2 CELL 0.71073 12.1027 12.4370 19.0386 102.097 99.622 92.954 ZERR 4.000 0.0053 0.0054 0.0082 0.005 0.005 0.005 LATT 1 SFAC C H N CU UNIT 140 116 16 4 TEMP -149.950 SIZE 0.02 0.15 0.28 L.S. 16 BOND LIST 6 FMAP 2 PLAN 20 acta WGHT 0.047100 0.321800 FVAR 0.23314 CU1 4 0.751121 0.945138 0.319324 11.00000 0.01538 0.02476 = 0.02882 0.01175 -0.00142 -0.00117 N1 3 0.643574 0.913328 0.222522 11.00000 0.01841 0.01690 = 0.02111 0.00531 0.00209 0.00101 N2 3 0.600039 0.911893 0.352503 11.00000 0.01583 0.01877 = 0.02031 0.00547 0.00211 0.00175 N3 3 0.827547 1.093984 0.336795 11.00000 0.01796 0.02273 = 0.02488 0.00950 0.00402 -0.00001 N4 3 0.880615 0.872871 0.355645 11.00000 0.01713 0.02190 = 0.02182 0.00625 0.00216 0.00086 C1 1 0.987566 1.236020 0.382586 11.00000 0.02667 0.02829 = 0.04582 0.00582 0.00118 -0.00416 AFIX 137 H1A 2 0.995246 1.253412 0.335657 11.00000 -1.50000 H1B 2 1.062065 1.242595 0.413471 11.00000 -1.50000 H1C 2 0.940117 1.287663 0.406996 11.00000 -1.50000 AFIX 0 C2 1 0.933863 1.119103 0.369651 11.00000 0.02059 0.02511 = 0.02292 0.00329 0.00614 -0.00140 C3 1 1.001858 1.042326 0.395462 11.00000 0.01495 0.02819 = 0.02714 -0.00004 0.00128 -0.00250 AFIX 43 H3 2 1.074543 1.071946 0.421781 11.00000 -1.20000 AFIX 0 C4 1 0.978599 0.928839 0.388225 11.00000 0.01619 0.02777 = 0.02007 0.00410 0.00360 0.00370 C5 1 1.073204 0.868103 0.419877 11.00000 0.01939 0.03460 = 0.03195 0.00705 0.00017 0.00587 AFIX 137 H5A 2 1.055917 0.847339 0.464004 11.00000 -1.50000 H5B 2 1.143596 0.916204 0.432300 11.00000 -1.50000 H5C 2 1.081314 0.801469 0.383807 11.00000 -1.50000 AFIX 0 C10 1 0.672176 0.918806 0.156376 11.00000 0.02639 0.01619 = 0.02181 0.00485 0.00412 0.00118 C11 1 0.786782 0.923228 0.150986 11.00000 0.02893 0.02650 = 0.02799 0.00685 0.00673 0.00184 AFIX 43 H11 2 0.842442 0.925587 0.193002 11.00000 -1.20000 AFIX 0 C12 1 0.818208 0.924136 0.085257 11.00000 0.03361 0.03110 = 0.03473 0.00909 0.01285 -0.00102 AFIX 43 H12 2 0.895702 0.927177 0.081907 11.00000 -1.20000 AFIX 0 C13 1 0.736632 0.920599 0.022742 11.00000 0.05102 0.02878 = 0.02493 0.00610 0.01291 -0.00380 AFIX 43 H13 2 0.759182 0.920702 -0.022705 11.00000 -1.20000 AFIX 0 C14 1 0.625357 0.917026 0.027050 11.00000 0.04349 0.02506 = 0.02179 0.00789 0.00133 -0.00064 AFIX 43 H14 2 0.570946 0.915324 -0.015467 11.00000 -1.20000 AFIX 0 C15 1 0.589775 0.915816 0.093814 11.00000 0.03343 0.01923 = 0.02245 0.00722 0.00210 0.00253 C16 1 0.475988 0.907274 0.101253 11.00000 0.02963 0.02456 = 0.02329 0.00542 -0.00553 0.00292 AFIX 43 H16 2 0.418420 0.905702 0.060373 11.00000 -1.20000 AFIX 0 C17 1 0.448350 0.901291 0.166512 11.00000 0.01915 0.02577 = 0.02935 0.00487 -0.00076 0.00504 AFIX 43 H17 2 0.371649 0.895476 0.171608 11.00000 -1.20000 AFIX 0 C18 1 0.534779 0.903789 0.226913 11.00000 0.02034 0.01819 = 0.02032 0.00327 -0.00041 0.00251 C20 1 0.584189 0.896823 0.419813 11.00000 0.01920 0.01816 = 0.02212 0.00406 0.00567 0.00348 C21 1 0.677202 0.916430 0.477285 11.00000 0.01836 0.02401 = 0.02375 0.00649 0.00403 0.00302 AFIX 43 H21 2 0.748734 0.941693 0.469652 11.00000 -1.20000 AFIX 0 C22 1 0.664736 0.899120 0.544310 11.00000 0.02457 0.02992 = 0.02315 0.00738 0.00283 0.00585 AFIX 43 H22 2 0.728309 0.911445 0.582696 11.00000 -1.20000 AFIX 0 C23 1 0.559583 0.863463 0.557251 11.00000 0.03472 0.02897 = 0.02345 0.00927 0.01075 0.00474 AFIX 43 H23 2 0.552573 0.851010 0.603930 11.00000 -1.20000 AFIX 0 C24 1 0.467452 0.846687 0.502809 11.00000 0.02565 0.02345 = 0.03085 0.00617 0.01237 0.00073 AFIX 43 H24 2 0.396002 0.824223 0.511992 11.00000 -1.20000 AFIX 0 C25 1 0.477894 0.862568 0.432962 11.00000 0.02152 0.01874 = 0.02398 0.00278 0.00737 0.00161 C26 1 0.385718 0.845504 0.374520 11.00000 0.01696 0.02424 = 0.03081 0.00291 0.00645 0.00001 AFIX 43 H26 2 0.312546 0.824206 0.381540 11.00000 -1.20000 AFIX 0 C27 1 0.402333 0.859738 0.308174 11.00000 0.01705 0.02520 = 0.02799 0.00196 0.00076 0.00166 AFIX 43 H27 2 0.340867 0.847515 0.268365 11.00000 -1.20000 AFIX 0 C28 1 0.511119 0.892745 0.298390 11.00000 0.01669 0.01530 = 0.02428 0.00223 0.00176 0.00325 C31 1 0.766850 1.172690 0.306239 11.00000 0.02270 0.01965 = 0.02314 0.00620 0.00024 -0.00560 C32 1 0.784847 1.196570 0.240710 11.00000 0.05411 0.03227 = 0.02906 0.01272 0.01294 0.00767 AFIX 43 H32 2 0.842666 1.164339 0.217564 11.00000 -1.20000 AFIX 0 C33 1 0.718099 1.267686 0.209118 11.00000 0.08120 0.03425 = 0.02709 0.01851 0.00347 0.00522 AFIX 43 H33 2 0.730507 1.283284 0.164156 11.00000 -1.20000 AFIX 0 C34 1 0.634845 1.315598 0.241666 11.00000 0.04722 0.02645 = 0.04427 0.01175 -0.01480 0.00193 AFIX 43 H34 2 0.590303 1.364852 0.219948 11.00000 -1.20000 AFIX 0 C35 1 0.616535 1.291533 0.306149 11.00000 0.02636 0.03122 = 0.04949 0.01002 0.00098 0.00219 AFIX 43 H35 2 0.558748 1.324226 0.329107 11.00000 -1.20000 AFIX 0 C36 1 0.681487 1.220093 0.338001 11.00000 0.02825 0.03107 = 0.03269 0.01327 0.00532 0.00086 AFIX 43 H36 2 0.667127 1.203472 0.382297 11.00000 -1.20000 AFIX 0 C41 1 0.867170 0.756831 0.349533 11.00000 0.01130 0.02533 = 0.03004 0.00912 0.00154 0.00281 C42 1 0.835332 0.713621 0.405415 11.00000 0.02643 0.03297 = 0.03782 0.01809 0.01259 0.01272 AFIX 43 H42 2 0.825280 0.762093 0.449147 11.00000 -1.20000 AFIX 0 C43 1 0.818042 0.600545 0.398127 11.00000 0.02411 0.04022 = 0.06020 0.02918 0.01215 0.00916 AFIX 43 H43 2 0.795975 0.572169 0.436787 11.00000 -1.20000 AFIX 0 C44 1 0.832620 0.528898 0.335196 11.00000 0.02365 0.02324 = 0.06742 0.01413 -0.00541 0.00071 AFIX 43 H44 2 0.821446 0.451358 0.330468 11.00000 -1.20000 AFIX 0 C45 1 0.863667 0.571179 0.279091 11.00000 0.02548 0.03373 = 0.04187 -0.00149 -0.00705 0.00484 AFIX 43 H45 2 0.873770 0.522386 0.235497 11.00000 -1.20000 AFIX 0 C46 1 0.880172 0.684181 0.285930 11.00000 0.01751 0.02875 = 0.02867 0.00412 -0.00205 0.00046 AFIX 43 H46 2 0.900591 0.712261 0.246715 11.00000 -1.20000 AFIX 0 CU1A 4 0.226690 0.558337 0.182317 11.00000 0.01461 0.02271 = 0.02979 0.01016 -0.00193 -0.00089 N1A 3 0.322735 0.582203 0.284050 11.00000 0.01763 0.01915 = 0.02241 0.00596 0.00162 0.00179 N2A 3 0.385768 0.589663 0.160103 11.00000 0.01641 0.01680 = 0.02389 0.00414 0.00245 0.00129 N3A 3 0.097203 0.628062 0.142254 11.00000 0.01724 0.01978 = 0.02014 0.00536 0.00129 0.00201 N4A 3 0.154381 0.406677 0.159749 11.00000 0.01652 0.02140 = 0.02276 0.00764 0.00280 0.00079 C1A 1 -0.095525 0.626969 0.074668 11.00000 0.01752 0.02628 = 0.03068 0.00758 0.00031 0.00328 AFIX 137 H1A1 2 -0.099496 0.698720 0.106928 11.00000 -1.50000 H1A2 2 -0.166447 0.581251 0.068228 11.00000 -1.50000 H1A3 2 -0.082740 0.637955 0.027070 11.00000 -1.50000 AFIX 0 C2A 1 0.000490 0.569742 0.108336 11.00000 0.01559 0.02757 = 0.01667 0.00644 0.00338 0.00336 C3A 1 -0.020944 0.456409 0.102329 11.00000 0.01561 0.02398 = 0.02159 0.00502 0.00117 -0.00275 AFIX 43 H3A 2 -0.094164 0.426141 0.077387 11.00000 -1.20000 AFIX 0 C4A 1 0.048521 0.380251 0.127292 11.00000 0.01984 0.02100 = 0.01835 0.00538 0.00387 -0.00236 C5A 1 -0.001818 0.262489 0.114084 11.00000 0.02528 0.02553 = 0.03657 0.01207 -0.00238 -0.00459 AFIX 137 H5A1 2 0.040760 0.213635 0.083386 11.00000 -1.50000 H5A2 2 -0.080406 0.256676 0.089362 11.00000 -1.50000 H5A3 2 0.001535 0.240758 0.160935 11.00000 -1.50000 AFIX 0 C10A 1 0.284193 0.577468 0.347173 11.00000 0.02307 0.01550 = 0.02449 0.00370 0.00370 0.00353 C11A 1 0.166975 0.577355 0.346527 11.00000 0.02224 0.02684 = 0.02827 0.00947 0.00353 0.00262 AFIX 43 H11A 2 0.116600 0.574575 0.302065 11.00000 -1.20000 AFIX 0 C12A 1 0.126274 0.581214 0.409371 11.00000 0.02877 0.03323 = 0.03789 0.01568 0.01197 0.00821 AFIX 43 H12A 2 0.047573 0.581499 0.408478 11.00000 -1.20000 AFIX 0 C13A 1 0.199466 0.584782 0.475566 11.00000 0.03960 0.03613 = 0.03217 0.01588 0.01528 0.01320 AFIX 43 H13A 2 0.170144 0.589112 0.519253 11.00000 -1.20000 AFIX 0 C14A 1 0.312134 0.582066 0.477392 11.00000 0.03767 0.03637 = 0.02756 0.01387 0.00595 0.01168 AFIX 43 H14A 2 0.360820 0.582962 0.522205 11.00000 -1.20000 AFIX 0 C15A 1 0.357085 0.577943 0.413492 11.00000 0.02680 0.02143 = 0.02697 0.00823 0.00166 0.00573 C16A 1 0.473571 0.578419 0.411810 11.00000 0.02419 0.03511 = 0.02959 0.00958 -0.00283 0.00921 AFIX 43 H16A 2 0.525541 0.576368 0.454728 11.00000 -1.20000 AFIX 0 C17A 1 0.510984 0.581793 0.349107 11.00000 0.01840 0.03273 = 0.02970 0.00720 -0.00140 0.00654 AFIX 43 H17A 2 0.589072 0.581415 0.347740 11.00000 -1.20000 AFIX 0 C18A 1 0.432969 0.585896 0.285462 11.00000 0.01827 0.01686 = 0.02710 0.00282 -0.00032 0.00285 C20A 1 0.413076 0.606795 0.095680 11.00000 0.02017 0.01457 = 0.02557 0.00480 0.00570 0.00082 C21A 1 0.325855 0.597929 0.035019 11.00000 0.01753 0.02455 = 0.02834 0.00757 0.00375 0.00134 AFIX 43 H21A 2 0.250201 0.580001 0.038948 11.00000 -1.20000 AFIX 0 C22A 1 0.350425 0.615178 -0.029366 11.00000 0.02576 0.02882 = 0.02970 0.00973 0.00417 0.00182 AFIX 43 H22A 2 0.291175 0.610019 -0.069864 11.00000 -1.20000 AFIX 0 C23A 1 0.462033 0.640486 -0.036849 11.00000 0.03174 0.02534 = 0.03019 0.00957 0.01038 0.00209 AFIX 43 H23A 2 0.477659 0.651734 -0.082177 11.00000 -1.20000 AFIX 0 C24A 1 0.547541 0.648810 0.021016 11.00000 0.02272 0.02285 = 0.03599 0.00719 0.01153 -0.00004 AFIX 43 H24A 2 0.622774 0.665594 0.015738 11.00000 -1.20000 AFIX 0 C25A 1 0.525463 0.632761 0.088633 11.00000 0.01968 0.01730 = 0.03116 0.00374 0.00668 0.00135 C26A 1 0.609845 0.641114 0.150519 11.00000 0.01491 0.02406 = 0.03822 0.00418 0.00672 0.00033 AFIX 43 H26A 2 0.686252 0.658085 0.147832 11.00000 -1.20000 AFIX 0 C27A 1 0.582582 0.625057 0.213913 11.00000 0.01489 0.02544 = 0.02949 0.00207 0.00048 -0.00004 AFIX 43 H27A 2 0.639569 0.631113 0.255783 11.00000 -1.20000 AFIX 0 C28A 1 0.468548 0.599169 0.217429 11.00000 0.01665 0.01651 = 0.02732 0.00341 0.00221 0.00336 C31A 1 0.108925 0.743248 0.144689 11.00000 0.01214 0.02250 = 0.02862 0.00804 0.00042 0.00206 C32A 1 0.111224 0.819403 0.209643 11.00000 0.02158 0.02840 = 0.02847 0.00562 -0.00125 0.00032 AFIX 43 H32A 2 0.104600 0.794298 0.252699 11.00000 -1.20000 AFIX 0 C33A 1 0.123114 0.932124 0.212488 11.00000 0.03132 0.02624 = 0.04017 -0.00269 -0.00529 0.00250 AFIX 43 H33A 2 0.123557 0.983351 0.257241 11.00000 -1.20000 AFIX 0 C34A 1 0.134253 0.969912 0.150784 11.00000 0.02845 0.02006 = 0.05168 0.01022 -0.00415 -0.00042 AFIX 43 H34A 2 0.142045 1.046919 0.152682 11.00000 -1.20000 AFIX 0 C35A 1 0.133972 0.894946 0.086389 11.00000 0.02924 0.03105 = 0.04573 0.02030 0.00475 0.00149 AFIX 43 H35A 2 0.142377 0.920482 0.043752 11.00000 -1.20000 AFIX 0 C36A 1 0.121495 0.782064 0.083096 11.00000 0.02697 0.02739 = 0.02833 0.00713 0.00645 0.00261 AFIX 43 H36A 2 0.121593 0.731199 0.038275 11.00000 -1.20000 AFIX 0 C41A 1 0.217149 0.326754 0.187288 11.00000 0.01960 0.01668 = 0.02314 0.00619 0.00002 -0.00090 C42A 1 0.298475 0.278023 0.151143 11.00000 0.02581 0.02785 = 0.02478 0.00704 0.00390 0.00170 AFIX 43 H42A 2 0.310268 0.296921 0.106967 11.00000 -1.20000 AFIX 0 C43A 1 0.362796 0.202005 0.178754 11.00000 0.02619 0.02868 = 0.03454 0.00246 0.00152 0.00512 AFIX 43 H43A 2 0.417303 0.168219 0.153000 11.00000 -1.20000 AFIX 0 C44A 1 0.347863 0.175372 0.243394 11.00000 0.03280 0.02257 = 0.03169 0.00648 -0.00779 0.00480 AFIX 43 H44A 2 0.391434 0.122843 0.262134 11.00000 -1.20000 AFIX 0 C45A 1 0.269485 0.225317 0.280607 11.00000 0.04536 0.02715 = 0.02404 0.01198 0.00105 0.00430 AFIX 43 H45A 2 0.259895 0.207879 0.325592 11.00000 -1.20000 AFIX 0 C46A 1 0.204083 0.301068 0.253156 11.00000 0.03381 0.02543 = 0.02557 0.00754 0.00669 0.00512 AFIX 43 H46A 2 0.150396 0.335300 0.279477 11.00000 -1.20000 AFIX 0 HKLF 4 REM dk4_a.res in P-1 REM wR2 = 0.1100, GooF = S = 1.034, Restrained GooF = 1.034 for all data REM R1 = 0.0416 for 8744 Fo > 4sig(Fo) and 0.0702 for all 12587 data REM 725 parameters refined using 0 restraints END WGHT 0.0471 0.3218 REM Highest difference peak 0.337, deepest hole -0.617, 1-sigma level 0.066 Q1 1 0.9488 1.2855 0.3522 11.00000 0.05 0.34 Q2 1 0.4101 0.5831 0.4132 11.00000 0.05 0.33 Q3 1 0.8700 1.1024 0.3545 11.00000 0.05 0.33 Q4 1 0.5253 0.6135 0.2163 11.00000 0.05 0.32 Q5 1 -0.0480 0.6080 0.0966 11.00000 0.05 0.32 Q6 1 0.1669 0.6023 0.1356 11.00000 0.05 0.31 Q7 1 0.1026 0.3994 0.1456 11.00000 0.05 0.30 Q8 1 0.1004 0.7827 0.1733 11.00000 0.05 0.30 Q9 1 0.2606 0.4989 0.2221 11.00000 0.05 0.29 Q10 1 0.9964 0.9851 0.3658 11.00000 