#------------------------------------------------------------------------------
#$Date: 2016-03-26 15:12:35 +0200 (Sat, 26 Mar 2016) $
#$Revision: 180293 $
#$URL: svn://www.crystallography.net/cod/cif/7/15/07/7150786.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7150786
loop_
_publ_author_name
'Maag, Roman'
'Northrop, Brian H.'
'Butterfield, Anna'
'Linden, Anthony'
'Zerbe, Oliver'
'Lee, Young Min'
'Chi, Ki-Whan'
'Stang, Peter J.'
'Siegel, Jay S.'
_publ_section_title
;
 Synthesis and X-ray structural analysis of platinum and
 ethynyl-platinum corannulenes: supramolecular tectons
;
_journal_issue                   23
_journal_name_full               'Organic & Biomolecular Chemistry'
_journal_page_first              4881
_journal_page_last               4885
_journal_paper_doi               10.1039/b916020e
_journal_volume                  7
_journal_year                    2009
_chemical_formula_moiety         'C80 H155 Cl5 P10 Pt5'
_chemical_formula_sum            'C80 H155 Cl5 P10 Pt5'
_chemical_formula_weight         2579.11
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             09-05-28
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 110.8408(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   38.9473(4)
_cell_length_b                   14.4159(1)
_cell_length_c                   39.1396(4)
_cell_measurement_reflns_used    587979
_cell_measurement_temperature    160(1)
_cell_measurement_theta_max      25.0
_cell_measurement_theta_min      2.0
_cell_volume                     20537.5(3)
_computing_cell_refinement       'DENZO-SMN (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Nonius, 2000)'
_computing_data_reduction
'DENZO-SMN and SCALEPACK (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  'SHELXL97 and PLATON (Spek, 2003)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      160(1)
_diffrn_detector                 '65 mm CCD camera on \k goniostat'
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type
'Nonius KappaCCD area-detector diffractometer'
_diffrn_measurement_method       'ω scans with κ offsets'
_diffrn_radiation_monochromator  'horizontally mounted graphite crystal'
_diffrn_radiation_source         'Nonius FR590 sealed tube generator'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1044
_diffrn_reflns_av_sigmaI/netI    0.0643
_diffrn_reflns_limit_h_max       46
_diffrn_reflns_limit_h_min       -46
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       46
_diffrn_reflns_limit_l_min       -46
_diffrn_reflns_number            238902
_diffrn_reflns_theta_full        25.02
_diffrn_reflns_theta_max         25.02
_diffrn_reflns_theta_min         2.11
_diffrn_standards_decay_%        0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    7.079
_exptl_absorpt_correction_T_max  0.448
_exptl_absorpt_correction_T_min  0.195
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Blessing, 1995)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.668
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             10080
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.13
_refine_diff_density_max         5.469
_refine_diff_density_min         -3.999
_refine_diff_density_rms         0.212
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.138
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2361
_refine_ls_number_reflns         35799
_refine_ls_number_restraints     6428
_refine_ls_restrained_S_all      1.049
_refine_ls_R_factor_all          0.0986
_refine_ls_R_factor_gt           0.0658
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0187P)²+390.6599P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1225
_refine_ls_wR_factor_ref         0.1334
_reflns_number_gt                26731
_reflns_number_total             35803
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            b916020e.txt
_cod_data_source_block           1
_cod_database_code               7150786
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.274222(13) -0.12223(4) 0.633002(14) 0.04663(13) Uani 1 1 d . A .
Pt2 Pt 0.267106(13) 0.22308(4) 0.539961(13) 0.04272(13) Uani 1 1 d . A .
Pt3 Pt 0.120416(13) 0.42235(3) 0.504693(12) 0.04011(12) Uani 1 1 d . A .
Pt4 Pt 0.051773(12) 0.25873(3) 0.612721(13) 0.03684(11) Uani 1 1 d . A .
Pt5 Pt 0.144783(13) -0.07228(3) 0.691759(12) 0.03578(11) Uani 1 1 d . A .
Cl1 Cl 0.32094(11) -0.2359(3) 0.66266(13) 0.0850(14) Uani 1 1 d . . .
Cl2 Cl 0.32596(9) 0.2599(3) 0.53640(10) 0.0675(11) Uani 1 1 d . . .
Cl3 Cl 0.15834(8) 0.4966(2) 0.55918(8) 0.0436(7) Uani 1 1 d . . .
