Crystallography Open Database

Information card for entry 7134358

Preview

Coordinates	7134358.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H46 Cl2 F6 Ge O8 P2 S2
Calculated formula	C39 H46 Cl2 F6 Ge O8 P2 S2
Title of publication	An intramolecular phosphine-oxide stabilized germanium(iv) di-cation with enhanced Lewis acidity and catalytic applications
Authors of publication	Kumari, Akanksha; Peddi, Balakrishna; Yildiz, Cem. B.; Majumdar, Moumita
Journal of publication	Chemical Communications
Year of publication	2025
Journal volume	61
Journal issue	35
Pages of publication	6506 - 6509
a	11.237 ± 0.004 Å
b	13.727 ± 0.005 Å
c	15.396 ± 0.005 Å
α	86.231 ± 0.008°
β	72.039 ± 0.008°
γ	80.057 ± 0.008°
Cell volume	2225 ± 1.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0672
Residual factor for significantly intense reflections	0.0484
Weighted residual factors for significantly intense reflections	0.1206
Weighted residual factors for all reflections included in the refinement	0.1312
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
300508 (current)	2025-07-06	cif/ Updating files of 7134358, 7134359, 7134360, 7134361 Original log message: Adding full bibliography for 7134358--7134361.cif.	7134358.cif
298622	2025-03-28	cif/ Adding structures of 7134358, 7134359, 7134360, 7134361 via cif-deposit CGI script.	7134358.cif