0.05 0.29 Q11 1 0.9483 1.0847 0.3991 11.00000 0.05 0.29 Q12 1 0.8100 0.9016 0.3646 11.00000 0.05 0.29 Q13 1 0.5275 0.9066 0.2646 11.00000 0.05 0.29 Q14 1 0.2276 0.5850 0.3489 11.00000 0.05 0.29 Q15 1 0.4339 0.5647 0.1841 11.00000 0.05 0.28 Q16 1 0.9624 1.1797 0.3545 11.00000 0.05 0.27 Q17 1 0.4373 0.8645 0.4039 11.00000 0.05 0.27 Q18 1 0.5384 0.6213 0.0573 11.00000 0.05 0.27 Q19 1 0.8437 0.9528 0.3665 11.00000 0.05 0.27 Q20 1 0.5239 0.8867 0.4235 11.00000 0.05 0.27 ; _shelx_res_checksum 32368 _shelx_hkl_file ; -1 0 0 187.58 5.60 -1 0 0 182.68 5.50 -1 0 0 177.78 5.50 1 0 0 170.08 5.50 1 0 0 195.38 5.60 -2 0 0 152.18 5.30 -2 0 0 158.78 5.20 -2 0 0 157.38 4.70 -2 0 0 160.68 5.30 2 0 0 157.58 5.20 2 0 0 164.78 4.70 2 0 0 152.38 5.30 -3 0 0 233.08 7.70 -3 0 0 225.78 7.60 -3 0 0 226.28 7.60 3 0 0 230.38 7.70 3 0 0 221.18 7.60 3 0 0 232.58 6.90 -4 0 0 20.50 2.00 -4 0 0 21.60 1.90 -4 0 0 23.30 2.00 4 0 0 19.30 1.90 4 0 0 21.40 1.20 4 0 0 25.30 2.00 -5 0 0 45.10 3.00 -5 0 0 41.90 2.90 -5 0 0 43.20 3.00 5 0 0 49.40 3.10 5 0 0 46.70 2.00 5 0 0 48.40 3.10 -6 0 0 5.40 1.50 -6 0 0 5.00 1.40 6 0 0 3.30 1.20 6 0 0 5.50 0.80 6 0 0 3.20 1.30 -7 0 0 4.90 1.40 -7 0 0 8.50 1.80 7 0 0 6.20 1.70 7 0 0 7.50 1.00 7 0 0 3.90 1.30 -8 0 0 292.37 11.90 -8 0 0 307.67 11.80 8 0 0 319.27 12.00 8 0 0 301.67 11.90 -9 0 0 169.68 8.30 -9 0 0 169.68 8.00 9 0 0 163.58 8.20 9 0 0 163.88 8.10 -10 0 0 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-4 0 230.48 9.60 -7 -4 0 213.98 9.30 -7 -4 0 223.88 8.00 7 4 0 212.28 8.60 7 4 0 215.08 9.10 -8 -4 0 288.27 11.40 -8 -4 0 254.47 10.30 -8 -4 0 265.27 11.10 8 4 0 264.47 10.40 8 4 0 251.27 10.80 -9 -4 0 5.40 2.20 -9 -4 0 6.70 2.30 9 4 0 7.60 2.10 9 4 0 5.40 2.00 -10 -4 0 99.49 6.80 -10 -4 0 113.29 7.20 10 4 0 100.69 6.60 10 4 0 104.59 6.30 -11 -4 0 -2.30 1.70 -11 -4 0 -0.20 1.90 11 4 0 0.30 1.60 11 4 0 0.30 1.50 -12 -4 0 37.30 5.40 -12 -4 0 39.50 5.60 12 4 0 40.10 5.30 12 4 0 33.30 4.50 -13 -4 0 37.00 5.70 -13 -4 0 42.60 5.70 13 4 0 48.70 5.90 13 4 0 32.00 5.30 -14 -4 0 0.70 2.90 -14 -4 0 2.20 2.90 14 4 0 -0.70 2.50 15 -5 0 29.40 5.70 15 -5 0 18.70 4.70 -15 5 0 16.20 4.20 -15 5 0 17.60 4.40 14 -5 0 1.90 2.90 14 -5 0 0.00 2.40 -14 5 0 3.90 2.80 -14 5 0 2.00 2.60 13 -5 0 53.69 6.70 13 -5 0 58.49 6.70 -13 5 0 51.79 6.30 -13 5 0 47.30 5.80 12 -5 0 0.30 2.00 12 -5 0 -1.30 2.10 -12 5 0 -0.90 1.70 -12 5 0 0.80 1.80 11 -5 0 73.79 7.10 11 -5 0 74.79 5.70 -11 5 0 65.29 5.40 -11 5 0 62.89 5.50 10 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-3 -5 0 25.90 1.70 -3 -5 0 29.10 2.30 3 5 0 31.60 3.10 3 5 0 29.10 1.80 3 5 0 31.50 2.10 -4 -5 0 4.90 1.60 -4 -5 0 8.60 1.30 -4 -5 0 5.70 1.30 4 5 0 4.00 1.10 4 5 0 5.40 1.20 4 5 0 5.30 1.60 -5 -5 0 24.70 2.70 -5 -5 0 22.40 2.20 -5 -5 0 29.40 3.30 -5 -5 0 22.40 2.30 5 5 0 19.20 2.60 5 5 0 22.40 2.30 5 5 0 26.00 2.60 -6 -5 0 9.00 2.20 -6 -5 0 9.30 1.60 -6 -5 0 6.90 1.70 6 5 0 7.80 1.60 6 5 0 9.50 1.90 6 5 0 6.60 1.80 -7 -5 0 6.20 1.50 -7 -5 0 16.40 2.90 -7 -5 0 9.00 2.10 -7 -5 0 9.30 1.70 7 5 0 10.30 2.30 7 5 0 11.60 2.10 7 5 0 12.10 2.10 -8 -5 0 22.60 3.40 -8 -5 0 22.50 3.30 8 5 0 34.10 4.30 8 5 0 26.00 3.30 8 5 0 25.20 3.10 -9 -5 0 -0.40 1.50 -9 -5 0 2.10 1.80 9 5 0 1.20 1.50 9 5 0 -0.70 1.50 9 5 0 2.40 1.70 -10 -5 0 86.89 6.40 -10 -5 0 74.29 6.00 10 5 0 76.19 5.80 10 5 0 78.99 5.50 -11 -5 0 23.80 4.10 -11 -5 0 26.10 4.30 -12 -5 0 2.60 2.30 -12 -5 0 2.50 2.60 12 5 0 2.60 2.40 -13 -5 0 25.80 4.80 -13 -5 0 23.00 4.80 13 5 0 27.10 4.60 -14 -5 0 12.60 4.30 14 5 0 12.30 3.80 14 -6 0 21.60 4.50 14 -6 0 17.70 4.50 -14 6 0 23.10 4.50 -14 6 0 23.40 5.00 13 -6 0 3.90 3.10 13 -6 0 3.40 2.60 -13 6 0 -0.60 2.30 -13 6 0 1.10 2.20 12 -6 0 71.79 6.20 12 -6 0 74.09 7.20 -12 6 0 77.79 7.50 -12 6 0 76.99 7.30 11 -6 0 -1.10 2.00 11 -6 0 -0.50 1.70 -11 6 0 1.90 2.00 -11 6 0 1.50 1.70 10 -6 0 1.10 1.70 10 -6 0 1.50 2.00 -10 6 0 2.90 2.00 -10 6 0 1.50 1.70 9 -6 0 33.70 4.00 9 -6 0 25.30 3.80 -9 6 0 26.00 3.40 -9 6 0 23.20 3.80 8 -6 0 32.20 3.90 8 -6 0 28.10 3.40 -8 6 0 30.40 3.50 -8 6 0 26.30 3.50 7 -6 0 130.89 5.80 7 -6 0 133.19 6.70 7 -6 0 124.49 6.20 -7 6 0 133.49 6.30 -7 6 0 130.99 7.00 6 -6 0 48.50 3.60 6 -6 0 48.60 3.20 -6 6 0 44.00 3.20 -6 6 0 42.10 4.20 5 -6 0 249.78 9.10 5 -6 0 247.78 9.60 5 -6 0 257.37 9.40 -5 6 0 259.57 9.10 -5 6 0 251.57 10.20 4 -6 0 42.40 2.90 4 -6 0 39.00 2.40 4 -6 0 43.00 2.90 -4 6 0 39.40 3.30 -4 6 0 40.90 2.50 3 -6 0 128.09 5.60 -3 6 0 125.79 4.70 -3 6 0 127.49 6.10 2 -6 0 67.99 3.70 2 -6 0 66.89 3.20 -2 6 0 66.09 2.60 -2 6 0 62.49 4.00 1 -6 0 167.48 6.90 1 -6 0 173.98 6.00 -1 6 0 177.08 7.40 -1 6 0 173.28 5.30 0 -6 0 2390.36 68.59 0 -6 0 2378.76 69.99 0 6 0 2493.95 70.69 -1 -6 0 142.29 6.10 -1 -6 0 141.29 4.70 1 6 0 146.49 6.60 1 6 0 143.79 4.70 -2 -6 0 150.38 5.10 -2 -6 0 145.59 6.30 -2 -6 0 163.98 7.10 2 6 0 150.88 5.40 2 6 0 166.58 7.00 -3 -6 0 95.19 3.70 -3 -6 0 99.29 4.70 -3 -6 0 90.49 5.10 3 6 0 92.99 4.00 3 6 0 93.79 5.20 3 6 0 99.99 3.80 -4 -6 0 9.90 2.20 -4 -6 0 8.60 1.70 -4 -6 0 8.90 1.30 4 6 0 11.20 1.50 4 6 0 12.00 1.70 4 6 0 8.90 2.00 -5 -6 0 333.57 11.90 -5 -6 0 334.17 13.00 5 6 0 352.56 11.40 5 6 0 346.37 11.90 5 6 0 321.77 12.80 -6 -6 0 210.48 8.40 -6 -6 0 251.17 10.30 -6 -6 0 235.58 9.30 -6 -6 0 224.58 8.80 6 6 0 232.28 8.60 6 6 0 234.28 9.20 6 6 0 215.38 9.80 -7 -6 0 20.50 3.40 -7 -6 0 20.70 2.90 -7 -6 0 17.00 2.40 7 6 0 16.20 2.90 7 6 0 12.60 2.30 -8 -6 0 4.80 2.00 -8 -6 0 6.70 2.50 8 6 0 6.30 2.20 8 6 0 3.40 1.60 -9 -6 0 116.39 6.90 -9 -6 0 111.79 7.20 9 6 0 101.59 6.50 9 6 0 96.29 6.70 -10 -6 0 8.80 2.90 -10 -6 0 4.70 2.40 10 6 0 5.40 2.50 10 6 0 5.30 2.30 -11 -6 0 47.80 5.60 -11 -6 0 55.89 6.30 11 6 0 50.09 6.00 11 6 0 53.39 5.70 -12 -6 0 -2.30 2.30 12 6 0 0.20 2.10 12 6 0 2.20 2.10 -13 -6 0 11.00 4.00 13 6 0 15.30 4.00 13 6 0 11.50 3.70 14 -7 0 32.60 5.40 14 -7 0 27.20 5.10 -14 7 0 20.10 4.30 -14 7 0 32.50 5.80 13 -7 0 30.10 5.10 13 -7 0 37.70 5.50 -13 7 0 30.20 4.90 -13 7 0 45.10 6.20 12 -7 0 -1.20 1.90 12 -7 0 2.70 2.80 -12 7 0 -0.30 1.90 -12 7 0 1.70 2.20 11 -7 0 46.20 5.10 11 -7 0 59.09 6.50 -11 7 0 60.89 6.20 -11 7 0 46.10 5.10 10 -7 0 1.30 1.80 10 -7 0 3.80 2.40 -10 7 0 1.40 1.80 -10 7 0 -0.20 1.40 9 -7 0 4.60 2.20 9 -7 0 7.50 2.20 -9 7 0 3.60 2.00 -9 7 0 3.10 1.70 8 -7 0 6.60 1.60 8 -7 0 5.70 2.30 8 -7 0 7.10 1.90 -8 7 0 6.50 2.00 -8 7 0 6.70 2.20 7 -7 0 0.00 0.80 7 -7 0 0.50 0.90 7 -7 0 1.30 1.60 -7 7 0 5.00 1.60 -7 7 0 0.20 1.20 6 -7 0 -0.10 0.90 6 -7 0 0.30 1.00 6 -7 0 0.40 1.20 -6 7 0 -0.20 1.00 -6 7 0 -0.10 1.10 5 -7 0 12.30 2.10 5 -7 0 10.30 1.80 5 -7 0 11.70 1.70 -5 7 0 8.60 1.50 -5 7 0 8.20 2.10 4 -7 0 13.50 2.10 4 -7 0 10.50 1.80 4 -7 0 11.50 1.50 -4 7 0 9.40 1.30 -4 7 0 11.90 2.30 3 -7 0 51.69 3.00 3 -7 0 47.60 2.30 3 -7 0 48.90 3.40 -3 7 0 48.40 3.80 -3 7 0 46.30 2.30 2 -7 0 0.10 0.70 2 -7 0 0.00 0.90 -2 7 0 -0.20 0.40 -2 7 0 1.70 1.30 1 -7 0 9.60 1.80 1 -7 0 9.80 1.30 -1 7 0 8.60 1.90 0 -7 0 4.10 1.40 0 -7 0 4.00 0.80 0 7 0 2.10 1.10 -1 -7 0 -0.60 0.50 -1 -7 0 -1.10 0.80 1 7 0 0.60 0.40 1 7 0 0.30 1.10 -2 -7 0 0.40 1.00 -2 -7 0 -0.80 0.50 2 7 0 -0.20 0.50 2 7 0 1.10 1.10 -3 -7 0 7.90 2.10 -3 -7 0 10.00 1.80 3 7 0 9.00 1.30 3 7 0 6.70 1.70 3 7 0 9.40 1.30 -4 -7 0 10.10 2.30 -4 -7 0 11.60 2.00 4 7 0 10.80 1.60 4 7 0 6.70 2.00 -5 -7 0 2.60 1.30 -5 -7 0 0.90 1.60 5 7 0 1.00 1.00 5 7 0 1.40 1.50 -6 -7 0 58.19 5.40 -6 -7 0 48.00 3.80 6 7 0 52.79 3.70 6 7 0 57.59 4.60 -7 -7 0 5.10 2.20 -7 -7 0 7.50 2.00 7 7 0 3.90 1.50 7 7 0 4.70 2.00 -8 -7 0 3.90 2.40 8 7 0 9.90 2.30 8 7 0 6.90 2.60 -9 -7 0 1.50 2.20 9 7 0 0.20 1.50 9 7 0 2.70 2.00 -10 -7 0 48.20 6.00 10 7 0 49.90 5.20 10 7 0 39.60 5.20 -11 -7 0 -0.60 2.40 11 7 0 2.00 2.40 11 7 0 -1.40 1.60 -12 -7 0 50.09 6.60 12 7 0 52.09 6.00 12 7 0 40.20 6.00 -13 -7 0 0.70 3.20 13 7 0 9.40 3.40 13 7 0 2.50 2.90 14 -8 0 9.50 4.20 -14 8 0 11.50 3.90 13 -8 0 19.40 4.50 -13 8 0 17.00 4.30 12 -8 0 3.90 3.00 -12 8 0 -1.10 2.40 11 -8 0 0.20 2.00 -11 8 0 0.30 2.10 10 -8 0 33.60 4.60 -10 8 0 35.50 5.00 9 -8 0 32.40 4.50 -9 8 0 27.60 4.40 8 -8 0 64.99 5.10 8 -8 0 65.19 4.40 -8 8 0 68.79 5.40 7 -8 0 46.70 3.70 7 -8 0 47.20 4.60 -7 8 0 59.29 5.60 6 -8 0 3.50 1.50 6 -8 0 2.90 1.40 -6 8 0 1.40 1.50 5 -8 0 34.20 3.50 5 -8 0 40.00 3.30 -5 8 0 50.69 4.20 4 -8 0 139.29 6.70 -4 8 0 148.69 7.50 3 -8 0 93.99 5.10 3 -8 0 87.69 4.30 -3 8 0 86.09 5.40 2 -8 0 1596.84 48.30 2 -8 0 1625.34 47.00 -2 8 0 1618.24 49.20 1 -8 0 140.69 5.40 1 -8 0 145.69 6.70 -1 8 0 147.29 7.30 0 -8 0 258.67 10.30 0 8 0 277.97 11.10 -1 -8 0 52.09 3.80 1 8 0 50.89 4.10 -2 -8 0 73.89 4.50 2 8 0 65.49 4.80 -3 -8 0 85.19 5.00 3 8 0 85.79 5.50 -4 -8 0 133.69 6.50 -4 -8 0 145.39 7.50 4 8 0 114.19 6.90 -5 -8 0 154.38 8.20 -5 -8 0 145.69 7.10 5 8 0 153.98 8.00 -6 -8 0 27.30 4.10 6 8 0 29.60 4.10 -7 -8 0 33.40 3.70 -7 -8 0 27.60 4.20 7 8 0 23.60 3.90 -8 -8 0 86.59 6.80 8 8 0 95.09 6.70 -9 -8 0 58.89 6.40 9 8 0 53.39 5.90 -10 -8 0 2.30 3.00 10 8 0 10.20 3.30 -11 -8 0 48.10 6.20 11 8 0 40.00 5.90 -12 -8 0 8.20 3.80 12 8 0 11.40 3.90 13 -9 0 -1.90 2.70 -13 9 0 -0.60 2.40 12 -9 0 25.40 4.80 -12 9 0 22.30 4.70 11 -9 0 14.50 3.70 -11 9 0 21.80 4.30 10 -9 0 10.90 3.20 -10 9 0 9.60 3.10 9 -9 0 23.00 3.90 -9 9 0 24.70 4.30 8 -9 0 1.90 2.00 8 -9 0 3.90 1.70 -8 9 0 0.80 1.80 7 -9 0 11.60 2.30 7 -9 0 8.10 2.50 -7 9 0 5.80 2.20 6 -9 0 1.50 1.20 6 -9 0 1.90 1.60 -6 9 0 0.70 1.50 5 -9 0 5.20 1.70 5 -9 0 0.30 0.90 -5 9 0 3.60 2.00 4 -9 0 5.00 1.60 4 -9 0 6.20 1.80 -4 9 0 7.80 2.40 3 -9 0 31.60 3.60 -3 9 0 22.50 3.30 2 -9 0 5.30 1.70 -2 9 0 9.60 2.40 1 -9 0 2.70 1.30 -1 9 0 3.40 1.80 0 -9 0 0.30 1.20 0 9 0 0.10 1.20 -1 -9 0 0.90 1.30 1 9 0 -0.20 1.20 -2 -9 0 0.60 1.40 2 9 0 0.00 1.30 -3 -9 0 13.90 2.50 3 9 0 7.30 2.30 -4 -9 0 6.90 2.40 -4 -9 0 9.30 2.20 4 9 0 6.60 2.20 -5 -9 0 3.40 2.30 -5 -9 0 1.10 1.60 5 9 0 0.10 1.40 -6 -9 0 26.60 4.20 -6 -9 0 31.90 3.80 6 9 0 37.50 4.80 -7 -9 0 9.30 2.90 -7 -9 0 13.30 2.70 7 9 0 4.80 2.30 -8 -9 0 1.70 2.60 8 9 0 6.70 2.90 -9 -9 0 21.30 4.30 9 9 0 19.10 4.00 -10 -9 0 0.50 2.90 10 9 0 3.70 2.70 -11 -9 0 5.60 3.60 11 9 0 3.90 2.90 12 -10 0 4.10 3.30 -12 10 0 -1.40 2.40 11 -10 0 7.20 3.20 -11 10 0 16.50 4.00 10 -10 0 -1.10 2.40 -10 10 0 5.10 3.00 9 -10 0 15.40 3.30 -9 10 0 20.80 4.10 8 -10 0 55.59 5.50 8 -10 0 64.29 4.90 -8 10 0 62.99 6.50 7 -10 0 4.20 1.90 7 -10 0 6.00 2.40 -7 10 0 9.90 3.00 6 -10 0 21.10 3.30 6 -10 0 30.90 3.60 -6 10 0 23.80 3.80 5 -10 0 11.80 2.50 -5 10 0 18.10 3.50 4 -10 0 198.68 9.10 -4 10 0 200.78 9.90 3 -10 0 3.40 1.80 -3 10 0 1.20 1.70 2 -10 0 109.59 6.20 -2 10 0 101.59 6.70 1 -10 0 341.97 13.10 -1 10 0 319.97 13.70 0 -10 0 -1.40 1.30 0 10 0 0.10 1.50 -1 -10 0 23.60 3.40 1 10 0 19.40 3.40 -2 -10 0 1.00 1.50 2 10 0 0.40 1.70 -3 -10 0 2.00 1.60 3 10 0 -1.50 1.50 -4 -10 0 151.58 7.70 4 10 0 141.39 8.30 -5 -10 0 4.30 2.10 -5 -10 0 1.70 2.30 5 10 0 2.10 1.80 -6 -10 0 167.48 9.80 -6 -10 0 179.08 8.90 6 10 0 173.08 9.70 -7 -10 0 3.10 2.60 -7 -10 0 3.90 2.30 7 10 0 7.80 3.00 -8 -10 0 63.89 6.80 8 10 0 54.89 6.30 -9 -10 0 22.90 4.80 9 10 0 22.40 4.60 -10 -10 0 4.40 3.60 10 10 0 3.70 2.90 -11 -10 0 0.10 3.30 11 10 0 6.40 3.60 12 -11 0 2.10 3.40 -12 11 0 6.80 3.60 11 -11 0 1.90 3.00 -11 11 0 3.20 2.80 10 -11 0 1.80 2.70 -10 11 0 3.10 2.80 9 -11 0 -3.00 2.10 -9 11 0 0.90 2.30 8 -11 0 17.70 3.30 -8 11 0 27.20 4.70 7 -11 0 -0.80 1.60 -7 11 0 3.10 2.30 6 -11 0 1.20 1.60 -6 11 0 0.40 2.00 5 -11 0 6.70 2.30 -5 11 0 8.60 2.60 4 -11 0 9.70 2.50 -4 11 0 12.00 3.10 3 -11 0 2.10 1.60 -3 11 0 0.60 1.80 2 -11 0 10.40 2.60 -2 11 0 11.80 3.00 1 -11 0 0.30 1.60 -1 11 0 -1.40 1.60 0 -11 0 -0.50 1.60 0 11 0 0.40 1.60 -1 -11 0 7.90 2.40 1 11 0 6.00 2.50 -2 -11 0 -1.00 1.80 2 11 0 1.80 2.10 -3 -11 0 -0.70 1.70 3 11 0 -0.70 1.70 -4 -11 0 1.90 2.00 4 11 0 2.30 2.20 -5 -11 0 2.60 2.00 5 11 0 3.40 2.70 -6 -11 0 -0.50 2.00 6 11 0 2.40 2.30 -7 -11 0 23.40 4.00 -7 -11 0 23.50 4.60 7 11 0 28.90 4.80 -8 -11 0 2.20 3.00 8 11 0 0.80 2.40 -9 -11 0 4.80 3.80 9 11 0 8.80 3.70 -10 -11 0 2.90 3.60 10 11 0 -1.10 2.50 -11 12 0 5.90 3.40 -10 12 0 3.50 3.10 -9 12 0 3.30 2.90 8 -12 0 1.30 1.80 -8 12 0 0.80 2.40 7 -12 0 39.20 4.70 -7 12 0 34.50 5.30 6 -12 0 16.70 3.20 -6 12 0 14.70 3.50 5 -12 0 32.50 4.30 -5 12 0 35.20 5.10 4 -12 0 2.40 1.80 -4 12 0 1.80 2.30 3 -12 0 151.68 8.30 -3 12 0 142.09 8.70 2 -12 0 93.39 6.40 -2 12 0 94.69 7.10 1 -12 0 164.48 8.60 -1 12 0 144.89 9.00 0 -12 0 9.60 2.80 0 12 0 