Cl4 Cl 0.00304(9) 0.3492(3) 0.62068(11) 0.0622(10) Uani 1 1 d . . .
Cl5 Cl 0.12827(10) -0.1433(2) 0.73941(9) 0.0576(9) Uani 1 1 d . . .
P1 P 0.24247(10) -0.2314(2) 0.59000(11) 0.0521(9) Uani 1 1 d . . .
P2 P 0.30921(10) -0.0135(3) 0.67273(10) 0.0603(10) Uani 1 1 d D . .
P3 P 0.25363(13) 0.1366(4) 0.48812(13) 0.0900(17) Uani 1 1 d D . .
P4 P 0.27881(9) 0.3316(3) 0.58591(9) 0.0456(8) Uani 1 1 d . . .
P5 P 0.08092(11) 0.3470(3) 0.45774(10) 0.0614(11) Uani 1 1 d D . .
P6 P 0.12034(8) 0.5661(2) 0.47659(8) 0.0349(7) Uani 1 1 d . . .
P7 P 0.01232(9) 0.1367(2) 0.58909(10) 0.0500(9) Uani 1 1 d D . .
P8 P 0.09341(9) 0.3729(2) 0.64048(10) 0.0477(9) Uani 1 1 d D . .
P9 P 0.17183(11) 0.0485(3) 0.72950(10) 0.0534(9) Uani 1 1 d . . .
P10 P 0.11862(10) -0.1949(3) 0.65429(11) 0.0577(10) Uani 1 1 d D . .
C1 C 0.1739(3) 0.0298(8) 0.5881(3) 0.043(3) Uani 1 1 d . . .
C2 C 0.1784(3) 0.0909(8) 0.5609(3) 0.035(3) Uani 1 1 d . A .
C3 C 0.1497(3) 0.1532(8) 0.5511(3) 0.037(3) Uani 1 1 d . . .
C4 C 0.1272(3) 0.1337(9) 0.5704(3) 0.042(3) Uani 1 1 d . A .
C5 C 0.1412(3) 0.0612(9) 0.5928(3) 0.041(3) Uani 1 1 d . . .
C6 C 0.2015(4) -0.0215(9) 0.6137(3) 0.050(3) Uani 1 1 d . A .
C7 C 0.2345(3) -0.0230(10) 0.6069(4) 0.053(4) Uani 1 1 d . . .
C8 C 0.2421(3) 0.0421(8) 0.5818(3) 0.039(3) Uani 1 1 d . A .
H8 H 0.2656 0.0431 0.5796 0.047 Uiso 1 1 calc R . .
C9 C 0.2137(3) 0.1050(9) 0.5602(3) 0.043(3) Uani 1 1 d . . .
C10 C 0.2175(4) 0.1902(9) 0.5428(3) 0.054(4) Uani 1 1 d . A .
C11 C 0.1864(3) 0.2522(8) 0.5294(3) 0.038(3) Uani 1 1 d . . .
H11 H 0.1885 0.3044 0.5155 0.046 Uiso 1 1 calc R A .
C12 C 0.1536(3) 0.2408(9) 0.5356(3) 0.047(3) Uani 1 1 d . A .
C13 C 0.1248(3) 0.3018(9) 0.5359(3) 0.048(3) Uani 1 1 d . . .
C14 C 0.1011(3) 0.2821(8) 0.5556(3) 0.035(3) Uani 1 1 d . A .
H14 H 0.0826 0.3261 0.5546 0.043 Uiso 1 1 calc R . .
C15 C 0.1035(3) 0.2019(9) 0.5765(3) 0.044(3) Uani 1 1 d . . .
C16 C 0.0910(3) 0.1806(9) 0.6058(4) 0.051(3) Uani 1 1 d . A .
C17 C 0.1073(3) 0.1011(9) 0.6300(3) 0.047(3) Uani 1 1 d . . .
H17 H 0.0989 0.0883 0.6495 0.056 Uiso 1 1 calc R A .
C18 C 0.1350(3) 0.0430(9) 0.6258(3) 0.045(3) Uani 1 1 d . A .
C19 C 0.1587(3) -0.0214(9) 0.6500(3) 0.044(3) Uani 1 1 d . . .
C20 C 0.1919(4) -0.0528(9) 0.6442(3) 0.047(3) Uani 1 1 d . A .
