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Information card for entry 7150652
Preview
Coordinates | 7150652.cif |
---|---|
Original paper (by DOI) | HTML |
External links | ChemSpider |
Formula | C15 H23 N O5 |
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Calculated formula | C15 H23 N O5 |
SMILES | O1C(OCC([C@@H]1C(=O)NC=C/C=C/C(=O)OC)(C)C)(C)C |
Title of publication | Fast and efficient one step synthesis of dienamides |
Authors of publication | Mathieson, Jennifer E.; Crawford, James J.; Schmidtmann, Marc; Marquez, Rodolfo |
Journal of publication | Organic & Biomolecular Chemistry |
Year of publication | 2009 |
Journal volume | 7 |
Journal issue | 10 |
Pages of publication | 2170 - 2175 |
a | 6.1541 ± 0.0012 Å |
b | 7.9492 ± 0.0016 Å |
c | 8.6988 ± 0.0017 Å |
α | 71.93 ± 0.03° |
β | 70.89 ± 0.03° |
γ | 83 ± 0.03° |
Cell volume | 382.17 ± 0.16 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 4 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0362 |
Residual factor for significantly intense reflections | 0.0345 |
Weighted residual factors for significantly intense reflections | 0.0933 |
Weighted residual factors for all reflections included in the refinement | 0.095 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.098 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
202017 (current) | 2017-10-14 | cif/ Marking COD entries in range 7 that are known to be related to ChemSpider entries using the _cod_related_entry data loop. |
7150652.cif |
180292 | 2016-03-26 | cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/06. |
7150652.cif |
120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7150652.cif |
35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7150652.cif |
1167 | 2010-05-13 | cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19. |
7150652.cif |
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Users of the data should acknowledge the original authors of the
structural data.