14.60 3.50 -1 -12 0 23.00 3.80 1 12 0 15.10 3.50 -2 -12 0 87.09 6.60 2 12 0 104.39 7.50 -3 -12 0 99.19 6.80 3 12 0 84.39 7.00 -4 -12 0 42.30 5.00 4 12 0 30.80 4.90 -5 -12 0 44.70 5.40 5 12 0 47.40 6.30 -6 -12 0 64.59 6.30 6 12 0 42.80 5.80 -7 -12 0 4.60 2.90 7 12 0 4.80 2.80 -8 -12 0 9.80 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6.50 3.20 8 10 -3 8.40 3.00 -8 -10 3 7.90 3.30 7 10 -3 10.00 2.90 -7 -10 3 12.80 2.80 -7 -10 3 13.00 3.60 6 10 -3 2.80 2.00 -6 -10 3 1.90 2.50 -6 -10 3 0.60 1.70 5 10 -3 18.40 3.70 -5 -10 3 15.10 2.80 -5 -10 3 12.60 3.20 4 10 -3 0.10 1.60 -4 -10 3 2.80 1.90 3 10 -3 0.70 1.50 -3 -10 3 1.20 1.60 2 10 -3 1.20 1.60 -2 -10 3 1.50 1.60 1 10 -3 -0.20 1.40 -1 -10 3 0.60 1.40 0 10 -3 0.10 1.50 0 -10 3 0.40 1.40 -1 10 -3 2.40 1.80 1 -10 3 0.80 1.40 -2 10 -3 3.20 2.10 2 -10 3 0.50 1.40 -3 10 -3 26.70 3.90 3 -10 3 31.90 4.00 -4 10 -3 5.40 2.20 4 -10 3 4.40 1.90 -5 10 -3 11.30 2.80 5 -10 3 13.10 2.50 -6 10 -3 8.80 2.80 6 -10 3 10.20 2.40 6 -10 3 0.20 1.50 -7 10 -3 12.10 3.00 7 -10 3 18.00 3.10 7 -10 3 15.90 2.90 -8 10 -3 37.40 5.10 8 -10 3 35.40 4.50 8 -10 3 29.80 3.90 -9 10 -3 -1.90 1.80 9 -10 3 1.30 2.20 -10 10 -3 46.80 6.10 10 -10 3 56.39 6.10 -11 10 -3 14.60 3.80 11 -10 3 25.20 4.80 -12 10 -3 4.20 3.30 12 -10 3 2.50 3.20 12 9 -3 0.50 2.50 -12 -9 3 0.70 3.20 11 9 -3 62.09 7.50 -11 -9 3 49.30 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1.80 6 -11 4 1.60 1.80 -7 11 -4 35.50 4.70 7 -11 4 35.70 4.40 -8 11 -4 2.30 2.30 8 -11 4 2.30 1.80 -9 11 -4 111.39 8.10 -10 11 -4 0.00 2.50 10 -11 4 0.30 3.00 -11 11 -4 29.60 5.20 11 -11 4 33.70 5.50 11 10 -4 20.30 4.70 -11 -10 4 13.60 4.40 10 10 -4 40.60 6.10 9 10 -4 29.60 5.20 -9 -10 4 26.70 5.10 8 10 -4 6.30 2.80 -8 -10 4 3.30 2.70 7 10 -4 98.49 7.30 -7 -10 4 112.59 6.40 -7 -10 4 107.29 7.80 6 10 -4 5.70 2.30 -6 -10 4 4.50 2.10 -6 -10 4 -1.00 2.30 5 10 -4 102.59 7.00 -5 -10 4 99.89 6.90 -5 -10 4 101.49 6.10 4 10 -4 21.40 3.50 -4 -10 4 25.00 3.50 3 10 -4 32.50 4.50 -3 -10 4 35.90 4.00 2 10 -4 28.40 3.90 -2 -10 4 30.00 3.90 1 10 -4 73.29 5.50 -1 -10 4 75.59 5.20 0 10 -4 30.30 3.90 0 -10 4 35.90 4.00 -1 10 -4 35.80 4.20 1 -10 4 31.90 3.80 -2 10 -4 48.30 5.00 2 -10 4 43.00 4.50 -3 10 -4 178.98 8.90 3 -10 4 152.08 8.10 -4 10 -4 111.09 6.90 4 -10 4 105.69 6.40 -5 10 -4 67.49 6.40 5 -10 4 51.29 5.00 -6 10 -4 10.70 2.80 6 -10 4 13.80 2.90 -7 10 -4 -0.60 1.80 7 -10 4 0.80 1.60 7 -10 4 1.80 2.00 -8 10 -4 133.49 8.30 8 -10 4 131.69 7.40 8 -10 4 126.19 7.70 -9 10 -4 0.00 2.30 9 -10 4 -1.80 1.90 -10 10 -4 44.40 6.00 10 -10 4 47.60 5.80 -11 10 -4 18.60 4.20 11 -10 4 21.90 4.40 -12 10 -4 0.10 2.70 12 -10 4 -0.60 2.80 12 9 -4 12.20 3.70 -12 -9 4 15.20 4.70 11 9 -4 6.10 3.10 -11 -9 4 3.20 3.40 10 9 -4 44.00 6.00 -10 -9 4 40.50 6.10 9 9 -4 13.10 3.40 -9 -9 4 11.80 3.40 8 9 -4 14.20 3.50 -8 -9 4 18.70 4.20 7 9 -4 12.80 3.00 -7 -9 4 13.00 2.50 -7 -9 4 7.40 2.80 6 9 -4 53.89 5.90 -6 -9 4 65.19 5.60 -6 -9 4 56.39 4.30 5 9 -4 1.10 1.70 -5 -9 4 -0.30 1.20 -5 -9 4 2.80 2.10 4 9 -4 17.70 3.30 -4 -9 4 17.10 2.80 -4 -9 4 11.90 2.80 3 9 -4 2.30 1.80 -3 -9 4 0.30 1.40 2 9 -4 0.50 1.20 -2 -9 4 1.20 1.30 1 9 -4 -1.40 1.10 -1 -9 4 0.60 1.20 0 9 -4 5.20 2.00 0 -9 4 4.70 1.80 -1 9 -4 -1.40 1.10 1 -9 4 -0.10 1.10 -2 9 -4 3.00 1.70 2 -9 4 3.80 1.60 -3 9 -4 2.00 1.50 3 -9 4 3.00 1.50 -4 9 -4 11.80 2.10 -4 9 -4 10.60 2.60 4 -9 4 13.20 2.10 4 -9 4 15.00 2.60 -5 9 -4 -0.20 1.00 -5 9 -4 1.70 1.70 5 -9 4 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4 17.30 2.00 -5 3 -4 51.09 3.50 -5 3 -4 57.19 3.40 -5 3 -4 55.39 3.60 5 -3 4 53.49 3.10 5 -3 4 56.89 3.70 -6 3 -4 32.40 3.20 -6 3 -4 32.10 3.40 -6 3 -4 26.80 3.30 6 -3 4 30.30 2.40 6 -3 4 29.30 3.30 -7 3 -4 260.27 10.60 -7 3 -4 255.87 10.00 -7 3 -4 250.57 10.30 7 -3 4 255.17 9.20 7 -3 4 249.18 10.50 -8 3 -4 9.50 2.10 -8 3 -4 5.30 1.80 -8 3 -4 8.50 2.30 8 -3 4 5.00 2.00 8 -3 4 9.00 1.60 -9 3 -4 210.48 9.20 -9 3 -4 185.68 9.30 -9 3 -4 188.28 9.40 9 -3 4 187.28 9.30 9 -3 4 201.58 9.60 -10 3 -4 14.00 2.90 -10 3 -4 13.40 3.20 10 -3 4 16.50 3.40 10 -3 4 14.30 3.10 -11 3 -4 11.50 3.00 -11 3 -4 9.30 2.70 11 -3 4 9.90 3.00 11 -3 4 11.00 3.00 -12 3 -4 111.19 7.30 -12 3 -4 96.69 7.40 12 -3 4 96.69 7.60 12 -3 4 115.99 8.20 -13 3 -4 1.10 2.30 -13 3 -4 2.60 2.30 13 -3 4 6.00 3.00 13 -3 4 1.50 2.70 -14 3 -4 31.80 5.60 -14 3 -4 29.10 5.10 14 -3 4 26.20 5.20 14 -3 4 19.90 4.60 15 2 -4 3.60 3.00 15 2 -4 2.20 3.00 -15 -2 4 6.90 3.70 14 2 -4 0.10 2.30 14 2 -4 -0.50 2.00 -14 -2 4 -2.10 2.30 13 2 -4 16.50 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3.80 -8 11 -5 30.20 4.70 8 -11 5 35.30 4.60 -9 11 -5 48.90 6.20 -10 11 -5 0.50 2.70 -11 11 -5 -2.30 2.30 11 -11 5 3.10 3.10 11 10 -5 47.50 7.00 -11 -10 5 44.10 6.70 10 10 -5 1.00 2.30 -10 -10 5 1.00 2.90 9 10 -5 25.60 5.00 -9 -10 5 29.90 5.20 8 10 -5 2.10 2.30 -8 -10 5 0.30 2.50 7 10 -5 20.30 3.90 -7 -10 5 21.90 4.30 -7 -10 5 24.70 3.40 6 10 -5 8.00 2.70 -6 -10 5 4.50 2.40 -6 -10 5 3.60 2.00 5 10 -5 -1.60 1.40 -5 -10 5 -1.00 1.50 -5 -10 5 3.00 2.20 4 10 -5 3.50 2.00 -4 -10 5 -2.80 1.30 3 10 -5 -0.30 1.20 -3 -10 5 -0.50 1.40 2 10 -5 0.40 1.50 -2 -10 5 -1.60 1.30 1 10 -5 -0.70 1.40 -1 -10 5 0.90 1.60 0 10 -5 0.80 1.40 0 -10 5 0.80 1.60 -1 10 -5 -1.20 1.10 1 -10 5 -0.40 1.30 -2 10 -5 14.80 3.20 2 -10 5 7.80 2.30 -3 10 -5 0.60 1.70 3 -10 5 -1.00 1.40 -4 10 -5 9.80 2.90 4 -10 5 6.60 2.10 5 -10 5 3.40 1.80 -6 10 -5 22.10 3.80 6 -10 5 26.80 3.70 -7 10 -5 2.50 2.00 7 -10 5 3.80 2.00 -8 10 -5 68.89 6.00 8 -10 5 75.09 5.80 8 -10 5 70.19 5.40 -9 10 -5 21.90 4.20 9 -10 5 17.50 3.70 9 -10 5 13.40 3.40 -10 10 -5 39.50 5.50 -11 10 -5 4.40 3.00 11 -10 5 2.40 2.80 -12 10 -5 7.10 3.50 12 -10 5 11.20 3.90 12 9 -5 3.20 2.70 -12 -9 5 9.60 4.30 11 9 -5 7.00 3.10 -11 -9 5 2.80 3.30 10 9 -5 139.79 9.30 10 9 -5 141.09 8.40 -10 -9 5 139.29 9.60 9 9 -5 4.20 2.30 9 9 -5 3.10 1.90 -9 -9 5 6.50 3.20 8 9 -5 80.89 6.40 8 9 -5 69.19 5.20 -8 -9 5 77.59 6.60 7 9 -5 6.90 2.00 7 9 -5 7.20 2.40 -7 -9 5 2.50 2.10 -7 -9 5 6.70 2.00 6 9 -5 163.68 7.60 6 9 -5 150.78 8.70 -6 -9 5 178.48 7.90 -6 -9 5 155.48 8.90 5 9 -5 17.90 3.40 5 9 -5 17.50 2.60 -5 -9 5 15.60 3.20 4 9 -5 96.79 5.10 4 9 -5 97.69 6.30 -4 -9 5 94.69 5.60 -4 -9 5 102.99 6.60 3 9 -5 3.00 1.70 -3 -9 5 1.60 1.60 2 9 -5 112.19 6.80 2 9 -5 116.69 5.40 -2 -9 5 124.09 6.40 1 9 -5 8.60 1.60 1 9 -5 7.30 2.30 -1 -9 5 6.40 1.90 0 9 -5 167.48 8.10 0 9 -5 148.49 6.30 0 -9 5 161.98 7.80 -1 9 -5 0.70 0.90 -1 9 -5 -0.40 1.10 1 -9 5 -0.90 1.10 -2 9 -5 114.09 5.20 -2 9 -5 119.99 6.60 2 -9 5 102.09 6.10 -3 9 -5 166.58 7.90 -3 9 -5 127.29 6.10 3 -9 5 147.69 7.40 -4 9 -5 13.50 2.10 -4 9 -5 10.30 2.50 4 -9 5 15.10 2.20 4 -9 5 16.80 2.70 -5 9 -5 108.49 6.50 -5 9 -5 96.79 5.40 5 -9 5 105.89 6.10 -6 9 -5 94.59 6.30 -6 9 -5 88.79 5.30 6 -9 5 100.79 5.90 6 -9 5 94.99 5.70 -7 9 -5 71.19 5.70 -7 9 -5 75.29 5.10 7 -9 5 83.79 5.40 7 -9 5 66.99 5.20 -8 9 -5 1.50 1.80 -8 9 -5 -0.50 1.40 8 -9 5 -1.00 1.90 8 -9 5 0.40 1.50 -9 9 -5 105.99 7.30 -9 9 -5 96.59 6.50 9 -9 5 100.69 7.10 9 -9 5 101.59 6.70 -10 9 -5 2.10 2.10 -10 9 -5 4.00 2.50 10 -9 5 -0.20 2.00 10 -9 5 0.40 2.20 -11 9 -5 16.30 3.60 -11 9 -5 24.10 4.70 11 -9 5 10.40 3.50 11 -9 5 14.60 4.00 -12 9 -5 0.90 2.40 -12 9 -5 2.40 2.80 12 -9 5 1.60 2.80 12 -9 5 1.40 3.50 13 8 -5 48.30 6.30 13 8 -5 42.80 6.20 -13 -8 5 64.29 8.00 12 8 -5 6.80 3.30 12 8 -5 4.10 2.60 -12 -8 5 2.90 3.30 11 8 -5 54.19 6.80 11 8 -5 47.90 5.60 -11 -8 5 45.90 6.10 10 8 -5 19.60 4.20 10 8 -5 18.30 3.50 -10 -8 5 20.20 4.40 9 8 -5 -0.80 1.50 9 8 -5 0.90 1.60 -9 -8 5 -0.70 2.20 8 8 -5 2.50 1.50 -8 -8 5 1.90 2.20 7 8 -5 5.00 1.70 7 8 -5 11.80 2.70 -7 -8 5 11.20 2.80 -7 -8 5 0.30 0.70 6 8 -5 6.10 1.80 6 8 -5 6.40 2.30 -6 -8 5 5.30 1.80 -6 -8 5 4.40 2.20 5 8 -5 17.50 2.40 5 8 -5 13.50 2.70 -5 -8 5 14.10 2.40 -5 -8 5 13.50 2.90 4 8 -5 0.40 1.20 4 8 -5 0.30 1.00 -4 -8 5 0.50 1.30 -4 -8 5 0.30 1.10 3 8 -5 11.00 2.50 3 8 -5 14.80 2.10 -3 -8 5 12.50 2.20 -3 -8 5 11.60 2.50 2 8 -5 -0.60 1.00 2 8 -5 0.10 0.80 -2 -8 5 0.60 1.20 1 8 -5 0.10 1.30 1 8 -5 -0.10 0.70 -1 -8 5 0.30 1.10 0 8 -5 0.50 1.00 0 8 -5 -0.60 0.70 0 -8 5 -0.70 0.90 -1 8 -5 10.10 2.30 -1 8 -5 9.20 1.60 1 -8 5 6.10 1.80 -2 8 -5 6.60 1.40 -2 8 -5 5.10 1.60 2 -8 5 4.20 1.60 2 -8 5 2.10 0.90 -3 8 -5 3.70 1.20 -3 8 -5 4.00 1.70 3 -8 5 3.00 1.60 3 -8 5 3.00 1.10 -4 8 -5 0.80 1.30 -4 8 -5 -0.90 0.80 4 -8 5 1.10 1.30 4 -8 5 0.20 1.00 -5 8 -5 -1.20 1.20 -5 8 -5 0.00 1.00 5 -8 5 0.60 1.30 5 -8 5 1.60 1.30 -6 8 -5 15.10 2.50 -6 8 -5 13.90 2.90 6 -8 5 17.70 2.80 6 -8 5 16.10 2.70 -7 8 -5 58.69 4.50 -7 8 -5 66.09 5.10 7 -8 5 62.09 4.60 7 -8 5 67.19 5.10 -8 8 -5 18.10 3.40 -8 8 -5 10.70 2.60 8 -8 5 11.40 2.50 8 -8 5 10.90 3.00 -9 8 -5 131.09 7.60 -9 8 -5 118.89 7.60 9 -8 5 129.89 7.20 9 -8 5 146.09 8.20 -10 8 -5 11.70 2.80 -10 8 -5 11.40 3.30 10 -8 5 11.70 3.20 10 -8 5 6.50 2.90 -11 8 -5 2.30 2.30 -11 8 -5 0.40 2.00 11 -8 5 8.30 3.40 11 -8 5 2.60 2.50 -12 8 -5 40.20 5.60 -12 8 -5 41.80 5.90 12 -8 5 45.20 5.70 12 -8 5 43.00 6.40 -13 8 -5 3.00 2.70 -13 8 -5 4.70 3.20 13 -8 5 6.20 3.60 13 -8 5 7.50 3.90 13 7 -5 20.10 4.50 13 7 -5 21.30 4.30 -13 -7 5 23.10 5.30 12 7 -5 53.69 6.50 12 7 -5 62.19 6.50 -12 -7 5 66.69 7.70 11 7 -5 50.19 6.30 11 7 -5 50.29 5.80 -11 -7 5 46.00 5.90 10 7 -5 48.40 5.10 10 7 -5 34.20 4.70 -10 -7 5 55.89 6.30 9 7 -5 8.70 2.40 9 7 -5 5.60 2.50 -9 -7 5 5.60 2.70 8 7 -5 10.30 2.40 8 7 -5 10.50 2.80 -8 -7 5 7.00 2.40 7 7 -5 90.19 5.30 7 7 -5 78.39 5.70 -7 -7 5 78.49 5.80 -7 -7 5 82.99 4.50 6 7 -5 98.99 5.50 6 7 -5 104.39 6.30 -6 -7 5 100.69 6.20 5 7 -5 15.10 2.80 5 7 -5 14.60 2.30 -5 -7 5 16.50 2.30 -5 -7 5 15.00 2.70 4 7 -5 72.39 4.10 4 7 -5 74.29 4.90 -4 -7 5 76.59 5.00 -4 -7 5 66.79 4.10 3 7 -5 18.40 2.80 3 7 -5 17.90 2.10 -3 -7 5 19.00 2.80 -3 -7 5 14.50 2.20 2 7 -5 308.67 10.80 2 7 -5 318.97 12.00 -2 -7 5 312.47 11.40 -2 -7 5 316.57 12.00 1 7 -5 29.60 3.20 1 7 -5 29.00 2.30 -1 -7 5 32.50 3.20 0 7 -5 350.16 11.70 0 7 -5 364.06 12.80 0 -7 5 352.66 12.50 0 -7 5 324.37 10.40 -1 7 -5 -0.40 1.00 -1 7 -5 0.70 0.70 1 -7 5 1.00 1.10 1 -7 5 0.50 0.60 -2 7 -5 367.96 13.50 -2 7 -5 380.76 12.70 2 -7 5 365.66 12.20 2 -7 5 389.16 13.60 -3 7 -5 259.67 9.80 -3 7 -5 271.67 10.50 3 -7 5 265.67 10.40 3 -7 5 264.77 9.60 -4 7 -5 341.17 12.50 -4 7 -5 352.96 12.00 4 -7 5 341.67 12.40 4 -7 5 285.27 11.50 -5 7 -5 1.00 1.10 -5 7 -5 0.50 1.40 5 -7 5 1.80 1.30 5 -7 5 2.20 1.40 -6 7 -5 8.50 2.00 -6 7 -5 6.10 1.90 6 -7 5 10.30 2.20 6 -7 5 7.00 1.90 -7 7 -5 68.59 4.80 -7 7 -5 78.39 5.20 7 -7 5 75.29 5.20 7 -7 5 61.89 4.50 -8 7 -5 65.39 5.00 -8 7 -5 83.59 5.60 8 -7 5 67.59 4.80 8 -7 5 76.19 5.60 -9 7 -5 -0.90 1.60 -9 7 -5 2.00 1.70 9 -7 5 3.10 1.70 9 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5.80 2.40 -6 11 -8 29.30 4.60 6 -11 8 41.80 5.10 -7 11 -8 1.30 2.40 7 -11 8 2.60 2.20 -8 11 -8 37.30 5.30 8 -11 8 20.60 3.70 -9 11 -8 25.10 4.60 9 -11 8 21.30 4.00 -10 11 -8 25.40 5.00 11 10 -8 2.50 2.50 -11 -10 8 0.80 3.00 10 10 -8 14.50 3.90 -10 -10 8 26.50 5.10 9 10 -8 3.50 2.70 -9 -10 8 4.40 3.10 8 10 -8 52.69 6.20 8 10 -8 37.20 5.20 -8 -10 8 48.80 6.00 7 10 -8 4.80 2.60 7 10 -8 9.10 2.60 -7 -10 8 3.00 2.80 6 10 -8 26.60 3.50 6 10 -8 28.40 4.60 -6 -10 8 24.10 4.20 -6 -10 8 29.60 3.90 5 10 -8 1.20 1.40 5 10 -8 -0.10 1.80 -5 -10 8 1.10 1.80 -5 -10 8 3.80 2.40 4 10 -8 243.28 10.20 4 10 -8 234.98 11.40 -4 -10 8 258.87 10.80 3 10 -8 4.50 1.70 3 10 -8 5.70 2.30 -3 -10 8 3.90 2.00 2 10 -8 444.26 17.60 2 10 -8 474.25 16.30 -2 -10 8 466.45 17.10 1 10 -8 0.70 1.70 1 10 -8 2.30 1.50 -1 -10 8 -0.50 1.60 0 10 -8 17.30 2.60 0 10 -8 14.50 3.00 0 -10 8 15.20 3.00 -1 10 -8 135.49 7.60 -1 10 -8 133.09 6.60 1 -10 8 135.59 7.50 -2 10 -8 38.80 3.80 -2 10 -8 48.30 5.10 2 -10 8 48.40 5.10 -3 10 -8 77.09 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4 -13 9 35.20 5.20 -5 13 -9 41.70 5.70 5 -13 9 52.29 6.00 -6 13 -9 2.80 2.70 6 -13 9 -0.50 1.90 -7 13 -9 25.20 4.80 7 -13 9 28.50 4.80 -8 13 -9 2.50 2.80 8 -13 9 4.40 2.70 9 12 -9 0.60 2.50 -9 -12 9 1.50 3.30 8 12 -9 13.30 4.00 -8 -12 9 9.80 3.70 7 12 -9 18.20 4.20 -7 -12 9 11.20 3.80 6 12 -9 16.10 4.10 -6 -12 9 13.70 3.40 5 12 -9 2.20 2.40 -5 -12 9 5.10 2.60 4 12 -9 5.40 2.70 -4 -12 9 2.50 2.40 3 12 -9 16.80 3.80 -3 -12 9 19.10 3.70 2 12 -9 0.60 2.20 -2 -12 9 5.40 2.60 1 12 -9 -1.20 1.80 -1 -12 9 -0.20 2.10 0 12 -9 -1.50 1.60 0 -12 9 1.70 2.30 -1 12 -9 2.60 2.40 1 -12 9 4.40 2.50 -2 12 -9 0.90 1.90 2 -12 9 1.80 2.20 -3 12 -9 -3.00 1.70 3 -12 9 2.70 2.20 -4 12 -9 3.40 2.40 4 -12 9 -0.60 1.80 -5 12 -9 8.40 3.00 5 -12 9 7.70 2.80 -6 12 -9 7.30 3.00 6 -12 9 6.40 2.70 -7 12 -9 4.30 2.80 7 -12 9 8.20 2.90 -8 12 -9 14.30 3.90 8 -12 9 7.30 2.80 -9 12 -9 17.00 4.30 9 -12 9 11.10 3.60 10 11 -9 13.20 3.70 -10 -11 9 7.40 3.70 9 11 -9 12.00 3.70 -9 -11 9 15.90 4.20 8 11 -9 44.60 5.90 -8 -11 9 44.00 6.10 7 11 -9 6.30 3.00 -7 -11 9 6.90 3.20 6 11 -9 32.50 5.00 -6 -11 9 34.10 5.00 -6 -11 9 43.40 4.90 5 11 -9 2.30 2.20 -5 -11 9 -0.10 1.90 4 11 -9 78.59 6.30 -4 -11 9 73.79 5.70 3 11 -9 34.90 4.80 -3 -11 9 39.10 4.70 2 11 -9 51.49 5.80 -2 -11 9 49.80 5.30 1 11 -9 -0.50 1.60 -1 -11 9 -0.80 1.80 0 11 -9 7.20 2.50 0 -11 9 6.50 2.50 -1 11 -9 1.70 2.00 1 -11 9 0.60 1.90 -2 11 -9 76.49 5.90 2 -11 9 87.49 6.20 -3 11 -9 4.30 2.30 3 -11 9 7.30 2.50 -4 11 -9 69.89 5.80 4 -11 9 78.79 6.00 -5 11 -9 0.50 2.10 5 -11 9 2.40 2.20 -6 11 -9 81.49 6.40 6 -11 9 70.49 6.90 -7 11 -9 36.10 5.10 7 -11 9 30.70 4.70 -8 11 -9 4.20 2.60 8 -11 9 8.40 3.00 -9 11 -9 20.60 4.20 9 -11 9 11.40 3.30 -10 11 -9 28.80 5.10 11 10 -9 1.30 2.60 -11 -10 9 3.80 3.20 10 10 -9 -2.40 1.90 10 10 -9 -0.80 1.90 -10 -10 9 1.30 2.90 9 10 -9 0.70 2.30 9 10 -9 -0.80 1.60 -9 -10 9 -1.80 2.30 8 10 -9 0.30 1.80 8 10 -9 2.40 2.40 -8 -10 9 2.00 2.70 7 10 -9 10.90 3.20 7 10 -9 11.00 2.80 -7 -10 9 12.10 3.70 6 10 -9 -0.70 1.40 6 10 -9 0.90 1.90 -6 -10 9 -2.00 1.40 -6 -10 9 2.30 2.50 5 10 -9 6.30 2.00 5 10 -9 4.90 2.50 -5 -10 9 8.10 2.40 -5 -10 9 5.60 2.50 4 10 -9 30.80 4.30 4 10 -9 32.80 3.80 -4 -10 9 27.10 3.80 3 10 -9 0.80 1.50 3 10 -9 -0.80 1.50 -3 -10 9 0.00 1.70 2 10 -9 -0.20 1.40 2 10 -9 2.90 2.00 -2 -10 9 2.50 2.00 1 10 -9 9.10 2.10 1 10 -9 4.20 2.10 -1 -10 9 5.20 2.20 0 10 -9 1.10 1.40 0 10 -9 -0.50 1.50 0 -10 9 2.90 1.90 -1 10 -9 3.90 2.00 -1 10 -9 2.50 1.40 1 -10 9 1.10 1.90 -2 10 -9 6.70 1.90 -2 10 -9 4.30 2.00 2 -10 9 10.30 2.50 -3 10 -9 1.20 1.30 -3 10 -9 1.10 1.70 3 -10 9 0.10 1.40 -4 10 -9 13.70 3.00 -4 10 -9 9.80 2.40 4 -10 9 10.60 2.90 -5 10 -9 12.20 2.90 -5 10 -9 9.70 2.50 5 -10 9 17.40 3.30 -6 10 -9 12.50 2.80 -6 10 -9 12.40 3.00 6 -10 9 10.30 2.90 -7 10 -9 78.89 6.10 -7 10 -9 77.49 5.80 -8 10 -9 -0.20 1.70 -8 10 -9 0.50 2.20 8 -10 9 0.50 2.20 8 -10 9 -0.50 1.80 -9 10 -9 31.70 4.80 -9 10 -9 31.50 4.70 9 -10 9 25.20 4.60 9 -10 9 19.20 3.90 -10 10 -9 23.60 4.40 -10 10 -9 15.10 3.60 10 -10 9 27.60 4.80 -11 10 -9 5.80 2.90 11 -10 9 9.30 3.80 12 9 -9 16.20 4.00 12 9 -9 9.60 3.60 -12 -9 9 0.90 3.20 11 9 -9 19.10 3.90 11 9 -9 17.20 4.30 -11 -9 9 18.30 4.40 10 9 -9 2.10 2.10 10 9 -9 3.00 2.40 -10 -9 9 0.30 2.40 9 9 -9 137.59 8.70 9 9 -9 137.09 8.00 -9 -9 9 119.19 8.50 8 9 -9 17.60 3.30 8 9 -9 19.10 3.80 -8 -9 9 18.10 4.10 7 9 -9 18.20 3.10 7 9 -9 27.40 4.40 -7 -9 9 18.60 3.90 6 9 -9 81.49 6.20 6 9 -9 82.79 5.50 -6 -9 9 75.09 6.10 -6 -9 9 90.59 5.40 5 9 -9 32.80 3.80 5 9 -9 45.30 5.00 -5 -9 9 36.10 4.00 -5 -9 9 40.20 4.90 4 9 -9 1.60 1.70 4 9 -9 3.10 1.50 -4 -9 9 2.20 1.60 -4 -9 9 0.80 1.80 3 9 -9 185.28 8.50 3 9 -9 195.68 9.30 -3 -9 9 199.98 9.00 2 9 -9 23.80 3.50 2 9 -9 27.00 3.20 -2 -9 9 28.40 3.60 1 9 -9 534.25 18.50 1 9 -9 555.04 19.40 -1 -9 9 535.95 19.10 0 9 -9 64.19 4.90 0 9 -9 67.49 4.50 0 -9 9 57.09 4.70 -1 9 -9 179.18 8.00 -1 9 -9 180.08 8.70 1 -9 9 181.98 8.80 -2 9 -9 364.46 13.90 -2 9 -9 363.76 13.40 2 -9 9 339.67 13.90 -3 9 -9 -1.30 1.00 -3 9 -9 1.20 1.60 3 -9 9 -1.40 1.30 -4 9 -9 53.49 4.50 -4 9 -9 53.59 4.30 4 -9 9 53.39 5.30 -5 9 -9 8.40 2.40 -5 9 -9 7.50 2.20 -5 9 -9 4.20 1.80 5 -9 9 4.30 1.90 5 -9 9 1.40 1.90 -6 9 -9 82.79 5.90 -6 9 -9 85.69 5.80 -6 9 -9 85.29 5.90 6 -9 9 94.09 6.00 6 -9 9 83.49 6.00 -7 9 -9 10.20 2.80 -7 9 -9 12.70 3.00 -7 9 -9 10.20 2.70 7 -9 9 7.70 2.80 7 -9 9 11.10 2.80 -8 9 -9 107.09 7.20 -8 9 -9 111.29 7.20 8 -9 9 112.29 7.50 8 -9 9 116.79 7.30 -9 9 -9 0.50 1.70 -9 9 -9 2.00 2.20 9 -9 9 0.20 2.60 9 -9 9 2.90 2.20 -10 9 -9 37.90 5.30 -10 9 -9 32.40 4.80 10 -9 9 40.20 5.60 -11 9 -9 1.80 2.40 11 -9 9 10.60 3.80 13 8 -9 3.50 2.90 13 8 -9 6.70 3.60 -13 -8 9 1.80 3.30 12 8 -9 9.70 3.40 12 8 -9 17.10 4.00 -12 -8 9 11.90 4.20 11 8 -9 1.80 2.40 11 8 -9 -1.30 1.90 -11 -8 9 2.50 2.70 10 8 -9 0.60 1.90 10 8 -9 -0.60 2.10 -10 -8 9 0.60 2.40 9 8 -9 -0.60 1.70 9 8 -9 -0.60 1.60 -9 -8 9 2.60 2.50 8 8 -9 76.29 5.60 8 8 -9 75.19 6.10 -8 -8 9 76.29 6.20 7 8 -9 0.00 1.70 7 8 -9 -1.30 1.30 -7 -8 9 2.70 2.00 6 8 -9 4.60 2.20 6 8 -9 3.70 1.70 -6 -8 9 6.00 2.40 -6 -8 9 2.80 1.60 5 8 -9 16.00 3.00 5 8 -9 13.90 2.50 -5 -8 9 15.70 2.90 -5 -8 9 14.90 2.50 4 8 -9 23.20 3.10 4 8 -9 26.60 3.60 -4 -8 9 22.50 3.50 -4 -8 9 21.70 3.00 3 8 -9 5.30 1.70 3 8 -9 5.10 1.90 -3 -8 9 7.10 2.20 -3 -8 9 5.70 2.00 2 8 -9 9.10 2.10 2 8 -9 10.20 2.10 -2 -8 9 9.10 2.20 1 8 -9 8.50 2.10 1 8 -9 12.80 2.30 -1 -8 9 9.50 2.30 0 8 -9 13.80 2.40 0 8 -9 14.50 2.50 0 -8 9 17.20 2.90 -1 8 -9 1.00 1.10 -1 8 -9 1.80 1.40 1 -8 9 1.80 1.50 -2 8 -9 7.40 2.00 -2 8 -9 6.20 1.80 2 -8 9 6.90 2.10 -3 8 -9 0.10 1.30 -3 8 -9 0.90 1.30 -3 8 -9 3.50 1.50 3 -8 9 1.30 1.40 3 -8 9 2.70 1.60 -4 8 -9 5.40 1.90 -4 8 -9 8.50 2.00 -4 8 -9 8.00 2.10 4 -8 9 5.60 2.20 4 -8 9 5.20 1.60 -5 8 -9 28.50 3.70 -5 8 -9 19.30 3.10 -5 8 -9 23.80 3.40 5 -8 9 26.80 3.50 5 -8 9 20.40 3.20 -6 8 -9 0.50 1.60 -6 8 -9 -0.80 1.20 -6 8 -9 0.70 1.80 6 -8 9 1.90 1.70 6 -8 9 1.00 1.80 -7 8 -9 10.10 2.70 -7 8 -9 15.20 2.90 -7 8 -9 14.00 2.90 7 -8 9 12.00 2.70 7 -8 9 10.30 3.00 -8 8 -9 3.50 2.10 -8 8 -9 5.70 2.70 -8 8 -9 1.10 1.60 8 -8 9 0.20 2.20 8 -8 9 1.10 1.80 -9 8 -9 31.40 4.50 -9 8 -9 36.60 4.70 -9 8 -9 30.70 4.80 9 -8 9 29.60 4.70 9 -8 9 32.20 4.30 -10 8 -9 4.60 2.50 -10 8 -9 8.70 3.00 10 -8 9 5.60 3.30 -11 8 -9 34.10 5.30 11 -8 9 32.50 5.50 -12 8 -9 5.80 3.10 12 -8 9 3.70 3.30 12 -8 9 2.00 3.30 13 7 -9 31.50 5.10 13 7 -9 36.90 5.60 -13 -7 9 24.20 5.10 12 7 -9 12.40 3.80 12 7 -9 16.20 3.90 -12 -7 9 13.30 3.50 11 7 -9 134.09 8.70 11 7 -9 119.39 8.10 -11 -7 9 117.59 8.40 10 7 -9 11.60 3.10 10 7 -9 18.00 3.60 -10 -7 9 26.40 4.50 9 7 -9 2.50 1.80 9 7 -9 6.10 2.60 -9 -7 9 3.40 2.30 8 7 -9 56.79 4.70 8 7 -9 52.39 5.40 -8 -7 9 51.19 5.50 7 7 -9 46.10 4.70 7 7 -9 59.29 5.60 -7 -7 9 55.89 5.40 6 7 -9 0.80 1.50 6 7 -9 0.50 1.30 -6 -7 9 0.00 0.80 -6 -7 9 -0.20 1.30 5 7 -9 220.18 9.70 5 7 -9 219.68 9.40 -5 -7 9 199.38 9.50 -5 -7 9 221.98 8.80 4 7 -9 78.49 5.00 4 7 -9 73.79 4.80 -4 -7 9 74.19 4.50 -4 -7 9 72.09 4.90 3 7 -9 345.87 13.20 3 7 -9 352.76 13.00 -3 -7 9 344.87 12.80 -3 -7 9 353.86 13.30 2 7 -9 94.29 5.30 2 7 -9 94.99 5.30 -2 -7 9 93.79 5.40 1 7 -9 -0.50 1.00 1 7 -9 1.20 0.80 1 7 -9 -1.20 0.80 -1 -7 9 1.70 1.30 0 7 -9 75.59 3.60 0 7 -9 66.79 4.30 0 7 -9 67.99 4.40 0 -7 9 75.69 4.70 -1 7 -9 93.29 5.20 -1 7 -9 91.09 5.10 -1 7 -9 95.19 4.40 1 -7 9 87.59 4.40 1 -7 9 93.99 5.50 -2 7 -9 59.89 4.00 -2 7 -9 58.09 3.60 -2 7 -9 58.39 4.10 2 -7 9 60.09 4.30 2 -7 9 55.09 3.50 -3 7 -9 49.00 3.50 -3 7 -9 51.99 3.90 -3 7 -9 50.99 3.80 3 -7 9 45.90 4.30 -4 7 -9 1.70 1.40 -4 7 -9 2.00 1.30 -4 7 -9 2.70 1.40 4 -7 9 3.90 1.80 4 -7 9 5.70 1.80 -5 7 -9 103.59 5.80 -5 7 -9 106.99 6.20 -5 7 -9 95.49 5.70 5 -7 9 105.39 6.00 5 -7 9 106.39 6.10 -6 7 -9 5.10 1.80 -6 7 -9 7.10 2.10 -6 7 -9 5.50 2.10 6 -7 9 6.10 1.90 6 -7 9 10.90 2.60 -7 7 -9 45.20 5.00 -7 7 -9 49.80 4.20 -7 7 -9 42.50 4.90 7 -7 9 52.09 5.40 7 -7 9 42.60 4.60 -8 7 -9 9.40 2.80 -8 7 -9 6.20 2.30 -8 7 -9 12.30 2.90 8 -7 9 15.80 3.50 8 -7 9 17.00 3.20 -9 7 -9 48.70 5.70 -9 7 -9 58.99 5.80 -9 7 -9 42.40 5.30 9 -7 9 50.99 5.40 9 -7 9 40.20 5.30 -10 7 -9 10.30 2.90 -10 7 -9 6.50 3.30 -10 7 -9 6.50 2.70 10 -7 9 4.00 2.90 -11 7 -9 1.50 2.20 11 -7 9 3.00 3.20 -12 7 -9 29.90 5.20 12 -7 9 28.30 5.10 12 -7 9 28.60 5.10 14 6 -9 4.30 3.20 14 6 -9 1.00 2.60 -14 -6 9 -1.10 2.90 13 6 -9 64.89 7.20 -13 -6 9 61.79 7.50 12 6 -9 19.90 4.10 -12 -6 9 22.00 4.60 11 6 -9 8.00 2.80 11 6 -9 5.80 2.70 -11 -6 9 2.60 2.40 10 6 -9 10.40 3.00 10 6 -9 11.30 3.20 -10 -6 9 3.90 2.30 9 6 -9 2.50 1.80 9 6 -9 6.70 2.70 -9 -6 9 7.30 2.70 8 6 -9 84.29 5.80 8 6 -9 98.29 6.20 -8 -6 9 77.29 5.80 7 6 -9 0.90 1.50 7 6 -9 5.80 1.90 -7 -6 9 6.30 2.20 6 6 -9 4.80 1.80 6 6 -9 7.80 2.10 -6 -6 9 9.30 2.30 -6 -6 9 8.00 1.60 5 6 -9 21.20 2.20 5 6 -9 17.60 2.70 5 6 -9 14.10 2.40 -5 -6 9 20.10 2.90 4 6 -9 17.00 2.60 4 6 -9 12.10 1.50 4 6 -9 12.10 2.20 -4 -6 9 10.10 1.90 -4 -6 9 7.80 2.00 3 6 -9 34.50 3.40 3 6 -9 30.30 2.10 3 6 -9 34.00 3.40 -3 -6 9 36.70 3.40 -3 -6 9 38.30 3.20 2 6 -9 24.30 1.80 2 6 -9 27.00 3.00 2 6 -9 20.00 2.60 -2 -6 9 21.50 2.60 -2 -6 9 21.50 2.80 1 6 -9 19.70 1.90 1 6 -9 19.50 2.60 1 6 -9 25.30 2.80 -1 -6 9 23.60 2.80 0 6 -9 6.90 1.60 0 6 -9 7.00 1.30 0 6 -9 8.60 1.90 0 -6 9 8.30 1.80 -1 6 -9 -0.10 0.80 -1 6 -9 -0.80 0.50 -1 6 -9 -0.30 0.90 1 -6 9 1.90 1.20 -2 6 -9 1.60 1.20 -2 6 -9 1.80 1.10 -2 6 -9 0.00 0.50 2 -6 9 0.40 0.70 2 -6 9 2.30 1.40 -3 6 -9 2.00 1.40 -3 6 -9 1.50 1.30 -3 6 -9 -0.20 0.50 3 -6 9 3.20 1.40 3 -6 9 0.70 1.10 -4 6 -9 -0.10 0.50 -4 6 -9 2.10 1.30 -4 6 -9 1.70 1.40 4 -6 9 0.90 1.30 4 -6 9 2.70 1.50 -5 6 -9 5.90 1.60 -5 6 -9 2.50 1.50 -5 6 -9 2.90 1.70 5 -6 9 6.30 2.00 5 -6 9 4.90 1.90 -6 6 -9 25.00 3.10 -6 6 -9 26.10 3.60 -6 6 -9 26.40 3.70 6 -6 9 24.70 3.30 6 -6 9 28.50 3.70 -7 6 -9 1.00 1.60 -7 6 -9 4.20 1.90 -7 6 -9 3.70 1.70 7 -6 9 1.40 1.70 7 -6 9 3.70 2.20 -8 6 -9 51.99 5.60 -8 6 -9 49.50 4.30 -8 6 -9 42.20 5.00 8 -6 9 55.29 5.60 8 -6 9 50.39 4.90 -9 6 -9 1.60 1.90 -9 6 -9 2.20 2.00 -9 6 -9 1.70 2.40 9 -6 9 0.90 2.40 9 -6 9 0.60 1.70 -10 6 -9 45.50 5.40 -10 6 -9 48.60 5.80 10 -6 9 49.99 5.90 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2.40 -1 -5 9 11.00 1.90 0 5 -9 32.70 2.30 0 5 -9 34.30 3.40 0 5 -9 30.50 2.40 0 -5 9 26.60 2.90 -1 5 -9 156.38 6.20 -1 5 -9 148.19 6.00 -1 5 -9 146.39 6.80 1 -5 9 138.89 6.60 -2 5 -9 92.19 5.20 -2 5 -9 90.69 4.70 -2 5 -9 90.99 4.40 2 -5 9 103.29 5.30 -3 5 -9 187.38 7.60 -3 5 -9 173.28 7.80 -3 5 -9 168.38 6.90 3 -5 9 171.88 7.60 3 -5 9 167.68 7.40 -4 5 -9 23.20 2.90 -4 5 -9 32.50 3.60 -4 5 -9 25.40 2.60 4 -5 9 23.80 3.00 4 -5 9 22.20 2.80 -5 5 -9 100.79 5.10 -5 5 -9 111.19 6.00 -5 5 -9 99.69 5.90 5 -5 9 109.99 5.80 5 -5 9 101.99 5.80 -6 5 -9 16.40 2.90 -6 5 -9 18.50 3.20 6 -5 9 20.70 3.10 6 -5 9 17.80 2.70 -7 5 -9 159.28 7.50 -7 5 -9 168.18 8.50 -7 5 -9 174.18 8.70 7 -5 9 167.28 8.70 7 -5 9 168.08 8.00 -8 5 -9 5.10 2.40 -8 5 -9 8.80 2.20 -8 5 -9 6.10 2.20 8 -5 9 5.70 1.90 8 -5 9 2.00 2.20 -9 5 -9 132.49 8.10 -9 5 -9 128.09 7.20 -9 5 -9 132.79 8.10 9 -5 9 132.29 7.20 9 -5 9 122.69 7.90 -10 5 -9 5.30 2.90 -10 5 -9 7.20 2.80 10 -5 9 8.80 3.00 -11 5 -9 48.40 5.90 -11 5 -9 41.60 6.00 11 -5 9 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37.40 4.30 4 10 -10 116.19 7.30 4 10 -10 98.89 6.20 -4 -10 10 106.69 6.60 3 10 -10 191.48 9.20 3 10 -10 209.88 10.30 -3 -10 10 211.68 9.80 2 10 -10 14.80 3.20 2 10 -10 12.00 2.40 -2 -10 10 11.40 2.80 1 10 -10 0.80 1.70 1 10 -10 3.60 1.70 -1 -10 10 3.60 2.00 0 10 -10 7.20 2.10 0 10 -10 12.70 2.90 0 -10 10 16.10 3.30 -1 10 -10 49.00 4.10 -1 10 -10 55.59 5.50 1 -10 10 63.49 6.10 -2 10 -10 41.60 4.30 -2 10 -10 32.20 4.10 2 -10 10 32.30 4.50 -3 10 -10 3.60 1.70 -3 10 -10 7.40 2.40 3 -10 10 8.30 2.60 -4 10 -10 17.10 3.00 -4 10 -10 21.10 3.50 4 -10 10 13.70 3.10 -5 10 -10 184.68 9.60 -5 10 -10 184.98 9.30 5 -10 10 214.38 10.20 -6 10 -10 10.20 3.00 -6 10 -10 16.10 3.10 6 -10 10 12.20 3.20 -7 10 -10 55.19 5.70 -7 10 -10 53.69 5.80 7 -10 10 58.09 6.10 -8 10 -10 27.90 4.40 -8 10 -10 38.40 5.10 8 -10 10 32.90 5.30 8 -10 10 35.70 4.90 -9 10 -10 13.00 3.20 9 -10 10 13.00 3.50 9 -10 10 18.60 4.40 -10 10 -10 16.00 3.80 10 -10 10 12.10 3.90 -11 10 -10 -1.20 2.40 11 -10 10 3.40 3.40 12 9 -10 1.80 2.70 12 9 -10 0.00 2.50 -12 -9 10 -1.90 3.00 11 9 -10 18.30 3.90 11 9 -10 12.20 3.90 -11 -9 10 12.60 3.70 10 9 -10 25.50 4.40 10 9 -10 30.10 4.60 -10 -9 10 35.30 5.60 9 9 -10 7.40 2.60 9 9 -10 7.30 2.90 -9 -9 10 5.50 3.00 8 9 -10 230.38 10.90 8 9 -10 230.58 11.50 -8 -9 10 209.98 11.40 7 9 -10 65.49 6.40 7 9 -10 72.79 5.50 -7 -9 10 55.19 6.00 6 9 -10 15.60 3.30 6 9 -10 12.80 2.80 -6 -9 10 7.90 2.70 -6 -9 10 12.40 2.60 5 9 -10 2.30 2.00 5 9 -10 6.00 2.10 -5 -9 10 7.10 2.50 -5 -9 10 4.00 2.00 4 9 -10 9.30 2.30 4 9 -10 -0.40 1.70 -4 -9 10 2.60 2.20 -4 -9 10 7.50 2.30 3 9 -10 2.90 1.60 3 9 -10 2.40 1.70 -3 -9 10 0.60 1.70 2 9 -10 -1.60 1.30 2 9 -10 1.40 1.40 -2 -9 10 -1.80 1.30 1 9 -10 