H20 H 0.2077 -0.0952 0.6612 0.057 Uiso 1 1 calc R . .
C21 C 0.2587(5) -0.2370(13) 0.5520(5) 0.086(5) Uani 1 1 d . . .
H21A H 0.2451 -0.2869 0.5352 0.103 Uiso 1 1 calc R . .
H21B H 0.2526 -0.1778 0.5384 0.103 Uiso 1 1 calc R . .
C22 C 0.2991(5) -0.2545(13) 0.5621(5) 0.090(6) Uani 1 1 d . . .
H22A H 0.3130 -0.2045 0.5780 0.135 Uiso 1 1 calc R . .
H22B H 0.3052 -0.2566 0.5399 0.135 Uiso 1 1 calc R . .
H22C H 0.3055 -0.3139 0.5750 0.135 Uiso 1 1 calc R . .
C23 C 0.2474(5) -0.3491(10) 0.6064(5) 0.075(5) Uani 1 1 d . . .
H23A H 0.2349 -0.3911 0.5857 0.090 Uiso 1 1 calc R . .
H23B H 0.2738 -0.3656 0.6159 0.090 Uiso 1 1 calc R . .
C24 C 0.2319(5) -0.3651(12) 0.6363(5) 0.087(5) Uani 1 1 d . . .
H24A H 0.2454 -0.3274 0.6577 0.131 Uiso 1 1 calc R . .
H24B H 0.2343 -0.4308 0.6431 0.131 Uiso 1 1 calc R . .
H24C H 0.2059 -0.3475 0.6274 0.131 Uiso 1 1 calc R . .
C25 C 0.1927(4) -0.2184(9) 0.5662(4) 0.064(4) Uani 1 1 d . . .
H25A H 0.1824 -0.2807 0.5579 0.076 Uiso 1 1 calc R . .
H25B H 0.1820 -0.1966 0.5843 0.076 Uiso 1 1 calc R . .
C26 C 0.1802(5) -0.1557(11) 0.5346(4) 0.086(6) Uani 1 1 d . . .
H26A H 0.1879 -0.0922 0.5426 0.129 Uiso 1 1 calc R . .
H26B H 0.1534 -0.1582 0.5235 0.129 Uiso 1 1 calc R . .
H26C H 0.1910 -0.1748 0.5166 0.129 Uiso 1 1 calc R . .
C27A C 0.2856(11) 0.095(2) 0.6738(11) 0.080(5) Uani 0.61(2) 1 d PDU A 1
H27A H 0.2825 0.1306 0.6512 0.096 Uiso 0.61(2) 1 calc PR A 1
H27B H 0.2607 0.0811 0.6739 0.096 Uiso 0.61(2) 1 calc PR A 1
C28A C 0.3056(10) 0.1559(16) 0.7066(11) 0.080(5) Uani 0.61(2) 1 d PDU A 1
H28A H 0.3128 0.1182 0.7289 0.121 Uiso 0.61(2) 1 calc PR A 1
H28B H 0.2893 0.2060 0.7084 0.121 Uiso 0.61(2) 1 calc PR A 1
H28C H 0.3276 0.1825 0.7038 0.121 Uiso 0.61(2) 1 calc PR A 1
C29A C 0.3228(5) -0.054(4) 0.7199(6) 0.105(7) Uani 0.61(2) 1 d PDU A 1
H29A H 0.3361 -0.1139 0.7221 0.126 Uiso 0.61(2) 1 calc PR A 1
H29B H 0.3400 -0.0089 0.7362 0.126 Uiso 0.61(2) 1 calc PR A 1
C30A C 0.2905(7) -0.068(3) 0.7326(5) 0.105(7) Uani 0.61(2) 1 d PDU A 1
H30A H 0.2766 -0.0102 0.7295 0.158 Uiso 0.61(2) 1 calc PR A 1
H30B H 0.2997 -0.0857 0.7585 0.158 Uiso 0.61(2) 1 calc PR A 1
H30C H 0.2745 -0.1172 0.7181 0.158 Uiso 0.61(2) 1 calc PR A 1
C31A C 0.3532(3) 0.003(2) 0.6667(6) 0.098(8) Uani 0.61(2) 1 d PDU A 1
H31A H 0.3679 0.0491 0.6847 0.117 Uiso 0.61(2) 1 calc PR A 1
