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Information card for entry 7131671
Preview
Coordinates | 7131671.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C66 H39 B F20 Pb |
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Calculated formula | C66 H39 B F20 Pb |
SMILES | [Pb](c1c2C3(c4ccccc4c4c3cccc4)CC(C)(c2cc2C(C)(C)CC3(c4c(c5c3cccc5)cccc4)c12)C)(C)C.Fc1c(c(F)c(F)c(F)c1F)[B-](c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)c1c(F)c(F)c(F)c(F)c1F |
Title of publication | Aryldimethylelement cations of the heavier group 14 elements. An essentially three-coordinate plumbylium ion. |
Authors of publication | Janssen, Marvin; Mebs, Stefan; Beckmann, Jens |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2023 |
Journal volume | 59 |
Journal issue | 47 |
Pages of publication | 7267 - 7270 |
a | 10.2803 ± 0.001 Å |
b | 14.774 ± 0.002 Å |
c | 18.3384 ± 0.0019 Å |
α | 86.552 ± 0.007° |
β | 78.805 ± 0.004° |
γ | 85.707 ± 0.005° |
Cell volume | 2721.6 ± 0.5 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0333 |
Residual factor for significantly intense reflections | 0.0256 |
Weighted residual factors for significantly intense reflections | 0.0508 |
Weighted residual factors for all reflections included in the refinement | 0.0526 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
284858 (current) | 2023-07-05 | cif/ Updating files of 7131666, 7131667, 7131668, 7131669, 7131670, 7131671 Original log message: Adding full bibliography for 7131666--7131671.cif. |
7131671.cif |
283874 | 2023-05-19 | cif/ Adding structures of 7131666, 7131667, 7131668, 7131669, 7131670, 7131671 via cif-deposit CGI script. |
7131671.cif |
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Users of the data should acknowledge the original authors of the
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