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Information card for entry 7133288
Preview
| Coordinates | 7133288.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C25 H27 N O5 S |
|---|---|
| Calculated formula | C25 H27 N O5 S |
| Title of publication | Pd-catalyzed 5-<i>exo-dig</i> cyclization/etherification cascade of <i>N</i>-propargyl arylamines for the synthesis of polysubstituted furans. |
| Authors of publication | Li, Meng-Ru; Zheng, Meng-Yao; Wang, Dong-Chao; Guo, Hai-Ming |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 60 |
| Pages of publication | 7721 - 7724 |
| a | 10.6593 ± 0.0004 Å |
| b | 11.0723 ± 0.0005 Å |
| c | 11.354 ± 0.0005 Å |
| α | 90.428 ± 0.004° |
| β | 111.448 ± 0.004° |
| γ | 105.959 ± 0.004° |
| Cell volume | 1190.4 ± 0.1 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0541 |
| Residual factor for significantly intense reflections | 0.0478 |
| Weighted residual factors for significantly intense reflections | 0.1297 |
| Weighted residual factors for all reflections included in the refinement | 0.1349 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 293702 (current) | 2024-08-05 | cif/ Updating files of 7133288 Original log message: Adding full bibliography for 7133288.cif. |
7133288.cif |
| 293334 | 2024-07-10 | cif/ Adding structures of 7133288 via cif-deposit CGI script. |
7133288.cif |
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Users of the data should acknowledge the original authors of the
structural data.