H31B H 0.3669 -0.0563 0.6717 0.117 Uiso 0.61(2) 1 calc PR A 1
C32A C 0.3493(7) 0.036(2) 0.6285(6) 0.097(8) Uani 0.61(2) 1 d PDU A 1
H32A H 0.3345 -0.0089 0.6104 0.146 Uiso 0.61(2) 1 calc PR A 1
H32B H 0.3737 0.0410 0.6267 0.146 Uiso 0.61(2) 1 calc PR A 1
H32C H 0.3372 0.0965 0.6239 0.146 Uiso 0.61(2) 1 calc PR A 1
C27B C 0.2881(13) 0.096(3) 0.678(2) 0.080(5) Uani 0.39(2) 1 d PDU A 2
H27C H 0.2762 0.1245 0.6538 0.096 Uiso 0.39(2) 1 calc PR A 2
H27D H 0.2688 0.0831 0.6884 0.096 Uiso 0.39(2) 1 calc PR A 2
C28B C 0.3153(18) 0.165(2) 0.7028(19) 0.080(5) Uani 0.39(2) 1 d PDU A 2
H28D H 0.3247 0.1412 0.7279 0.120 Uiso 0.39(2) 1 calc PR A 2
H28E H 0.3029 0.2245 0.7023 0.120 Uiso 0.39(2) 1 calc PR A 2
H28F H 0.3357 0.1740 0.6942 0.120 Uiso 0.39(2) 1 calc PR A 2
C29B C 0.3351(7) -0.056(7) 0.7187(11) 0.105(8) Uani 0.39(2) 1 d PDU A 2
H29C H 0.3510 -0.1078 0.7169 0.126 Uiso 0.39(2) 1 calc PR A 2
H29D H 0.3512 -0.0056 0.7329 0.126 Uiso 0.39(2) 1 calc PR A 2
C30B C 0.3108(13) -0.089(4) 0.7393(8) 0.105(7) Uani 0.39(2) 1 d PDU A 2
H30D H 0.2969 -0.0365 0.7436 0.157 Uiso 0.39(2) 1 calc PR A 2
H30E H 0.3262 -0.1157 0.7628 0.157 Uiso 0.39(2) 1 calc PR A 2
H30F H 0.2937 -0.1363 0.7248 0.157 Uiso 0.39(2) 1 calc PR A 2
C31B C 0.3429(13) 0.0437(17) 0.6572(17) 0.097(8) Uani 0.39(2) 1 d PDU A 2
H31C H 0.3301 0.0904 0.6384 0.117 Uiso 0.39(2) 1 calc PR A 2
H31D H 0.3608 0.0770 0.6781 0.117 Uiso 0.39(2) 1 calc PR A 2
C32B C 0.3635(11) -0.023(3) 0.6413(15) 0.097(8) Uani 0.39(2) 1 d PDU A 2
H32D H 0.3767 -0.0686 0.6599 0.146 Uiso 0.39(2) 1 calc PR A 2
H32E H 0.3812 0.0119 0.6336 0.146 Uiso 0.39(2) 1 calc PR A 2
H32F H 0.3461 -0.0548 0.6201 0.146 Uiso 0.39(2) 1 calc PR A 2
C33A C 0.2086(6) 0.081(3) 0.4716(9) 0.133(9) Uani 0.761(16) 1 d PDU B 1
H33A H 0.2073 0.0356 0.4901 0.159 Uiso 0.761(16) 1 calc PR B 1
H33B H 0.1895 0.1284 0.4688 0.159 Uiso 0.761(16) 1 calc PR B 1
C34A C 0.2002(6) 0.031(2) 0.4353(7) 0.134(9) Uani 0.761(16) 1 d PDU B 1
H34A H 0.1844 0.0699 0.4154 0.202 Uiso 0.761(16) 1 calc PR B 1
H34B H 0.1877 -0.0278 0.4357 0.202 Uiso 0.761(16) 1 calc PR B 1
H34C H 0.2232 0.0182 0.4313 0.202 Uiso 0.761(16) 1 calc PR B 1
C35A C 0.2547(7) 0.2098(16) 0.4503(6) 0.138(10) Uani 0.761(16) 1 d PDU B 1
H35A H 0.2794 0.2374 0.4569 0.165 Uiso 0.761(16) 1 calc PR B 1
H35B H 0.2503 0.1705 0.4285 0.165 Uiso 0.761(16) 1 calc PR B 1