5.80 1.90 1 9 -10 1.00 1.50 -1 -9 10 3.70 2.10 0 9 -10 16.00 2.80 0 9 -10 16.30 2.90 0 -9 10 18.10 3.20 -1 9 -10 4.90 1.80 -1 9 -10 4.20 1.70 1 -9 10 2.50 2.00 -2 9 -10 13.20 2.70 -2 9 -10 20.00 3.00 2 -9 10 13.40 2.90 -3 9 -10 10.30 2.30 -3 9 -10 13.20 2.70 3 -9 10 15.40 2.90 -4 9 -10 0.30 1.60 -4 9 -10 4.60 1.90 4 -9 10 2.50 1.90 -5 9 -10 0.60 1.70 -5 9 -10 2.70 1.80 -5 9 -10 1.30 1.70 5 -9 10 0.90 1.70 5 -9 10 4.00 2.10 -6 9 -10 0.00 1.70 -6 9 -10 1.00 1.90 -6 9 -10 2.50 1.70 6 -9 10 -0.90 1.60 6 -9 10 0.40 1.80 -7 9 -10 0.60 1.60 -7 9 -10 0.10 2.00 -7 9 -10 0.50 1.80 7 -9 10 -1.90 1.80 7 -9 10 1.90 1.90 -8 9 -10 42.30 5.20 -8 9 -10 39.40 4.90 -8 9 -10 36.20 4.70 8 -9 10 40.70 5.20 8 -9 10 32.10 4.50 -9 9 -10 1.10 1.90 9 -9 10 -0.70 2.40 9 -9 10 1.50 2.10 -10 9 -10 21.50 4.20 10 -9 10 25.40 4.90 -11 9 -10 38.70 5.70 11 -9 10 36.20 5.70 13 8 -10 3.00 2.90 13 8 -10 -3.10 2.10 -13 -8 10 6.30 3.70 12 8 -10 25.00 4.60 12 8 -10 29.60 5.00 -12 -8 10 26.90 5.20 11 8 -10 -2.00 2.00 11 8 -10 -0.50 1.90 -11 -8 10 -2.50 2.40 10 8 -10 19.70 4.00 10 8 -10 20.20 3.80 -10 -8 10 12.00 3.50 9 8 -10 26.60 4.40 -9 -8 10 19.60 4.00 8 8 -10 192.78 9.60 8 8 -10 191.68 10.00 -8 -8 10 187.38 10.10 7 8 -10 30.00 4.20 7 8 -10 30.60 4.10 -7 -8 10 25.30 4.00 6 8 -10 62.19 6.00 6 8 -10 60.19 4.70 -6 -8 10 53.09 5.40 5 8 -10 344.07 13.70 5 8 -10 360.76 14.20 -5 -8 10 362.96 13.30 -5 -8 10 348.07 14.20 4 8 -10 45.10 4.80 4 8 -10 44.00 3.80 -4 -8 10 35.80 4.20 -4 -8 10 42.90 4.20 3 8 -10 1.30 1.60 3 8 -10 1.70 1.40 -3 -8 10 2.00 1.70 -3 -8 10 1.30 1.50 2 8 -10 14.20 2.60 2 8 -10 10.70 2.40 -2 -8 10 10.00 2.40 1 8 -10 14.10 2.50 1 8 -10 16.30 2.60 -1 -8 10 14.20 2.70 0 8 -10 105.49 5.90 0 8 -10 111.69 6.00 0 -8 10 99.89 6.10 -1 8 -10 451.35 16.10 -1 8 -10 433.26 15.90 1 -8 10 449.86 16.40 -2 8 -10 23.40 3.20 -2 8 -10 24.10 3.30 2 -8 10 22.40 2.70 2 -8 10 24.10 3.30 -3 8 -10 206.68 9.20 -3 8 -10 204.38 9.00 -3 8 -10 212.88 8.70 3 -8 10 208.58 9.60 3 -8 10 209.48 8.60 -4 8 -10 -0.50 1.10 -4 8 -10 2.10 1.50 -4 8 -10 0.80 1.50 4 -8 10 1.80 1.70 4 -8 10 0.90 1.50 -5 8 -10 114.49 6.80 -5 8 -10 123.69 6.70 -5 8 -10 110.29 6.40 5 -8 10 118.39 6.60 5 -8 10 107.49 6.70 -6 8 -10 -1.00 1.70 -6 8 -10 -0.80 1.30 -6 8 -10 2.10 1.70 6 -8 10 -0.60 1.70 6 -8 10 -0.60 1.30 -7 8 -10 23.90 3.60 -7 8 -10 18.40 3.30 -7 8 -10 27.30 4.10 7 -8 10 22.90 3.90 7 -8 10 16.90 3.30 -8 8 -10 2.00 2.30 -8 8 -10 1.90 1.90 8 -8 10 5.70 2.90 8 -8 10 0.30 1.70 -9 8 -10 84.39 6.70 -9 8 -10 100.09 7.30 9 -8 10 83.39 7.00 9 -8 10 91.99 6.60 -10 8 -10 6.50 2.70 -10 8 -10 2.40 2.90 10 -8 10 1.40 2.80 -11 8 -10 25.20 4.70 11 -8 10 29.60 5.40 -12 8 -10 9.10 3.50 12 -8 10 1.50 3.60 13 7 -10 56.99 7.00 13 7 -10 53.39 6.90 -13 -7 10 38.10 6.00 12 7 -10 0.70 2.40 12 7 -10 3.70 2.70 -12 -7 10 3.70 2.90 11 7 -10 44.50 5.90 11 7 -10 45.60 5.60 -11 -7 10 45.40 5.90 10 7 -10 12.00 3.30 -10 -7 10 9.80 3.00 9 7 -10 64.29 6.20 9 7 -10 55.99 5.90 -9 -7 10 68.99 6.70 8 7 -10 4.80 2.30 8 7 -10 5.90 2.20 -8 -7 10 6.00 2.50 7 7 -10 55.79 5.70 7 7 -10 47.80 4.90 -7 -7 10 46.80 5.00 6 7 -10 8.70 2.30 6 7 -10 7.40 2.20 -6 -7 10 -0.30 0.70 -6 -7 10 2.60 1.70 5 7 -10 64.49 4.60 5 7 -10 66.69 4.80 -5 -7 10 61.59 4.10 -5 -7 10 66.99 5.00 4 7 -10 11.30 2.50 4 7 -10 13.30 2.50 -4 -7 10 8.80 2.30 -4 -7 10 7.10 1.90 3 7 -10 8.40 2.10 3 7 -10 9.20 2.20 -3 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2.20 2 6 -10 60.79 4.30 2 6 -10 71.49 4.20 2 6 -10 67.89 3.40 -2 -6 10 60.59 3.90 -2 -6 10 62.89 4.20 1 6 -10 0.20 0.90 1 6 -10 -0.10 0.70 1 6 -10 0.00 0.60 -1 -6 10 -0.90 0.90 0 6 -10 134.69 6.80 0 6 -10 153.68 6.10 0 -6 10 144.39 7.00 -1 6 -10 -0.10 0.80 -1 6 -10 0.80 1.10 -1 6 -10 -0.30 0.90 1 -6 10 0.00 1.20 -2 6 -10 148.99 7.30 -2 6 -10 150.08 6.50 -2 6 -10 159.28 6.80 2 -6 10 150.98 7.30 -3 6 -10 12.00 2.10 -3 6 -10 7.20 1.60 -3 6 -10 10.70 2.30 3 -6 10 10.80 2.20 3 -6 10 9.80 2.20 -4 6 -10 138.69 6.10 -4 6 -10 130.59 6.50 -4 6 -10 113.39 6.50 4 -6 10 119.89 6.40 4 -6 10 117.79 6.50 -5 6 -10 51.89 5.00 -5 6 -10 40.50 4.10 -5 6 -10 37.60 3.20 5 -6 10 46.80 4.60 5 -6 10 38.50 4.00 -6 6 -10 55.09 5.40 -6 6 -10 52.99 5.20 6 -6 10 57.69 4.60 6 -6 10 68.39 5.20 -7 6 -10 11.20 2.90 -7 6 -10 12.60 2.80 7 -6 10 13.10 3.20 7 -6 10 14.80 2.80 -8 6 -10 100.09 6.90 -8 6 -10 117.79 7.50 8 -6 10 110.09 7.30 8 -6 10 109.79 6.60 -9 6 -10 38.00 4.90 -9 6 -10 42.00 5.50 9 -6 10 42.80 4.70 9 -6 10 59.89 6.40 -10 6 -10 31.30 5.00 -10 6 -10 28.80 4.60 10 -6 10 40.40 5.60 -11 6 -10 17.00 4.30 -11 6 -10 19.50 4.60 11 -6 10 26.50 5.20 -12 6 -10 3.30 2.80 -12 6 -10 5.10 3.50 12 -6 10 4.40 3.30 14 5 -10 13.50 3.90 -14 -5 10 17.00 4.40 13 5 -10 1.50 2.50 -13 -5 10 2.30 2.80 12 5 -10 15.50 3.70 -12 -5 10 7.30 3.00 11 5 -10 3.50 2.60 -11 -5 10 11.20 3.10 10 5 -10 19.40 3.60 -10 -5 10 13.10 3.10 9 5 -10 170.98 9.10 -9 -5 10 185.78 9.30 8 5 -10 202.28 9.90 8 5 -10 220.98 8.80 -8 -5 10 217.08 10.00 7 5 -10 -0.50 1.10 7 5 -10 1.50 1.10 7 5 -10 -0.50 1.30 -7 -5 10 -0.70 1.40 6 5 -10 0.90 1.30 6 5 -10 -0.50 0.90 6 5 -10 0.40 1.20 -6 -5 10 0.00 1.30 5 5 -10 55.39 3.20 5 5 -10 52.49 3.80 -5 -5 10 34.30 2.90 -5 -5 10 57.29 4.00 4 5 -10 2.00 1.20 4 5 -10 4.20 1.10 4 5 -10 4.90 1.50 -4 -5 10 4.40 1.50 -4 -5 10 5.20 1.60 3 5 -10 1.70 1.10 3 5 -10 -0.10 0.70 3 5 -10 0.40 1.00 -3 -5 10 0.30 1.00 -3 -5 10 0.60 1.00 2 5 -10 0.10 1.00 2 5 -10 2.00 0.90 2 5 -10 0.20 0.40 -2 -5 10 0.10 1.00 -2 -5 10 0.30 1.10 1 5 -10 0.90 0.90 1 5 -10 -0.50 0.90 1 5 -10 0.40 0.80 -1 -5 10 1.20 1.10 0 5 -10 1.50 1.20 0 5 -10 0.10 0.80 0 5 -10 -0.80 0.70 0 -5 10 0.70 1.10 -1 5 -10 1.20 1.30 -1 5 -10 1.40 0.90 -1 5 -10 0.00 0.90 1 -5 10 1.50 1.20 -2 5 -10 3.00 1.10 -2 5 -10 1.50 1.20 -2 5 -10 1.00 1.20 2 -5 10 -0.10 1.00 -3 5 -10 14.80 2.00 -3 5 -10 12.20 2.40 -3 5 -10 12.70 2.20 3 -5 10 8.90 2.00 -4 5 -10 6.70 1.90 -4 5 -10 6.50 1.50 -4 5 -10 2.30 1.30 4 -5 10 4.60 1.70 4 -5 10 2.60 1.40 -5 5 -10 20.10 3.00 -5 5 -10 19.70 2.40 -5 5 -10 19.40 3.20 5 -5 10 19.40 3.00 5 -5 10 23.90 3.30 -6 5 -10 0.20 1.40 -6 5 -10 1.90 1.50 -6 5 -10 0.80 1.20 6 -5 10 1.10 1.30 6 -5 10 -0.10 1.80 -7 5 -10 57.59 5.70 -7 5 -10 57.89 4.90 7 -5 10 61.89 4.70 7 -5 10 56.39 5.70 -8 5 -10 30.70 4.50 -8 5 -10 31.10 4.30 8 -5 10 41.50 4.40 8 -5 10 41.90 5.30 -9 5 -10 27.60 4.40 -9 5 -10 19.00 3.80 9 -5 10 19.20 3.80 9 -5 10 28.00 3.80 -10 5 -10 50.19 6.00 -10 5 -10 53.29 6.20 10 -5 10 54.89 6.40 -11 5 -10 63.09 7.10 -11 5 -10 52.69 6.40 11 -5 10 45.30 6.00 -12 5 -10 6.00 3.10 -12 5 -10 -0.40 3.10 12 -5 10 7.60 3.80 14 4 -10 -2.90 2.20 -14 -4 10 0.00 2.60 13 4 -10 22.70 4.30 -13 -4 10 22.70 4.40 12 4 -10 0.80 1.80 -12 -4 10 3.70 2.40 11 4 -10 118.39 7.70 11 4 -10 113.29 6.70 -11 -4 10 120.59 7.80 10 4 -10 -1.30 1.50 10 4 -10 2.10 1.70 -10 -4 10 0.50 1.70 9 4 -10 176.48 9.00 9 4 -10 176.08 8.00 -9 -4 10 167.88 8.80 8 4 -10 -1.50 1.10 8 4 -10 0.80 1.30 -8 -4 10 1.40 1.50 7 4 -10 87.29 4.70 7 4 -10 83.59 5.50 -7 -4 10 78.19 5.10 6 4 -10 228.28 9.90 6 4 -10 231.18 8.90 -6 -4 10 245.68 9.80 -6 -4 10 237.88 8.60 5 4 -10 171.38 6.80 5 4 -10 159.08 7.70 5 4 -10 164.88 7.30 -5 -4 10 176.78 7.40 -5 -4 10 168.68 6.70 4 4 -10 185.38 6.90 4 4 -10 159.58 7.10 4 4 -10 177.68 7.90 -4 -4 10 175.98 7.20 -4 -4 10 171.18 6.90 3 4 -10 67.69 4.40 3 4 -10 67.89 3.60 -3 -4 10 72.19 4.00 -3 -4 10 72.49 3.90 2 4 -10 19.40 2.70 2 4 -10 16.20 2.00 2 4 -10 14.50 1.90 -2 -4 10 12.90 2.00 -2 -4 10 15.50 1.90 1 4 -10 45.30 2.70 1 4 -10 43.60 3.40 1 4 -10 45.30 2.90 -1 -4 10 43.50 3.20 0 4 -10 184.68 6.70 0 4 -10 187.28 7.30 0 4 -10 191.88 8.10 0 -4 10 186.68 7.70 -1 4 -10 192.58 6.80 -1 4 -10 181.78 8.20 -1 4 -10 195.08 7.70 1 -4 10 191.98 8.00 -2 4 -10 755.22 23.90 -2 4 -10 724.03 24.40 -2 4 -10 770.42 22.80 2 -4 10 766.12 24.20 -3 4 -10 56.09 3.90 -3 4 -10 60.79 4.20 -3 4 -10 58.39 3.10 3 -4 10 54.99 4.00 -4 4 -10 96.89 4.50 -4 4 -10 106.29 5.70 -4 4 -10 102.09 5.80 4 -4 10 104.69 5.60 -5 4 -10 30.20 3.70 -5 4 -10 30.70 3.80 5 -4 10 31.10 3.90 5 -4 10 25.20 3.20 -6 4 -10 104.19 6.40 -6 4 -10 112.19 6.60 6 -4 10 114.19 6.70 6 -4 10 105.39 6.00 -7 4 -10 2.60 2.10 -7 4 -10 7.20 2.40 7 -4 10 5.20 1.90 7 -4 10 3.50 2.20 -8 4 -10 86.79 6.30 -8 4 -10 86.79 6.20 8 -4 10 88.79 6.50 8 -4 10 85.79 5.60 -9 4 -10 -1.40 1.80 -9 4 -10 1.00 1.90 9 -4 10 1.10 2.20 9 -4 10 -1.50 1.30 -10 4 -10 33.40 5.00 -10 4 -10 36.80 5.50 10 -4 10 52.49 6.20 -11 4 -10 50.79 6.50 -11 4 -10 54.59 6.70 11 -4 10 33.90 5.30 -12 4 -10 11.80 4.00 -12 4 -10 13.50 3.80 12 -4 10 6.00 3.10 -13 4 -10 1.70 2.90 -13 4 -10 2.90 3.70 13 -4 10 0.30 3.00 13 -4 10 5.00 3.40 14 3 -10 6.10 3.20 -14 -3 10 6.10 2.90 13 3 -10 4.70 2.80 13 3 -10 3.70 2.30 -13 -3 10 8.50 3.20 12 3 -10 52.29 6.10 12 3 -10 34.50 4.50 -12 -3 10 31.90 4.60 11 3 -10 2.60 2.20 11 3 -10 0.00 1.50 -11 -3 10 -1.00 1.60 10 3 -10 112.99 6.30 10 3 -10 100.49 6.80 -10 -3 10 99.89 6.70 9 3 -10 5.30 2.10 9 3 -10 10.30 2.30 -9 -3 10 9.10 2.50 8 3 -10 241.78 9.50 8 3 -10 216.38 10.10 -8 -3 10 228.88 10.00 7 3 -10 0.50 1.20 7 3 -10 -0.50 1.00 -7 -3 10 0.70 1.20 6 3 -10 59.59 4.40 6 3 -10 68.99 4.00 -6 -3 10 68.79 4.30 -6 -3 10 66.99 3.40 5 3 -10 2.20 1.40 5 3 -10 2.90 1.20 -5 -3 10 3.90 1.30 -5 -3 10 3.80 1.20 4 3 -10 6.10 1.60 4 3 -10 7.00 1.50 -4 -3 10 4.40 1.20 3 3 -10 0.40 1.10 3 3 -10 1.50 0.90 3 3 -10 -0.20 0.70 -3 -3 10 0.30 0.70 -3 -3 10 0.60 0.90 2 3 -10 3.90 1.30 2 3 -10 4.50 1.30 2 3 -10 2.90 0.90 -2 -3 10 3.40 1.00 -2 -3 10 2.50 1.10 1 3 -10 25.40 1.70 1 3 -10 29.90 3.00 1 3 -10 28.30 2.70 -1 -3 10 23.60 2.60 0 3 -10 -0.30 0.80 0 3 -10 -0.20 0.50 0 3 -10 0.30 1.00 0 -3 10 0.10 1.00 -1 3 -10 -0.40 0.90 -1 3 -10 -0.10 0.50 -1 3 -10 0.60 0.90 1 -3 10 0.70 1.00 -2 3 -10 35.50 3.40 -2 3 -10 41.60 4.00 -2 3 -10 32.40 1.90 2 -3 10 36.70 3.30 -3 3 -10 33.50 3.50 -3 3 -10 30.20 2.00 -3 3 -10 33.90 3.40 3 -3 10 33.80 3.40 -4 3 -10 0.20 0.70 -4 3 -10 1.10 1.10 -4 3 -10 0.50 1.10 4 -3 10 0.00 1.10 -5 3 -10 90.49 5.60 -5 3 -10 86.89 5.40 5 -3 10 86.69 5.40 5 -3 10 86.69 5.20 -6 3 -10 1.60 1.40 -6 3 -10 -0.60 1.40 6 -3 10 2.10 1.40 6 -3 10 4.30 2.00 -7 3 -10 -1.00 1.40 -7 3 -10 5.50 2.10 7 -3 10 3.40 1.60 7 -3 10 5.80 2.40 -8 3 -10 0.30 1.40 -8 3 -10 0.70 1.70 8 -3 10 4.00 2.40 8 -3 10 -0.60 1.30 -9 3 -10 18.50 3.90 -9 3 -10 23.60 4.10 9 -3 10 18.00 3.90 9 -3 10 21.10 3.20 -10 3 -10 12.10 3.20 -10 3 -10 17.40 4.10 10 -3 10 9.40 3.30 -11 3 -10 54.69 6.50 -11 3 -10 62.69 7.20 11 -3 10 70.99 7.50 -12 3 -10 1.30 2.90 -12 3 -10 0.80 2.60 12 -3 10 3.20 2.90 12 -3 10 2.70 3.00 -13 3 -10 0.10 3.20 -13 3 -10 1.90 3.00 13 -3 10 0.50 3.00 13 -3 10 -2.70 2.90 15 2 -10 -3.10 2.60 15 2 -10 -1.00 2.40 -15 -2 10 2.70 3.10 14 2 -10 16.30 3.70 14 2 -10 14.00 4.10 -14 -2 10 5.50 3.10 13 2 -10 15.50 3.40 13 2 -10 15.80 4.10 -13 -2 10 18.10 3.80 12 2 -10 7.40 3.00 12 2 -10 6.30 2.60 -12 -2 10 6.10 2.70 11 2 -10 39.10 5.20 11 2 -10 33.00 4.20 -11 -2 10 34.70 4.50 10 2 -10 -1.30 1.20 10 2 -10 1.10 1.60 -10 -2 10 0.50 1.70 9 2 -10 -0.40 1.40 9 2 -10 1.20 1.60 -9 -2 10 1.70 1.70 8 2 -10 10.40 2.40 8 2 -10 6.50 2.00 -8 -2 10 7.60 2.00 7 2 -10 160.18 7.20 7 2 -10 153.58 7.70 -7 -2 10 154.88 7.30 6 2 -10 -0.20 1.00 6 2 -10 0.60 1.10 -6 -2 10 -0.10 0.70 -6 -2 10 1.20 1.10 5 2 -10 175.48 7.90 5 2 -10 173.68 7.30 -5 -2 10 178.78 6.60 -5 -2 10 173.48 7.10 4 2 -10 15.00 2.30 4 2 -10 13.10 2.00 -4 -2 10 21.40 2.20 3 2 -10 182.88 7.80 3 2 -10 179.68 7.20 -3 -2 10 174.38 6.90 -3 -2 10 181.98 6.60 2 2 -10 9.60 1.70 2 2 -10 9.00 1.80 2 2 -10 9.30 1.20 -2 -2 10 10.00 1.70 -2 -2 10 10.30 1.30 1 2 -10 17.80 2.20 1 2 -10 15.50 2.20 1 2 -10 14.30 1.20 -1 -2 10 15.90 1.20 -1 -2 10 17.80 2.20 0 2 -10 56.29 3.50 0 2 -10 52.29 3.70 0 -2 10 52.19 3.40 -1 2 -10 107.09 5.10 -1 2 -10 95.59 5.30 1 -2 10 97.29 5.00 -2 2 -10 46.30 3.60 -2 2 -10 44.30 1.80 -2 2 -10 45.90 3.40 2 -2 10 53.59 3.60 -3 2 -10 219.38 7.40 -3 2 -10 241.58 9.50 -3 2 -10 232.08 9.50 3 -2 10 232.78 9.20 -4 2 -10 46.00 3.70 -4 2 -10 54.89 4.10 4 -2 10 46.80 3.60 -5 2 -10 167.28 8.20 -5 2 -10 182.68 8.60 5 -2 10 198.28 8.20 -6 2 -10 183.68 9.10 -6 2 -10 201.78 9.30 6 -2 10 202.08 9.50 6 -2 10 191.68 8.50 -7 2 -10 1.60 1.70 -7 2 -10 -0.90 1.50 7 -2 10 2.30 1.50 7 -2 10 -1.30 1.80 -8 2 -10 14.50 3.10 -8 2 -10 18.60 3.40 8 -2 10 16.20 3.30 8 -2 10 18.10 3.00 -9 2 -10 66.69 6.60 -9 2 -10 58.19 6.20 9 -2 10 54.59 5.90 9 -2 10 57.29 4.60 -10 2 -10 46.70 6.00 -10 2 -10 35.70 5.20 10 -2 10 50.19 6.10 -11 2 -10 19.40 4.10 -11 2 -10 6.20 3.00 11 -2 10 20.10 4.30 -12 2 -10 22.30 5.00 -12 2 -10 13.40 3.80 12 -2 10 18.00 4.20 12 -2 10 14.50 4.10 -13 2 -10 1.80 3.00 -13 2 -10 3.50 3.30 13 -2 10 2.80 3.00 13 -2 10 0.70 2.90 15 1 -10 4.50 3.50 15 1 -10 6.40 3.20 -15 -1 10 8.60 3.70 14 1 -10 1.00 2.40 14 1 -10 -0.20 2.10 -14 -1 10 -2.90 1.80 13 1 -10 33.20 5.20 13 1 -10 17.00 3.60 -13 -1 10 13.20 3.50 12 1 -10 48.20 5.90 -12 -1 10 48.50 5.80 11 1 -10 16.00 3.40 11 1 -10 22.10 3.50 -11 -1 10 25.30 3.80 10 1 -10 143.69 8.10 10 1 -10 150.88 7.80 -10 -1 10 134.59 7.60 9 1 -10 117.99 6.60 9 1 -10 127.09 7.20 -9 -1 10 121.39 6.80 8 1 -10 2.60 1.50 8 1 -10 5.20 1.70 -8 -1 10 6.30 1.90 7 1 -10 28.60 3.50 7 1 -10 22.20 2.90 -7 -1 10 26.50 3.10 6 1 -10 43.10 3.70 6 1 -10 46.20 3.40 -6 -1 10 47.00 3.30 -6 -1 10 47.90 2.60 5 1 -10 14.50 2.30 5 1 -10 8.70 1.90 -5 -1 10 10.40 1.50 -5 -1 10 10.40 1.70 4 1 -10 22.50 2.70 4 1 -10 21.60 2.50 -4 -1 10 22.60 2.20 3 1 -10 8.60 1.70 3 1 -10 3.10 1.30 -3 -1 10 5.80 1.10 -3 -1 10 6.30 1.30 2 1 -10 6.60 1.70 2 1 -10 9.40 1.70 -2 -1 10 8.50 1.60 -2 -1 10 7.80 1.00 1 1 -10 26.70 2.90 1 1 -10 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10 -14 154.98 8.90 4 -10 14 171.18 9.60 -5 10 -14 12.30 3.50 5 -10 14 8.60 3.20 -6 10 -14 30.00 4.60 6 -10 14 22.50 4.20 -7 10 -14 17.40 3.80 7 -10 14 33.30 5.10 -8 10 -14 10.30 3.50 8 -10 14 11.40 3.50 -9 10 -14 16.50 4.00 9 -10 14 29.20 5.00 11 9 -14 1.30 2.80 11 9 -14 4.10 3.10 -11 -9 14 4.20 3.40 10 9 -14 13.10 3.60 10 9 -14 11.00 3.60 -10 -9 14 17.90 4.30 9 9 -14 12.90 3.40 9 9 -14 8.80 3.00 -9 -9 14 14.90 3.80 8 9 -14 -1.90 1.60 8 9 -14 -0.10 2.10 -8 -9 14 -0.50 2.40 7 9 -14 3.80 2.20 7 9 -14 5.70 2.70 -7 -9 14 1.20 2.40 6 9 -14 9.30 2.70 -6 -9 14 14.00 3.40 5 9 -14 0.00 1.80 5 9 -14 2.30 1.90 -5 -9 14 -0.20 1.90 -5 -9 14 -1.00 1.80 4 9 -14 -0.10 1.60 4 9 -14 -0.30 1.60 -4 -9 14 -0.90 1.80 3 9 -14 6.50 2.40 3 9 -14 5.50 2.20 -3 -9 14 4.60 2.20 2 9 -14 0.60 1.70 2 9 -14 1.30 1.70 -2 -9 14 2.00 2.30 1 9 -14 1.20 1.70 -1 -9 14 -1.50 1.60 0 9 -14 4.70 2.10 0 -9 14 3.80 2.40 -1 9 -14 1.60 1.60 1 -9 14 0.10 2.20 -2 9 -14 7.90 2.60 2 -9 14 8.20 2.80 -3 9 -14 7.60 2.50 3 -9 14 3.40 2.50 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1 7 -22 2.30 2.70 -1 -7 22 6.60 3.40 0 7 -22 3.10 2.80 0 -7 22 7.10 3.30 -1 7 -22 -0.60 2.50 -1 7 -22 -0.50 2.30 1 -7 22 -1.30 2.80 -2 7 -22 4.50 3.00 -2 7 -22 2.80 2.90 2 -7 22 -0.70 2.70 -3 7 -22 4.50 3.30 -3 7 -22 3.80 3.30 3 -7 22 -1.20 2.90 8 6 -22 0.10 3.00 7 6 -22 27.20 5.10 6 6 -22 0.90 2.90 5 6 -22 7.10 3.40 4 6 -22 0.60 2.60 -4 -6 22 2.00 2.70 3 6 -22 24.40 4.70 -3 -6 22 21.80 4.40 2 6 -22 0.70 2.40 2 6 -22 1.90 2.40 -2 -6 22 2.90 2.90 1 6 -22 22.50 4.60 1 6 -22 25.60 4.40 -1 -6 22 14.50 3.90 0 6 -22 0.50 2.40 0 6 -22 -1.90 2.20 0 -6 22 -3.00 2.10 -1 6 -22 30.70 4.90 -1 6 -22 26.20 5.10 1 -6 22 20.70 4.40 -2 6 -22 2.70 2.90 -2 6 -22 -0.20 2.60 2 -6 22 -3.40 2.60 -3 6 -22 5.70 3.20 -3 6 -22 8.70 3.40 3 -6 22 3.70 3.10 -4 6 -22 1.30 2.80 -4 6 -22 0.20 3.10 4 -6 22 1.40 2.80 8 5 -22 5.20 3.60 7 5 -22 1.40 2.70 6 5 -22 -1.30 2.70 5 5 -22 -0.40 2.60 5 5 -22 -3.60 1.90 4 5 -22 0.10 2.60 4 5 -22 3.00 2.40 -4 -5 22 0.60 2.60 3 5 -22 -0.20 2.00 3 5 -22 0.60 2.60 -3 -5 22 2.20 2.50 2 5 -22 4.90 2.80 2 5 -22 6.20 3.30 -2 -5 22 1.80 2.50 1 5 -22 -0.10 2.40 1 5 -22 0.00 2.60 -1 -5 22 0.50 2.60 0 5 -22 -1.10 2.30 0 5 -22 -0.30 2.20 0 -5 22 1.40 2.60 -1 5 -22 -0.70 2.30 -1 5 -22 3.10 3.10 1 -5 22 -0.40 2.70 -2 5 -22 2.70 2.80 -2 5 -22 -0.90 2.40 2 -5 22 -2.30 2.40 -3 5 -22 3.00 3.00 -3 5 -22 0.20 2.80 3 -5 22 0.10 2.60 -4 5 -22 12.40 3.80 -4 5 -22 14.60 4.40 4 -5 22 12.10 3.80 9 4 -22 28.40 5.40 8 4 -22 18.90 4.50 8 4 -22 14.70 3.90 7 4 -22 4.50 3.10 7 4 -22 8.50 3.20 6 4 -22 3.70 2.80 6 4 -22 4.60 3.00 5 4 -22 1.90 2.90 5 4 -22 -0.60 2.30 4 4 -22 8.90 3.20 4 4 -22 9.60 3.40 -4 -4 22 4.80 2.80 3 4 -22 14.00 3.80 3 4 -22 11.40 3.40 -3 -4 22 4.30 3.00 2 4 -22 12.40 3.30 2 4 -22 9.70 3.50 -2 -4 22 10.10 3.30 1 4 -22 30.30 5.00 1 4 -22 36.10 5.10 -1 -4 22 24.20 4.60 0 4 -22 0.20 2.50 0 4 -22 1.90 2.80 0 -4 22 2.10 2.90 -1 4 -22 10.90 3.60 -1 4 -22 12.40 4.10 1 -4 22 10.50 3.80 -2 4 -22 4.00 3.20 -2 4 -22 -0.20 2.50 2 -4 22 2.10 2.70 -3 4 -22 10.10 3.80 -3 4 -22 9.30 3.80 3 -4 22 9.40 3.60 -4 4 -22 20.70 4.70 -4 4 -22 16.20 4.50 4 -4 22 19.30 4.60 9 3 -22 23.10 5.10 9 3 -22 25.70 4.80 8 3 -22 0.50 2.70 8 3 -22 0.60 2.80 7 3 -22 2.10 2.90 7 3 -22 1.20 2.60 6 3 -22 3.20 2.80 6 3 -22 0.50 2.70 5 3 -22 2.20 2.60 5 3 -22 0.10 2.50 4 3 -22 0.70 2.10 4 3 -22 -1.20 2.20 -4 -3 22 5.30 2.80 3 3 -22 3.00 2.60 3 3 -22 0.70 2.20 -3 -3 22 -1.00 2.30 2 3 -22 1.60 2.50 2 3 -22 -1.00 2.30 -2 -3 22 4.30 2.80 1 3 -22 -2.50 2.20 1 3 -22 0.40 2.50 -1 -3 22 1.60 2.60 0 3 -22 2.70 2.80 0 3 -22 -0.20 2.10 0 -3 22 -3.70 2.30 -1 3 -22 -0.80 2.10 -1 3 -22 1.30 2.70 1 -3 22 0.80 2.70 -2 3 -22 -2.80 2.30 -2 3 -22 3.50 3.00 2 -3 22 2.10 2.80 -3 3 -22 8.00 3.60 -3 3 -22 2.90 3.00 3 -3 22 4.30 3.00 -4 3 -22 1.00 2.90 -4 3 -22 -2.90 2.80 4 -3 22 1.00 2.60 9 2 -22 -0.40 2.80 9 2 -22 0.30 2.80 8 2 -22 8.20 3.50 8 2 -22 12.50 3.80 7 2 -22 0.20 2.60 7 2 -22 0.70 2.80 6 2 -22 3.20 2.90 6 2 -22 1.10 2.50 5 2 -22 4.90 3.10 5 2 -22 5.10 2.80 4 2 -22 8.70 3.20 4 2 -22 3.60 2.90 -4 -2 22 5.20 2.70 3 2 -22 -1.90 2.10 3 2 -22 2.70 2.80 -3 -2 22 3.10 2.70 2 2 -22 18.40 4.00 2 2 -22 24.30 4.90 -2 -2 22 26.80 4.50 1 2 -22 14.50 4.00 1 2 -22 18.00 4.20 -1 -2 22 21.60 4.40 0 2 -22 27.40 4.70 0 2 -22 35.20 5.70 0 -2 22 30.70 5.00 -1 2 -22 23.80 4.70 -1 2 -22 32.60 5.30 1 -2 22 32.40 5.20 -2 2 -22 1.30 2.80 -2 2 -22 -2.60 2.40 2 -2 22 1.70 2.70 -3 2 -22 5.60 3.50 -3 2 -22 2.50 3.20 3 -2 22 6.60 3.50 -4 2 -22 0.70 2.90 -4 2 -22 4.60 3.60 4 -2 22 2.40 2.90 9 1 -22 5.00 3.40 9 1 -22 1.90 3.20 8 1 -22 0.70 2.90 8 1 -22 0.60 2.60 7 1 -22 9.50 3.60 7 1 -22 5.60 3.30 6 1 -22 0.90 2.50 6 1 -22 -0.60 2.60 5 1 -22 4.20 3.00 5 1 -22 7.20 3.10 4 1 -22 -1.20 2.30 4 1 -22 -1.10 2.20 -4 -1 22 1.80 2.50 3 1 -22 0.70 2.60 3 1 -22 4.00 3.10 -3 -1 22 1.70 2.40 2 1 -22 -1.80 2.30 2 1 -22 1.70 2.40 -2 -1 22 0.30 2.40 1 1 -22 4.00 3.10 1 1 -22 4.30 2.90 -1 -1 22 0.00 2.50 0 1 -22 -0.80 2.40 0 1 -22 2.50 2.80 0 -1 22 4.50 2.90 -1 1 -22 -0.10 2.50 -1 1 -22 5.80 3.40 1 -1 22 -0.70 2.60 -2 1 -22 13.60 3.90 -2 1 -22 10.20 3.50 2 -1 22 10.10 3.80 -3 1 -22 -0.30 2.80 -3 1 -22 2.30 2.90 3 -1 22 0.80 2.90 -4 1 -22 1.70 3.20 -4 1 -22 2.60 2.90 4 -1 22 2.40 3.10 9 0 -22 1.70 3.20 9 0 -22 3.30 3.20 8 0 -22 -0.50 2.70 8 0 -22 0.20 2.90 7 0 -22 15.90 4.30 7 0 -22 16.70 4.30 6 0 -22 39.20 5.60 6 0 -22 39.80 5.60 5 0 -22 1.10 2.90 5 0 -22 0.60 2.70 4 0 -22 5.70 3.20 4 0 -22 5.70 3.20 -4 0 22 9.10 3.40 3 0 -22 3.20 2.90 3 0 -22 7.00 3.30 -3 0 22 6.50 3.00 2 0 -22 21.80 4.50 2 0 -22 17.20 4.00 -2 0 22 27.80 4.80 1 0 -22 -2.20 2.50 1 0 -22 1.70 2.80 -1 0 22 1.00 2.50 0 0 -22 8.10 3.30 0 0 -22 3.10 2.70 0 0 22 8.10 3.30 -1 0 -22 5.30 3.10 -1 0 -22 3.10 3.00 1 0 22 1.30 2.70 -2 0 -22 7.70 3.60 -2 0 -22 6.10 3.30 2 0 22 2.20 3.00 -3 0 -22 12.80 4.40 -3 0 -22 9.50 3.60 3 0 22 8.40 3.70 8 -1 -22 6.90 3.40 8 -1 -22 5.70 3.60 7 -1 -22 -1.30 2.60 7 -1 -22 6.20 3.20 6 -1 -22 0.20 2.80 6 -1 -22 4.00 3.20 5 -1 -22 1.60 2.80 5 -1 -22 1.30 2.70 4 -1 -22 0.10 2.80 4 -1 -22 -0.30 2.50 -4 1 22 1.80 2.60 3 -1 -22 0.10 2.70 3 -1 -22 -2.30 2.40 -3 1 22 2.30 2.70 2 -1 -22 -1.60 2.40 2 -1 -22 2.20 2.80 -2 1 22 -1.80 2.40 1 -1 -22 1.70 2.60 1 -1 -22 4.30 3.10 -1 1 22 0.20 2.50 0 -1 -22 1.40 2.80 0 -1 -22 0.80 3.20 0 1 22 -0.10 2.70 -1 -1 -22 -0.40 2.50 -1 -1 -22 -0.10 2.60 1 1 22 -3.30 2.50 -2 -1 -22 -0.70 2.80 -2 -1 -22 2.40 3.00 2 1 22 1.20 3.00 -3 -1 -22 7.90 3.80 -3 -1 -22 2.40 3.00 3 1 22 2.80 3.00 7 -2 -22 12.80 3.90 6 -2 -22 3.30 3.10 5 -2 -22 3.50 3.40 4 -2 -22 5.00 3.40 -4 2 22 1.90 2.70 3 -2 -22 -2.90 2.60 -3 2 22 3.50 3.00 2 -2 -22 9.30 3.90 -2 2 22 8.70 3.40 1 -2 -22 -0.30 2.90 -1 2 22 0.00 2.80 0 -2 -22 3.20 3.40 0 2 22 -1.80 2.70 -1 -2 -22 8.50 3.90 1 2 22 13.10 4.20 -2 -2 -22 10.20 4.30 2 2 22 15.00 4.40 6 -3 -22 4.10 3.50 5 -3 -22 -1.50 3.00 4 -3 -22 0.80 3.20 -4 3 22 -2.60 2.60 3 -3 -22 1.90 3.20 -3 3 22 5.40 3.20 2 -3 -22 -0.50 3.10 -2 3 22 1.20 2.90 1 -3 -22 -0.10 3.00 -1 3 22 0.60 3.00 0 -3 -22 0.30 2.90 0 3 22 6.30 3.60 -1 -3 -22 -2.50 2.80 1 3 22 1.60 3.10 4 -4 -22 2.80 3.50 4 -4 -22 -2.60 2.60 -4 4 22 3.60 3.30 3 -4 -22 15.20 4.60 3 -4 -22 10.70 3.80 -3 4 22 11.00 3.90 2 -4 -22 -0.20 3.00 2 -4 -22 0.40 3.20 -2 4 22 1.60 3.00 5 8 -23 0.20 3.00 4 8 -23 6.30 3.50 -4 -8 23 -1.30 2.80 3 8 -23 -0.40 2.80 -3 -8 23 0.70 3.00 2 8 -23 1.80 3.10 -2 -8 23 0.90 3.10 1 8 -23 1.50 2.90 -1 -8 23 1.00 3.10 0 8 -23 -0.50 2.80 0 -8 23 2.30 3.30 -1 8 -23 24.50 4.90 1 -8 23 22.30 5.30 6 7 -23 1.00 2.80 5 7 -23 25.30 5.20 4 7 -23 -1.50 2.50 -4 -7 23 2.70 3.00 3 7 -23 22.40 4.90 -3 -7 23 18.80 4.40 2 7 -23 0.30 2.80 -2 -7 23 1.50 3.10 1 7 -23 12.30 4.20 -1 -7 23 10.80 4.10 0 7 -23 -2.40 2.60 0 -7 23 3.60 3.20 -1 7 -23 5.90 3.20 1 -7 23 8.10 3.70 -2 7 -23 6.40 3.40 -2 7 -23 6.10 3.60 2 -7 23 0.40 3.00 7 6 -23 7.50 3.80 6 6 -23 0.30 2.90 5 6 -23 7.60 3.60 4 6 -23 -1.80 2.60 -4 -6 23 -0.50 2.70 3 6 -23 4.30 3.10 -3 -6 23 -0.60 2.60 2 6 -23 4.50 3.10 2 6 -23 3.50 3.20 -2 -6 23 4.20 3.20 1 6 -23 11.80 4.00 1 6 -23 5.50 3.00 -1 -6 23 -4.20 2.40 0 6 -23 4.50 2.90 0 6 -23 -1.60 2.50 0 -6 23 0.40 2.70 -1 6 -23 1.90 3.10 -1 6 -23 2.40 2.90 1 -6 23 -4.00 2.40 -2 6 -23 1.80 3.00 -2 6 -23 -3.90 2.60 2 -6 23 0.30 2.80 7 5 -23 4.90 3.40 6 5 -23 13.90 4.30 5 5 -23 6.00 3.00 5 5 -23 0.50 3.00 4 5 -23 3.90 3.10 4 5 -23 4.10 2.60 -4 -5 23 5.70 3.00 3 5 -23 2.30 2.80 3 5 -23 -0.80 2.20 -3 -5 23 -1.30 2.50 2 5 -23 15.50 3.80 2 5 -23 8.90 3.50 -2 -5 23 12.80 3.90 1 5 -23 14.50 4.10 1 5 -23 11.40 3.70 -1 -5 23 15.00 4.10 0 5 -23 19.80 4.30 0 5 -23 14.40 4.30 0 -5 23 20.90 4.20 -1 5 -23 8.90 3.70 -1 5 -23 1.40 2.50 1 -5 23 7.70 3.70 -2 5 -23 8.10 3.70 -2 5 -23 5.00 3.40 2 -5 23 11.80 3.90 -3 5 -23 26.60 5.30 -3 5 -23 25.90 5.60 3 -5 23 34.30 5.70 7 4 -23 13.10 3.90 7 4 -23 6.70 3.70 6 4 -23 -1.40 2.80 6 4 -23 1.50 2.70 5 4 -23 2.60 2.80 5 4 -23 1.60 2.70 4 4 -23 1.70 2.90 4 4 -23 1.50 2.40 -4 -4 23 0.90 2.50 3 4 -23 3.70 2.80 3 4 -23 4.10 3.20 -3 -4 23 3.50 2.90 2 4 -23 4.00 2.70 2 4 -23 7.70 3.60 -2 -4 23 3.50 3.00 1 4 -23 12.00 3.70 1 4 -23 15.10 4.30 -1 -4 23 4.90 3.20 0 4 -23 5.80 3.20 0 4 -23 4.80 3.30 0 -4 23 4.20 3.00 -1 4 -23 1.20 3.00 -1 4 -23 1.10 2.80 1 -4 23 -2.50 2.60 -2 4 -23 -0.80 2.70 -2 4 -23 0.20 2.80 2 -4 23 3.70 3.20 -3 4 -23 3.60 3.50 -3 4 -23 2.30 3.10 3 -4 23 1.10 3.10 8 3 -23 41.10 6.00 7 3 -23 -2.50 2.50 7 3 -23 -0.40 2.60 6 3 -23 9.20 3.70 6 3 -23 14.30 3.90 5 3 -23 -0.70 2.70 5 3 -23 0.30 2.60 4 3 -23 1.90 2.90 4 3 -23 7.20 3.40 -4 -3 23 6.00 2.90 3 3 -23 12.60 3.70 3 3 -23 6.40 3.00 -3 -3 23 6.50 3.10 2 3 -23 60.49 6.90 2 3 -23 43.90 6.10 -2 -3 23 56.39 6.50 1 3 -23 1.20 2.60 1 3 -23 1.70 2.90 -1 -3 23 -1.20 2.50 0 3 -23 20.90 4.40 0 3 -23 19.90 4.50 0 -3 23 16.60 3.90 -1 3 -23 -0.60 2.70 -1 3 -23 -0.70 2.40 1 -3 23 -0.40 2.80 -2 3 -23 6.40 3.80 -2 3 -23 14.70 4.20 2 -3 23 11.00 3.90 -3 3 -23 13.20 4.60 -3 3 -23 19.10 4.90 3 -3 23 18.20 4.70 8 2 -23 20.50 4.70 8 2 -23 13.50 4.20 7 2 -23 3.70 3.00 7 2 -23 2.50 3.40 6 2 -23 15.50 4.40 6 2 -23 8.90 3.40 5 2 -23 2.50 3.00 5 2 -23 1.20 2.70 4 2 -23 2.60 3.10 4 2 -23 -1.50 2.40 -4 -2 23 0.20 2.30 3 2 -23 -0.20 2.40 3 2 -23 2.50 3.00 -3 -2 23 3.00 2.90 2 2 -23 0.10 2.60 2 2 -23 2.60 2.80 -2 -2 23 1.80 2.80 1 2 -23 -1.20 2.40 1 2 -23 -0.20 2.50 -1 -2 23 2.70 2.80 0 2 -23 5.00 3.20 0 2 -23 -0.90 2.60 0 -2 23 1.60 2.80 -1 2 -23 0.30 2.60 -1 2 -23 2.20 2.90 1 -2 23 -1.40 2.50 -2 2 -23 3.90 3.40 -2 2 -23 1.10 2.90 2 -2 23 0.50 2.90 -3 2 -23 0.90 3.10 -3 2 -23 -0.10 3.20 3 -2 23 0.70 3.20 7 1 -23 26.10 5.00 7 1 -23 35.80 5.60 6 1 -23 -1.90 2.50 6 1 -23 -3.50 2.30 5 1 -23 6.10 3.30 5 1 -23 9.20 3.30 4 1 -23 14.90 4.00 4 1 -23 7.50 3.40 -4 -1 23 13.90 3.70 3 1 -23 -0.70 2.50 3 1 -23 4.30 3.10 -3 -1 23 2.10 2.70 2 1 -23 11.20 3.70 2 1 -23 18.40 4.40 -2 -1 23 19.30 4.20 1 1 -23 1.30 3.00 1 1 -23 3.30 3.00 -1 -1 23 4.90 3.00 0 1 -23 10.80 3.70 0 1 -23 4.10 3.10 0 -1 23 5.40 3.30 -1 1 -23 -1.00 2.50 -1 1 -23 4.10 3.40 1 -1 23 2.10 2.90 -2 1 -23 31.30 5.50 -2 1 -23 36.90 6.30 2 -1 23 31.10 5.40 7 0 -23 3.10 3.20 7 