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Information card for entry 7132944
Preview
| Coordinates | 7132944.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C100 H86 N2 O32 P4 W10 |
|---|---|
| Calculated formula | C100 H86 N2 O32 P4 W10 |
| Title of publication | Photocatalytic aerobic α-oxygenation of amides to imides using a highly durable decatungstate tetraphenylphosphonium salt. |
| Authors of publication | Gu, Chen; Yatabe, Takafumi; Yamaguchi, Kazuya; Suzuki, Kosuke |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 37 |
| Pages of publication | 4906 - 4909 |
| a | 13.5793 ± 0.0002 Å |
| b | 15.3135 ± 0.0003 Å |
| c | 15.4699 ± 0.0002 Å |
| α | 117.216 ± 0.0016° |
| β | 113.848 ± 0.0016° |
| γ | 92.658 ± 0.0014° |
| Cell volume | 2508.49 ± 0.1 Å3 |
| Cell temperature | 93.15 K |
| Ambient diffraction temperature | 93.15 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0514 |
| Residual factor for significantly intense reflections | 0.036 |
| Weighted residual factors for significantly intense reflections | 0.0806 |
| Weighted residual factors for all reflections included in the refinement | 0.0857 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.025 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 291509 (current) | 2024-05-05 | cif/ Updating files of 7132944 Original log message: Adding full bibliography for 7132944.cif. |
7132944.cif |
| 291162 | 2024-04-11 | cif/ Adding structures of 7132944 via cif-deposit CGI script. |
7132944.cif |
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Users of the data should acknowledge the original authors of the
structural data.