C36A C 0.2264(7) 0.2873(13) 0.4408(6) 0.141(10) Uani 0.761(16) 1 d PDU B 1
H36A H 0.2195 0.3012 0.4621 0.212 Uiso 0.761(16) 1 calc PR B 1
H36B H 0.2045 0.2678 0.4203 0.212 Uiso 0.761(16) 1 calc PR B 1
H36C H 0.2368 0.3429 0.4338 0.212 Uiso 0.761(16) 1 calc PR B 1
C37A C 0.2876(7) 0.0497(12) 0.4877(7) 0.116(7) Uani 0.761(16) 1 d PDU B 1
H37A H 0.2811 0.0253 0.4626 0.139 Uiso 0.761(16) 1 calc PR B 1
H37B H 0.3119 0.0798 0.4945 0.139 Uiso 0.761(16) 1 calc PR B 1
C38A C 0.2902(7) -0.0309(12) 0.5136(7) 0.117(7) Uani 0.761(16) 1 d PDU B 1
H38A H 0.3014 -0.0095 0.5390 0.176 Uiso 0.761(16) 1 calc PR B 1
H38B H 0.3053 -0.0802 0.5090 0.176 Uiso 0.761(16) 1 calc PR B 1
H38C H 0.2655 -0.0550 0.5096 0.176 Uiso 0.761(16) 1 calc PR B 1
C33B C 0.2130(18) 0.062(6) 0.474(3) 0.134(9) Uani 0.239(16) 1 d PDU B 2
H33C H 0.2102 0.0356 0.4965 0.160 Uiso 0.239(16) 1 calc PR B 2
H33D H 0.1911 0.1004 0.4618 0.160 Uiso 0.239(16) 1 calc PR B 2
C34B C 0.215(3) -0.017(5) 0.449(3) 0.134(10) Uani 0.239(16) 1 d PDU B 2
H34D H 0.2146 0.0088 0.4259 0.201 Uiso 0.239(16) 1 calc PR B 2
H34E H 0.1934 -0.0573 0.4447 0.201 Uiso 0.239(16) 1 calc PR B 2
H34F H 0.2373 -0.0525 0.4607 0.201 Uiso 0.239(16) 1 calc PR B 2
C35B C 0.2769(17) 0.189(4) 0.4599(19) 0.139(10) Uani 0.239(16) 1 d PDU B 2
H35C H 0.3027 0.2029 0.4754 0.166 Uiso 0.239(16) 1 calc PR B 2
H35D H 0.2774 0.1442 0.4410 0.166 Uiso 0.239(16) 1 calc PR B 2
C36B C 0.259(2) 0.278(4) 0.441(2) 0.139(10) Uani 0.239(16) 1 d PDU B 2
H36D H 0.2335 0.2653 0.4253 0.209 Uiso 0.239(16) 1 calc PR B 2
H36E H 0.2725 0.3029 0.4264 0.209 Uiso 0.239(16) 1 calc PR B 2
H36F H 0.2589 0.3242 0.4596 0.209 Uiso 0.239(16) 1 calc PR B 2
C37B C 0.2751(13) 0.0245(18) 0.5044(19) 0.117(8) Uani 0.239(16) 1 d PDU B 2
H37C H 0.2602 -0.0090 0.5163 0.140 Uiso 0.239(16) 1 calc PR B 2
H37D H 0.2751 -0.0127 0.4832 0.140 Uiso 0.239(16) 1 calc PR B 2
C38B C 0.3143(13) 0.032(5) 0.5315(17) 0.117(8) Uani 0.239(16) 1 d PDU B 2
H38D H 0.3146 0.0688 0.5527 0.175 Uiso 0.239(16) 1 calc PR B 2
H38E H 0.3296 0.0631 0.5196 0.175 Uiso 0.239(16) 1 calc PR B 2
H38F H 0.3241 -0.0298 0.5395 0.175 Uiso 0.239(16) 1 calc PR B 2
C39 C 0.3176(3) 0.3034(11) 0.6268(3) 0.055(4) Uani 1 1 d . B .
H39A H 0.3107 0.2499 0.6388 0.066 Uiso 1 1 calc R . .
H39B H 0.3382 0.2833 0.6193 0.066 Uiso 1 1 calc R . .