0 -23 1.10 3.00 6 0 -23 5.30 3.30 6 0 -23 4.10 3.20 5 0 -23 -2.30 2.70 4 0 -23 1.90 2.90 -4 0 23 0.40 2.70 3 0 -23 10.30 3.90 -3 0 23 16.50 4.10 2 0 -23 1.50 2.50 -2 0 23 4.50 3.00 1 0 -23 -2.80 2.60 -1 0 23 0.60 2.70 0 0 -23 1.70 3.40 0 0 23 -3.20 2.60 -1 0 -23 0.20 2.80 -1 0 -23 -1.70 3.10 1 0 23 0.30 3.10 -2 0 -23 3.40 3.20 -2 0 -23 2.30 3.30 2 0 23 0.90 3.20 6 -1 -23 8.80 5.80 6 -1 -23 12.10 4.30 5 -1 -23 11.70 5.10 5 -1 -23 2.70 3.40 4 -1 -23 0.70 3.10 4 -1 -23 5.60 3.80 -4 1 23 3.40 2.90 3 -1 -23 24.10 6.50 3 -1 -23 20.20 4.90 -3 1 23 16.30 4.00 2 -1 -23 5.10 3.00 -2 1 23 -0.40 2.70 1 -1 -23 19.00 4.70 -1 1 23 10.80 3.80 0 -1 -23 3.40 3.40 0 1 23 3.90 3.20 -1 -1 -23 22.70 5.30 1 1 23 41.40 6.10 5 -2 -23 4.00 3.40 4 -2 -23 -0.60 3.20 -4 2 23 3.50 3.10 3 -2 -23 5.50 3.60 -3 2 23 2.20 3.20 2 -2 -23 0.80 3.30 -2 2 23 0.50 3.00 1 -2 -23 0.40 3.30 -1 2 23 0.10 3.00 2 7 -24 4.20 3.40 -2 -7 24 3.40 3.40 4 6 -24 18.20 4.80 -4 -6 24 6.00 3.60 3 6 -24 2.10 3.30 -3 -6 24 4.30 3.20 2 6 -24 29.20 5.60 -2 -6 24 34.80 5.60 1 6 -24 -0.90 2.70 1 6 -24 0.60 3.00 -1 -6 24 3.20 3.30 0 6 -24 24.30 5.20 0 6 -24 32.70 5.60 0 -6 24 30.10 5.50 5 5 -24 -1.90 2.90 4 5 -24 -0.10 2.60 4 5 -24 3.70 3.50 -4 -5 24 1.30 2.90 3 5 -24 2.20 2.60 3 5 -24 2.70 3.20 2 5 -24 -1.30 2.90 2 5 -24 -0.80 2.60 -2 -5 24 -1.10 2.80 1 5 -24 18.70 4.70 1 5 -24 11.40 3.80 -1 -5 24 15.60 4.50 0 5 -24 6.70 3.70 0 5 -24 8.40 3.80 0 -5 24 7.90 3.80 6 4 -24 0.20 2.60 6 4 -24 2.90 3.30 5 4 -24 17.10 4.70 5 4 -24 19.10 4.40 4 4 -24 3.00 2.90 4 4 -24 4.30 3.10 -4 -4 24 0.40 2.90 3 4 -24 60.39 6.90 3 4 -24 68.39 7.70 2 4 -24 38.00 6.00 2 4 -24 58.49 6.80 -2 -4 24 54.39 6.40 1 4 -24 8.60 3.60 1 4 -24 6.20 3.40 -1 -4 24 12.80 4.30 0 4 -24 1.20 3.00 0 4 -24 2.40 3.20 0 -4 24 7.10 3.70 -1 4 -24 12.30 4.10 -1 4 -24 14.90 4.60 1 -4 24 15.70 4.60 6 3 -24 2.20 3.10 6 3 -24 3.90 3.20 5 3 -24 2.10 3.10 5 3 -24 0.20 2.70 4 3 -24 3.80 2.80 4 3 -24 0.80 2.90 -4 -3 24 5.10 3.20 3 3 -24 14.20 4.00 3 3 -24 11.90 4.20 2 3 -24 8.80 3.50 2 3 -24 14.30 4.30 -2 -3 24 18.40 4.20 1 3 -24 15.20 4.20 1 3 -24 8.80 3.80 -1 -3 24 8.00 3.70 0 3 -24 4.80 3.10 0 3 -24 4.10 3.30 0 -3 24 4.00 3.40 -1 3 -24 -1.70 3.00 -1 3 -24 1.10 3.10 1 -3 24 0.80 3.00 6 2 -24 -0.70 2.70 6 2 -24 0.20 3.20 5 2 -24 11.10 4.00 5 2 -24 8.10 3.70 4 2 -24 1.20 3.00 4 2 -24 -0.80 2.80 -4 -2 24 -0.40 2.70 3 2 -24 37.00 5.90 3 2 -24 30.50 5.40 -3 -2 24 35.90 5.30 2 2 -24 -0.10 3.00 2 2 -24 -5.30 2.30 -2 -2 24 -0.40 2.90 1 2 -24 25.20 5.00 1 2 -24 30.60 5.60 -1 -2 24 32.70 5.40 0 2 -24 8.90 3.90 0 2 -24 7.60 3.90 0 -2 24 12.40 4.20 5 1 -24 0.90 2.90 5 1 -24 2.90 3.40 4 1 -24 0.90 2.90 4 1 -24 0.50 3.20 -4 -1 24 1.10 2.90 3 1 -24 0.40 2.90 3 1 -24 -4.80 2.60 -3 -1 24 0.30 2.80 2 1 -24 11.00 4.20 2 1 -24 7.80 3.70 -2 -1 24 12.10 3.70 1 1 -24 20.30 4.50 1 1 -24 20.40 4.90 -1 -1 24 19.90 4.50 0 1 -24 2.80 3.50 0 1 -24 4.90 3.60 0 -1 24 3.20 3.40 4 0 -24 14.20 4.40 4 0 -24 26.70 5.20 -4 0 24 23.30 4.50 3 0 -24 5.40 3.60 3 0 -24 5.70 3.40 -3 0 24 7.30 3.40 2 0 -24 18.00 4.70 2 0 -24 26.70 5.20 -2 0 24 19.50 4.50 1 0 -24 -2.70 3.00 1 0 -24 13.60 4.30 -1 0 24 3.40 3.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 75347 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.75112(2) 0.94514(2) 0.31932(2) 0.02287(9) Uani 1 1 d . . . . . N1 N 0.64357(14) 0.91333(15) 0.22252(10) 0.0188(4) Uani 1 1 d . . . . . N2 N 0.60004(14) 0.91189(15) 0.35250(10) 0.0183(4) Uani 1 1 d . . . . . N3 N 0.82755(14) 1.09398(15) 0.33679(10) 0.0213(4) Uani 1 1 d . . . . . N4 N 0.88062(14) 0.87287(16) 0.35565(10) 0.0203(4) Uani 1 1 d . . . . . C1 C 0.9876(2) 1.2360(2) 0.38259(15) 0.0348(6) Uani 1 1 d . . . . . H1A H 0.995246 1.253412 0.335657 0.052 Uiso 1 1 calc R U . . . H1B H 1.062065 1.242595 0.413471 0.052 Uiso 1 1 calc R U . . . H1C H 0.940117 1.287663 0.406996 0.052 Uiso 1 1 calc R U . . . C2 C 0.93386(18) 1.1191(2) 0.36965(12) 0.0230(5) Uani 1 1 d . . . . . C3 C 1.00186(17) 1.0423(2) 0.39546(12) 0.0248(5) Uani 1 1 d . . . . . H3 H 1.074543 1.071946 0.421781 0.030 Uiso 1 1 calc R U . . . C4 C 0.97860(17) 0.9288(2) 0.38823(12) 0.0214(5) Uani 1 1 d . . . . . C5 C 1.07320(18) 0.8681(2) 0.41988(13) 0.0291(6) Uani 1 1 d . . . . . H5A H 1.055917 0.847339 0.464004 0.044 Uiso 1 1 calc R U . . . H5B H 1.143596 0.916204 0.432300 0.044 Uiso 1 1 calc R U . . . H5C H 1.081314 0.801469 0.383807 0.044 Uiso 1 1 calc R U . . . C10 C 0.67218(18) 0.91881(18) 0.15638(12) 0.0214(5) Uani 1 1 d . . . . . C11 C 0.78678(19) 0.9232(2) 0.15099(13) 0.0275(5) Uani 1 1 d . . . . . H11 H 0.842442 0.925587 0.193002 0.033 Uiso 1 1 calc R U . . . C12 C 0.8182(2) 0.9241(2) 0.08526(14) 0.0322(6) Uani 1 1 d . . . . . H12 H 0.895702 0.927177 0.081907 0.039 Uiso 1 1 calc R U . . . C13 C 0.7366(2) 0.9206(2) 0.02274(14) 0.0344(6) Uani 1 1 d . . . . . H13 H 0.759182 0.920702 -0.022705 0.041 Uiso 1 1 calc R U . . . C14 C 0.6254(2) 0.9170(2) 0.02705(13) 0.0304(6) Uani 1 1 d . . . . . H14 H 0.570946 0.915324 -0.015467 0.036 Uiso 1 1 calc R U . . . C15 C 0.58978(19) 0.91582(19) 0.09381(12) 0.0250(5) Uani 1 1 d . . . . . C16 C 0.47599(19) 0.90727(19) 0.10125(13) 0.0270(6) Uani 1 1 d . . . . . H16 H 0.418420 0.905702 0.060373 0.032 Uiso 1 1 calc R U . . . C17 C 0.44835(18) 0.9013(2) 0.16651(13) 0.0254(5) Uani 1 1 d . . . . . H17 H 0.371649 0.895476 0.171608 0.031 Uiso 1 1 calc R U . . . C18 C 0.53478(17) 0.90379(18) 0.22691(12) 0.0202(5) Uani 1 1 d . . . . . C20 C 0.58419(17) 0.89682(18) 0.41981(12) 0.0196(5) Uani 1 1 d . . . . . C21 C 0.67720(18) 0.91643(19) 0.47729(12) 0.0218(5) Uani 1 1 d . . . . . H21 H 0.748734 0.941693 0.469652 0.026 Uiso 1 1 calc R U . . . C22 C 0.66474(19) 0.8991(2) 0.54431(13) 0.0257(5) Uani 1 1 d . . . . . H22 H 0.728309 0.911445 0.582696 0.031 Uiso 1 1 calc R U . . . C23 C 0.55958(19) 0.8635(2) 0.55725(13) 0.0278(6) Uani 1 1 d . . . . . H23 H 0.552573 0.851010 0.603930 0.033 Uiso 1 1 calc R U . . . C24 C 0.46745(19) 0.84669(19) 0.50281(13) 0.0258(5) Uani 1 1 d . . . . . H24 H 0.396002 0.824223 0.511992 0.031 Uiso 1 1 calc R U . . . C25 C 0.47789(18) 0.86257(19) 0.43296(12) 0.0213(5) Uani 1 1 d . . . . . C26 C 0.38572(18) 0.84550(19) 0.37452(13) 0.0243(5) Uani 1 1 d . . . . . H26 H 0.312546 0.824206 0.381540 0.029 Uiso 1 1 calc R U . . . C27 C 0.40233(18) 0.85974(19) 0.30817(13) 0.0244(5) Uani 1 1 d . . . . . H27 H 0.340867 0.847515 0.268365 0.029 Uiso 1 1 calc R U . . . C28 C 0.51112(17) 0.89275(18) 0.29839(12) 0.0192(5) Uani 1 1 d . . . . . C31 C 0.76685(18) 1.17269(19) 0.30624(12) 0.0223(5) Uani 1 1 d . . . . . C32 C 0.7848(2) 1.1966(2) 0.24071(14) 0.0368(6) Uani 1 1 d . . . . . H32 H 0.842666 1.164339 0.217564 0.044 Uiso 1 1 calc R U . . . C33 C 0.7181(3) 1.2677(2) 0.20912(15) 0.0465(8) Uani 1 1 d . . . . . H33 H 0.730507 1.283284 0.164156 0.056 Uiso 1 1 calc R U . . . C34 C 0.6348(2) 1.3156(2) 0.24167(15) 0.0415(7) Uani 1 1 d . . . . . H34 H 0.590303 1.364852 0.219948 0.050 Uiso 1 1 calc R U . . . C35 C 0.6165(2) 1.2915(2) 0.30615(15) 0.0362(7) Uani 1 1 d . . . . . H35 H 0.558748 1.324226 0.329107 0.043 Uiso 1 1 calc R U . . . C36 C 0.68149(19) 1.2201(2) 0.33800(14) 0.0298(6) Uani 1 1 d . . . . . H36 H 0.667127 1.203472 0.382297 0.036 Uiso 1 1 calc R U . . . C41 C 0.86717(16) 0.7568(2) 0.34953(13) 0.0220(5) Uani 1 1 d . . . . . C42 C 0.83533(19) 0.7136(2) 0.40541(14) 0.0297(6) Uani 1 1 d . . . . . H42 H 0.825280 0.762093 0.449147 0.036 Uiso 1 1 calc R U . . . C43 C 0.81804(19) 0.6005(2) 0.39813(16) 0.0381(7) Uani 1 1 d . . . . . H43 H 0.795975 0.572169 0.436787 0.046 Uiso 1 1 calc R U . . . C44 C 0.8326(2) 0.5289(2) 0.33520(17) 0.0392(7) Uani 1 1 d . . . . . H44 H 0.821446 0.451358 0.330468 0.047 Uiso 1 1 calc R U . . . C45 C 0.86367(19) 0.5712(2) 0.27909(15) 0.0366(7) Uani 1 1 d . . . . . H45 H 0.873770 0.522386 0.235497 0.044 Uiso 1 1 calc R U . . . C46 C 0.88017(17) 0.6842(2) 0.28593(13) 0.0261(5) Uani 1 1 d . . . . . H46 H 0.900591 0.712261 0.246715 0.031 Uiso 1 1 calc R U . . . Cu1A Cu 0.22669(2) 0.55834(2) 0.18232(2) 0.02252(9) Uani 1 1 d . . . . . N1A N 0.32273(14) 0.58220(15) 0.28405(10) 0.0198(4) Uani 1 1 d . . . . . N2A N 0.38577(14) 0.58966(15) 0.16010(10) 0.0192(4) Uani 1 1 d . . . . . N3A N 0.09720(14) 0.62806(15) 0.14225(10) 0.0192(4) Uani 1 1 d . . . . . N4A N 0.15438(14) 0.40668(15) 0.15975(10) 0.0199(4) Uani 1 1 d . . . . . C1A C -0.09552(17) 0.62697(19) 0.07467(13) 0.0251(5) Uani 1 1 d . . . . . H1A1 H -0.099496 0.698720 0.106928 0.038 Uiso 1 1 calc R U . . . H1A2 H -0.166447 0.581251 0.068228 0.038 Uiso 1 1 calc R U . . . H1A3 H -0.082740 0.637955 0.027070 0.038 Uiso 1 1 calc R U . . . C2A C 0.00049(17) 0.56974(19) 0.10834(12) 0.0196(5) Uani 1 1 d . . . . . C3A C -0.02094(17) 0.45641(19) 0.10233(12) 0.0208(5) Uani 1 1 d . . . . . H3A H -0.094164 0.426141 0.077387 0.025 Uiso 1 1 calc R U . . . C4A C 0.04852(17) 0.38025(19) 0.12729(12) 0.0197(5) Uani 1 1 d . . . . . C5A C -0.00182(19) 0.2625(2) 0.11408(14) 0.0295(6) Uani 1 1 d . . . . . H5A1 H 0.040760 0.213635 0.083386 0.044 Uiso 1 1 calc R U . . . H5A2 H -0.080406 0.256676 0.089362 0.044 Uiso 1 1 calc R U . . . H5A3 H 0.001535 0.240758 0.160935 0.044 Uiso 1 1 calc R U . . . C10A C 0.28419(18) 0.57747(18) 0.34717(12) 0.0211(5) Uani 1 1 d . . . . . C11A C 0.16698(18) 0.5774(2) 0.34653(13) 0.0254(5) Uani 1 1 d . . . . . H11A H 0.116600 0.574575 0.302065 0.030 Uiso 1 1 calc R U . . . C12A C 0.1263(2) 0.5812(2) 0.40937(14) 0.0312(6) Uani 1 1 d . . . . . H12A H 0.047573 0.581499 0.408478 0.037 Uiso 1 1 calc R U . . . C13A C 0.1995(2) 0.5848(2) 0.47557(14) 0.0333(6) Uani 1 1 d . . . . . H13A H 0.170144 0.589112 0.519253 0.040 Uiso 1 1 calc R U . . . C14A C 0.3121(2) 0.5821(2) 0.47739(14) 0.0326(6) Uani 1 1 d . . . . . H14A H 0.360820 0.582962 0.522205 0.039 Uiso 1 1 calc R U . . . C15A C 0.35709(19) 0.57794(19) 0.41349(13) 0.0249(5) Uani 1 1 d . . . . . C16A C 0.47357(19) 0.5784(2) 0.41181(13) 0.0300(6) Uani 1 1 d . . . . . H16A H 0.525541 0.576368 0.454728 0.036 Uiso 1 1 calc R U . . . C17A C 0.51098(18) 0.5818(2) 0.34911(13) 0.0274(6) Uani 1 1 d . . . . . H17A H 0.589072 0.581415 0.347740 0.033 Uiso 1 1 calc R U . . . C18A C 0.43297(17) 0.58590(19) 0.28546(12) 0.0215(5) Uani 1 1 d . . . . . C20A C 0.41308(17) 0.60680(18) 0.09568(12) 0.0199(5) Uani 1 1 d . . . . . C21A C 0.32585(18) 0.59793(19) 0.03502(13) 0.0233(5) Uani 1 1 d . . . . . H21A H 0.250201 0.580001 0.038948 0.028 Uiso 1 1 calc R U . . . C22A C 0.35042(19) 0.6152(2) -0.02937(13) 0.0277(6) Uani 1 1 d . . . . . H22A H 0.291175 0.610019 -0.069864 0.033 Uiso 1 1 calc R U . . . C23A C 0.46203(19) 0.6405(2) -0.03685(14) 0.0280(6) Uani 1 1 d . . . . . H23A H 0.477659 0.651734 -0.082177 0.034 Uiso 1 1 calc R U . . . C24A C 0.54754(19) 0.64881(19) 0.02102(13) 0.0264(5) Uani 1 1 d . . . . . H24A H 0.622774 0.665594 0.015738 0.032 Uiso 1 1 calc R U . . . C25A C 0.52546(18) 0.63276(19) 0.08863(13) 0.0227(5) Uani 1 1 d . . . . . C26A C 0.60985(18) 0.64111(19) 0.15052(13) 0.0260(5) Uani 1 1 d . . . . . H26A H 0.686252 0.658085 0.147832 0.031 Uiso 1 1 calc R U . . . C27A C 0.58258(17) 0.62506(19) 0.21391(13) 0.0244(5) Uani 1 1 d . . . . . H27A H 0.639569 0.631113 0.255783 0.029 Uiso 1 1 calc R U . . . C28A C 0.46855(17) 0.59917(18) 0.21743(12) 0.0205(5) Uani 1 1 d . . . . . C31A C 0.10892(16) 0.74325(19) 0.14469(12) 0.0211(5) Uani 1 1 d . . . . . C32A C 0.11122(18) 0.8194(2) 0.20964(13) 0.0270(6) Uani 1 1 d . . . . . H32A H 0.104600 0.794298 0.252699 0.032 Uiso 1 1 calc R U . . . C33A C 0.1231(2) 0.9321(2) 0.21249(15) 0.0355(6) Uani 1 1 d . . . . . H33A H 0.123557 0.983351 0.257241 0.043 Uiso 1 1 calc R U . . . C34A C 0.13425(19) 0.9699(2) 0.15078(15) 0.0345(6) Uani 1 1 d . . . . . H34A H 0.142045 1.046919 0.152682 0.041 Uiso 1 1 calc R U . . . C35A C 0.13397(19) 0.8949(2) 0.08639(15) 0.0339(6) Uani 1 1 d . . . . . H35A H 0.142377 0.920482 0.043752 0.041 Uiso 1 1 calc R U . . . C36A C 0.12149(18) 0.7821(2) 0.08310(13) 0.0272(5) Uani 1 1 d . . . . . H36A H 0.121593 0.731199 0.038275 0.033 Uiso 1 1 calc R U . . . C41A C 0.21715(17) 0.32675(18) 0.18729(12) 0.0201(5) Uani 1 1 d . . . . . C42A C 0.29848(18) 0.2780(2) 0.15114(13) 0.0261(5) Uani 1 1 d . . . . . H42A H 0.310268 0.296921 0.106967 0.031 Uiso 1 1 calc R U . . . C43A C 0.36280(19) 0.2020(2) 0.17875(14) 0.0309(6) Uani 1 1 d . . . . . H43A H 