Crystallography Open Database

Information card for entry 7132738

Preview

Coordinates	7132738.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H49 K O6 P2 S
Calculated formula	C43 H49 K O6 P2 S
Title of publication	From a mercury(II) bis(yldiide) complex to actinide yldiides.
Authors of publication	Jörges, Mike; Gremillion, Alexander J.; Knyszek, Daniel; Kelley, Steven P.; Walensky, Justin R.; Gessner, Viktoria H.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	23
Pages of publication	3190 - 3193
a	9.4692 ± 0.0001 Å
b	10.8945 ± 0.0001 Å
c	21.4146 ± 0.0003 Å
α	77.036 ± 0.001°
β	83.374 ± 0.001°
γ	73.667 ± 0.001°
Cell volume	2062.75 ± 0.04 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0864
Residual factor for significantly intense reflections	0.0753
Weighted residual factors for significantly intense reflections	0.1355
Weighted residual factors for all reflections included in the refinement	0.1403
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
290825 (current)	2024-04-05	cif/ Updating files of 7132735, 7132736, 7132737, 7132738, 7132739 Original log message: Adding full bibliography for 7132735--7132739.cif.	7132738.cif
289883	2024-02-21	cif/ Adding structures of 7132735, 7132736, 7132737, 7132738, 7132739 via cif-deposit CGI script.	7132738.cif