0.417303 0.168219 0.153000 0.037 Uiso 1 1 calc R U . . . C44A C 0.3479(2) 0.1754(2) 0.24339(14) 0.0305(6) Uani 1 1 d . . . . . H44A H 0.391434 0.122843 0.262134 0.037 Uiso 1 1 calc R U . . . C45A C 0.2695(2) 0.2253(2) 0.28061(13) 0.0318(6) Uani 1 1 d . . . . . H45A H 0.259895 0.207879 0.325592 0.038 Uiso 1 1 calc R U . . . C46A C 0.2041(2) 0.3011(2) 0.25316(13) 0.0277(5) Uani 1 1 d . . . . . H46A H 0.150396 0.335300 0.279477 0.033 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01538(14) 0.02476(18) 0.02882(17) 0.01175(13) -0.00142(11) -0.00117(11) N1 0.0184(9) 0.0169(11) 0.0211(10) 0.0053(8) 0.0021(7) 0.0010(7) N2 0.0158(8) 0.0188(11) 0.0203(10) 0.0055(8) 0.0021(7) 0.0018(7) N3 0.0180(9) 0.0227(11) 0.0249(11) 0.0095(9) 0.0040(7) 0.0000(8) N4 0.0171(9) 0.0219(11) 0.0218(10) 0.0063(8) 0.0022(7) 0.0009(7) C1 0.0267(13) 0.0283(16) 0.0458(17) 0.0058(13) 0.0012(11) -0.0042(11) C2 0.0206(11) 0.0251(14) 0.0229(12) 0.0033(10) 0.0061(9) -0.0014(9) C3 0.0150(10) 0.0282(15) 0.0271(13) 0.0000(11) 0.0013(9) -0.0025(9) C4 0.0162(10) 0.0278(14) 0.0201(12) 0.0041(10) 0.0036(9) 0.0037(9) C5 0.0194(11) 0.0346(16) 0.0319(14) 0.0070(12) 0.0002(10) 0.0059(10) C10 0.0264(12) 0.0162(13) 0.0218(12) 0.0048(10) 0.0041(9) 0.0012(9) C11 0.0289(12) 0.0265(15) 0.0280(14) 0.0069(11) 0.0067(10) 0.0018(10) C12 0.0336(13) 0.0311(16) 0.0347(15) 0.0091(12) 0.0128(11) -0.0010(11) C13 0.0510(16) 0.0288(16) 0.0249(14) 0.0061(12) 0.0129(12) -0.0038(12) C14 0.0435(15) 0.0251(15) 0.0218(13) 0.0079(11) 0.0013(11) -0.0006(11) C15 0.0334(13) 0.0192(14) 0.0225(13) 0.0072(10) 0.0021(10) 0.0025(10) C16 0.0296(12) 0.0246(14) 0.0233(13) 0.0054(11) -0.0055(10) 0.0029(10) C17 0.0192(11) 0.0258(14) 0.0293(14) 0.0049(11) -0.0008(9) 0.0050(9) C18 0.0203(11) 0.0182(13) 0.0203(12) 0.0033(10) -0.0004(9) 0.0025(9) C20 0.0192(10) 0.0182(13) 0.0221(12) 0.0041(10) 0.0057(9) 0.0035(9) C21 0.0184(10) 0.0240(14) 0.0237(12) 0.0065(10) 0.0040(9) 0.0030(9) C22 0.0246(12) 0.0299(15) 0.0232(13) 0.0074(11) 0.0028(9) 0.0059(10) C23 0.0347(13) 0.0290(15) 0.0235(13) 0.0093(11) 0.0108(10) 0.0047(11) C24 0.0256(12) 0.0235(14) 0.0308(14) 0.0062(11) 0.0124(10) 0.0007(10) C25 0.0215(11) 0.0187(13) 0.0240(13) 0.0028(10) 0.0074(9) 0.0016(9) C26 0.0170(10) 0.0242(14) 0.0308(14) 0.0029(11) 0.0064(9) 0.0000(9) C27 0.0171(10) 0.0252(14) 0.0280(13) 0.0020(11) 0.0008(9) 0.0017(9) C28 0.0167(10) 0.0153(12) 0.0243(12) 0.0022(10) 0.0018(9) 0.0033(8) C31 0.0227(11) 0.0197(13) 0.0231(12) 0.0062(10) 0.0002(9) -0.0056(9) C32 0.0541(17) 0.0323(17) 0.0291(15) 0.0127(12) 0.0129(12) 0.0077(13) C33 0.081(2) 0.0342(18) 0.0271(15) 0.0185(13) 0.0035(15) 0.0052(16) C34 0.0472(17) 0.0264(17) 0.0443(18) 0.0117(13) -0.0148(13) 0.0019(13) C35 0.0264(13) 0.0312(16) 0.0495(18) 0.0100(13) 0.0010(12) 0.0022(11) C36 0.0282(12) 0.0311(16) 0.0327(14) 0.0133(12) 0.0053(10) 0.0009(11) C41 0.0113(10) 0.0253(14) 0.0300(13) 0.0091(11) 0.0015(9) 0.0028(9) C42 0.0264(12) 0.0330(16) 0.0378(15) 0.0181(12) 0.0126(11) 0.0127(11) C43 0.0241(13) 0.0402(18) 0.060(2) 0.0292(15) 0.0122(12) 0.0092(11) C44 0.0237(12) 0.0232(16) 0.067(2) 0.0141(15) -0.0054(13) 0.0007(11) C45 0.0255(13) 0.0337(17) 0.0419(17) -0.0015(13) -0.0070(11) 0.0048(11) C46 0.0175(11) 0.0287(15) 0.0287(14) 0.0041(11) -0.0020(9) 0.0005(10) Cu1A 0.01461(14) 0.02271(18) 0.02979(17) 0.01016(13) -0.00193(11) -0.00089(11) N1A 0.0176(9) 0.0191(11) 0.0224(10) 0.0060(8) 0.0016(7) 0.0018(7) N2A 0.0164(9) 0.0168(11) 0.0239(10) 0.0041(8) 0.0025(7) 0.0013(7) N3A 0.0172(9) 0.0198(11) 0.0201(10) 0.0054(8) 0.0013(7) 0.0020(7) N4A 0.0165(9) 0.0214(11) 0.0228(10) 0.0076(8) 0.0028(7) 0.0008(7) C1A 0.0175(11) 0.0263(14) 0.0307(14) 0.0076(11) 0.0003(9) 0.0033(9) C2A 0.0156(10) 0.0276(14) 0.0167(11) 0.0064(10) 0.0034(8) 0.0034(9) C3A 0.0156(10) 0.0240(14) 0.0216(12) 0.0050(10) 0.0012(8) -0.0028(9) C4A 0.0198(10) 0.0210(13) 0.0183(12) 0.0054(10) 0.0039(9) -0.0024(9) C5A 0.0253(12) 0.0255(15) 0.0366(15) 0.0121(12) -0.0024(10) -0.0046(10) C10A 0.0231(11) 0.0155(13) 0.0245(13) 0.0037(10) 0.0037(9) 0.0035(9) C11A 0.0222(11) 0.0268(14) 0.0283(13) 0.0095(11) 0.0035(10) 0.0026(10) C12A 0.0288(13) 0.0332(16) 0.0379(15) 0.0157(12) 0.0120(11) 0.0082(11) C13A 0.0396(14) 0.0361(17) 0.0322(15) 0.0159(12) 0.0153(11) 0.0132(12) C14A 0.0377(14) 0.0364(17) 0.0276(14) 0.0139(12) 0.0060(11) 0.0117(12) C15A 0.0268(12) 0.0214(14) 0.0270(13) 0.0082(11) 0.0017(10) 0.0057(10) C16A 0.0242(12) 0.0351(16) 0.0296(14) 0.0096(12) -0.0028(10) 0.0092(10) C17A 0.0184(11) 0.0327(16) 0.0297(14) 0.0072(11) -0.0014(10) 0.0065(10) C18A 0.0183(10) 0.0169(13) 0.0271(13) 0.0028(10) -0.0003(9) 0.0028(9) C20A 0.0202(11) 0.0146(12) 0.0256(13) 0.0048(10) 0.0057(9) 0.0008(9) C21A 0.0175(10) 0.0246(14) 0.0283(13) 0.0076(11) 0.0037(9) 0.0013(9) C22A 0.0258(12) 0.0288(15) 0.0297(14) 0.0097(11) 0.0042(10) 0.0018(10) C23A 0.0317(13) 0.0253(15) 0.0302(14) 0.0096(11) 0.0104(10) 0.0021(10) C24A 0.0227(11) 0.0229(14) 0.0360(15) 0.0072(11) 0.0115(10) 0.0000(10) C25A 0.0197(11) 0.0173(13) 0.0312(14) 0.0037(10) 0.0067(9) 0.0014(9) C26A 0.0149(10) 0.0241(14) 0.0382(15) 0.0042(11) 0.0067(10) 0.0003(9) C27A 0.0149(10) 0.0254(14) 0.0295(13) 0.0021(11) 0.0005(9) 0.0000(9) C28A 0.0166(10) 0.0165(13) 0.0273(13) 0.0034(10) 0.0022(9) 0.0034(9) C31A 0.0121(10) 0.0225(14) 0.0286(13) 0.0080(11) 0.0004(9) 0.0021(9) C32A 0.0216(11) 0.0284(15) 0.0285(14) 0.0056(11) -0.0013(10) 0.0003(10) C33A 0.0313(13) 0.0262(16) 0.0402(16) -0.0027(12) -0.0053(11) 0.0025(11) C34A 0.0284(13) 0.0201(15) 0.0517(18) 0.0102(13) -0.0041(12) -0.0004(10) C35A 0.0292(13) 0.0311(16) 0.0457(17) 0.0203(13) 0.0047(11) 0.0015(11) C36A 0.0270(12) 0.0274(15) 0.0283(14) 0.0071(11) 0.0065(10) 0.0026(10) C41A 0.0196(10) 0.0167(13) 0.0231(12) 0.0062(10) 0.0000(9) -0.0009(9) C42A 0.0258(12) 0.0279(15) 0.0248(13) 0.0070(11) 0.0039(10) 0.0017(10) C43A 0.0262(12) 0.0287(15) 0.0345(15) 0.0025(12) 0.0015(10) 0.0051(10) C44A 0.0328(13) 0.0226(14) 0.0317(14) 0.0065(11) -0.0078(11) 0.0048(10) C45A 0.0454(15) 0.0271(16) 0.0240(13) 0.0120(11) 0.0011(11) 0.0043(12) C46A 0.0338(13) 0.0254(15) 0.0256(13) 0.0075(11) 0.0067(10) 0.0051(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N4 Cu1 N3 97.38(8) . . ? N4 Cu1 N1 132.23(8) . . ? N3 Cu1 N1 109.22(7) . . ? N4 Cu1 N2 117.72(8) . . ? N3 Cu1 N2 123.65(7) . . ? N1 Cu1 N2 79.30(8) . . ? C18 N1 C10 118.57(18) . . ? C18 N1 Cu1 115.14(14) . . ? C10 N1 Cu1 125.40(14) . . ? C28 N2 C20 118.00(18) . . ? C28 N2 Cu1 113.61(15) . . ? C20 N2 Cu1 128.02(14) . . ? C2 N3 C31 120.26(19) . . ? C2 N3 Cu1 122.75(16) . . ? C31 N3 Cu1 116.73(14) . . ? C4 N4 C41 119.55(18) . . ? C4 N4 Cu1 122.20(16) . . ? C41 N4 Cu1 118.19(13) . . ? N3 C2 C3 123.2(2) . . ? N3 C2 C1 120.2(2) . . ? C3 C2 C1 116.51(19) . . ? C4 C3 C2 129.7(2) . . ? N4 C4 C3 124.3(2) . . ? N4 C4 C5 119.3(2) . . ? C3 C4 C5 116.48(19) . . ? N1 C10 C11 118.4(2) . . ? N1 C10 C15 121.8(2) . . ? C11 C10 C15 119.7(2) . . ? C12 C11 C10 120.1(2) . . ? C11 C12 C13 120.5(2) . . ? C14 C13 C12 120.2(2) . . ? C13 C14 C15 120.9(2) . . ? C16 C15 C14 123.7(2) . . ? C16 C15 C10 117.7(2) . . ? C14 C15 C10 118.6(2) . . ? C17 C16 C15 120.2(2) . . ? C16 C17 C18 119.3(2) . . ? N1 C18 C17 122.4(2) . . ? N1 C18 C28 115.25(18) . . ? C17 C18 C28 122.3(2) . . ? N2 C20 C21 118.61(19) . . ? N2 C20 C25 122.30(19) . . ? C21 C20 C25 119.1(2) . . ? C22 C21 C20 120.0(2) . . ? C21 C22 C23 121.1(2) . . ? C24 C23 C22 120.0(2) . . ? C23 C24 C25 120.2(2) . . ? C24 C25 C26 122.6(2) . . ? C24 C25 C20 119.6(2) . . ? C26 C25 C20 117.8(2) . . ? C27 C26 C25 119.5(2) . . ? C26 C27 C28 119.9(2) . . ? N2 C28 C27 122.5(2) . . ? N2 C28 C18 115.36(19) . . ? C27 C28 C18 122.10(19) . . ? C36 C31 C32 118.5(2) . . ? C36 C31 N3 120.1(2) . . ? C32 C31 N3 121.1(2) . . ? C33 C32 C31 119.9(3) . . ? C34 C33 C32 121.1(3) . . ? C33 C34 C35 119.1(2) . . ? C34 C35 C36 120.6(3) . . ? C31 C36 C35 120.8(2) . . ? C42 C41 C46 118.5(2) . . ? C42 C41 N4 120.8(2) . . ? C46 C41 N4 120.6(2) . . ? C43 C42 C41 120.7(3) . . ? C44 C43 C42 120.5(3) . . ? C43 C44 C45 119.2(3) . . ? C44 C45 C46 120.5(3) . . ? C45 C46 C41 120.6(2) . . ? N3A Cu1A N4A 97.44(8) . . ? N3A Cu1A N1A 133.08(7) . . ? N4A Cu1A N1A 106.26(7) . . ? N3A Cu1A N2A 121.88(8) . . ? N4A Cu1A N2A 120.79(7) . . ? N1A Cu1A N2A 78.98(7) . . ? C18A N1A C10A 118.35(18) . . ? C18A N1A Cu1A 114.79(15) . . ? C10A N1A Cu1A 126.04(14) . . ? C28A N2A C20A 118.24(18) . . ? C28A N2A Cu1A 113.95(15) . . ? C20A N2A Cu1A 127.72(14) . . ? C2A N3A C31A 118.96(18) . . ? C2A N3A Cu1A 121.91(16) . . ? C31A N3A Cu1A 118.98(13) . . ? C4A N4A C41A 119.72(19) . . ? C4A N4A Cu1A 122.95(15) . . ? C41A N4A Cu1A 116.96(14) . . ? N3A C2A C3A 124.20(19) . . ? N3A C2A C1A 119.9(2) . . ? C3A C2A C1A 115.93(18) . . ? C2A C3A C4A 130.22(19) . . ? N4A C4A C3A 123.1(2) . . ? N4A C4A C5A 119.7(2) . . ? C3A C4A C5A 117.22(19) . . ? N1A C10A C15A 122.6(2) . . ? N1A C10A C11A 118.51(19) . . ? C15A C10A C11A 118.8(2) . . ? C12A C11A C10A 120.2(2) . . ? C11A C12A C13A 120.7(2) . . ? C14A C13A C12A 120.3(2) . . ? C13A C14A C15A 120.5(2) . . ? C14A C15A C10A 119.4(2) . . ? C14A C15A C16A 123.6(2) . . ? C10A C15A C16A 117.0(2) . . ? C17A C16A C15A 120.1(2) . . ? C16A C17A C18A 119.6(2) . . ? N1A C18A C17A 122.3(2) . . ? N1A C18A C28A 115.28(19) . . ? C17A C18A C28A 122.4(2) . . ? N2A C20A C21A 118.56(19) . . ? N2A C20A C25A 122.14(19) . . ? C21A C20A C25A 119.3(2) . . ? C22A C21A C20A 119.8(2) . . ? C21A C22A C23A 121.2(2) . . ? C24A C23A C22A 119.9(2) . . ? C23A C24A C25A 120.6(2) . . ? C26A C25A C24A 123.3(2) . . ? C26A C25A C20A 117.5(2) . . ? C24A C25A C20A 119.2(2) . . ? C27A C26A C25A 120.2(2) . . ? C26A C27A C28A 119.6(2) . . ? N2A C28A C27A 122.3(2) . . ? N2A C28A C18A 115.43(19) . . ? C27A C28A C18A 122.18(19) . . ? C36A C31A C32A 118.4(2) . . ? C36A C31A N3A 121.1(2) . . ? C32A C31A N3A 120.4(2) . . ? C31A C32A C33A 120.7(2) . . ? C34A C33A C32A 120.4(3) . . ? C35A C34A C33A 119.3(3) . . ? C34A C35A C36A 120.6(3) . . ? C31A C36A C35A 120.5(2) . . ? C42A C41A C46A 118.7(2) . . ? C42A C41A N4A 120.2(2) . . ? C46A C41A N4A 120.9(2) . . ? C41A C42A C43A 120.7(2) . . ? C44A C43A C42A 120.2(2) . . ? C45A C44A C43A 119.5(2) . . ? C44A C45A C46A 120.7(2) . . ? C41A C46A C45A 120.1(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 N4 1.9457(18) . ? Cu1 N3 1.964(2) . ? Cu1 N1 2.0215(18) . ? Cu1 N2 2.0811(19) . ? N1 C18 1.334(3) . ? N1 C10 1.375(3) . ? N2 C28 1.333(3) . ? N2 C20 1.376(3) . ? N3 C2 1.324(3) . ? N3 C31 1.416(3) . ? N4 C4 1.328(3) . ? N4 C41 1.422(3) . ? C1 C2 1.515(3) . ? C2 C3 1.405(3) . ? C3 C4 1.398(3) . ? C4 C5 1.515(3) . ? C10 C11 1.407(3) . ? C10 C15 1.413(3) . ? C11 C12 1.369(3) . ? C12 C13 1.405(3) . ? C13 C14 1.362(3) . ? C14 C15 1.411(3) . ? C15 C16 1.409(3) . ? C16 C17 1.355(3) . ? C17 C18 1.413(3) . ? C18 C28 1.469(3) . ? C20 C21 1.404(3) . ? C20 C25 1.412(3) . ? C21 C22 1.369(3) . ? C22 C23 1.403(3) . ? C23 C24 1.364(3) . ? C24 C25 1.410(3) . ? C25 C26 1.410(3) . ? C26 C27 1.357(3) . ? C27 C28 1.412(3) . ? C31 C36 1.379(3) . ? C31 C32 1.390(3) . ? C32 C33 1.390(4) . ? C33 C34 1.368(4) . ? C34 C35 1.373(4) . ? C35 C36 1.383(3) . ? C41 C42 1.387(3) . ? C41 C46 1.388(3) . ? C42 C43 1.385(4) . ? C43 C44 1.378(4) . ? C44 C45 1.381(4) . ? C45 C46 1.385(3) . ? Cu1A N3A 1.9513(18) . ? Cu1A N4A 1.968(2) . ? Cu1A N1A 2.0400(19) . ? Cu1A N2A 2.0739(19) . ? N1A C18A 1.328(3) . ? N1A C10A 1.371(3) . ? N2A C28A 1.333(3) . ? N2A C20A 1.377(3) . ? N3A C2A 1.333(3) . ? N3A C31A 1.423(3) . ? N4A C4A 1.318(3) . ? N4A C41A 1.415(3) . ? C1A C2A 1.515(3) . ? C2A C3A 1.397(3) . ? C3A C4A 1.402(3) . ? C4A C5A 1.511(3) . ? C10A C15A 1.413(3) . ? C10A C11A 1.417(3) . ? C11A C12A 1.361(3) . ? C12A C13A 1.405(3) . ? C13A C14A 1.361(3) . ? C14A C15A 1.406(3) . ? C15A C16A 1.415(3) . ? C16A C17A 1.353(3) . ? C17A C18A 1.418(3) . ? C18A C28A 1.469(3) . ? C20A C21A 1.410(3) . ? C20A C25A 1.416(3) . ? C21A C22A 1.365(3) . ? C22A C23A 1.408(3) . ? C23A C24A 1.362(3) . ? C24A C25A 1.409(3) . ? C25A C26A 1.406(3) . ? C26A C27A 1.354(3) . ? C27A C28A 1.417(3) . ? C31A C36A 1.386(3) . ? C31A C32A 1.386(3) . ? C32A C33A 1.391(3) . ? C33A C34A 1.377(4) . ? C34A C35A 1.375(4) . ? C35A C36A 1.391(3) . ? C41A C42A 1.387(3) . ? C41A C46A 1.389(3) . ? C42A C43A 1.387(3) . ? C43A C44A 1.377(4) . ? C44A C45A 1.374(4) . ? C45A C46A 1.390(3) . ?