C40 C 0.3315(4) 0.3812(13) 0.6550(4) 0.083(5) Uani 1 1 d . . .
H40A H 0.3420 0.4310 0.6448 0.125 Uiso 1 1 calc R B .
H40B H 0.3504 0.3566 0.6771 0.125 Uiso 1 1 calc R . .
H40C H 0.3110 0.4057 0.6613 0.125 Uiso 1 1 calc R . .
C41 C 0.2422(4) 0.3654(11) 0.6026(4) 0.062(4) Uani 1 1 d . B .
H41A H 0.2502 0.4216 0.6179 0.074 Uiso 1 1 calc R . .
H41B H 0.2201 0.3821 0.5813 0.074 Uiso 1 1 calc R . .
C42 C 0.2316(4) 0.2934(12) 0.6243(4) 0.070(5) Uani 1 1 d . . .
H42A H 0.2247 0.2362 0.6100 0.106 Uiso 1 1 calc R B .
H42B H 0.2107 0.3156 0.6304 0.106 Uiso 1 1 calc R . .
H42C H 0.2524 0.2809 0.6469 0.106 Uiso 1 1 calc R . .
C43 C 0.2917(4) 0.4407(11) 0.5707(4) 0.072(4) Uani 1 1 d . B .
H43A H 0.2955 0.4876 0.5902 0.086 Uiso 1 1 calc R . .
H43B H 0.3154 0.4323 0.5671 0.086 Uiso 1 1 calc R . .
C44 C 0.2639(5) 0.4766(11) 0.5360(4) 0.087(6) Uani 1 1 d . . .
H44A H 0.2632 0.4360 0.5157 0.130 Uiso 1 1 calc R B .
H44B H 0.2707 0.5395 0.5313 0.130 Uiso 1 1 calc R . .
H44C H 0.2397 0.4777 0.5383 0.130 Uiso 1 1 calc R . .
C45A C 0.0954(12) 0.336(4) 0.4184(7) 0.080(6) Uani 0.60(6) 1 d PDU C 1
H45A H 0.0749 0.3094 0.3977 0.096 Uiso 0.60(6) 1 calc PR C 1
H45B H 0.1008 0.3983 0.4111 0.096 Uiso 0.60(6) 1 calc PR C 1
C46A C 0.1292(8) 0.275(3) 0.4256(9) 0.080(6) Uani 0.60(6) 1 d PDU C 1
H46A H 0.1509 0.3072 0.4421 0.120 Uiso 0.60(6) 1 calc PR C 1
H46B H 0.1326 0.2616 0.4025 0.120 Uiso 0.60(6) 1 calc PR C 1
H46C H 0.1258 0.2166 0.4369 0.120 Uiso 0.60(6) 1 calc PR C 1
C47A C 0.0701(15) 0.2274(15) 0.4657(8) 0.092(6) Uani 0.60(6) 1 d PDU C 1
H47A H 0.0932 0.1917 0.4755 0.110 Uiso 0.60(6) 1 calc PR C 1
H47B H 0.0585 0.2272 0.4845 0.110 Uiso 0.60(6) 1 calc PR C 1
C48A C 0.0445(14) 0.1793(19) 0.4315(10) 0.092(6) Uani 0.60(6) 1 d PDU C 1
H48A H 0.0277 0.2249 0.4156 0.138 Uiso 0.60(6) 1 calc PR C 1
H48B H 0.0304 0.1314 0.4385 0.138 Uiso 0.60(6) 1 calc PR C 1
H48C H 0.0591 0.1506 0.4184 0.138 Uiso 0.60(6) 1 calc PR C 1
C49A C 0.0345(8) 0.393(5) 0.4464(9) 0.082(6) Uani 0.60(6) 1 d PDU C 1
H49A H 0.0340 0.4581 0.4382 0.098 Uiso 0.60(6) 1 calc PR C 1
H49B H 0.0175 0.3569 0.4258 0.098 Uiso 0.60(6) 1 calc PR C 1
C50A C 0.0207(7) 0.390(3) 0.4783(10) 0.082(6) Uani 0.60(6) 1 d PDU C 1
H50A H 0.0149 0.3259 0.4824 0.123 Uiso 0.60(6) 1 calc PR C 1
H50B H -0.0014 0.4284 0.4725 0.123 Uiso 0.60(6) 1 calc PR C 1
H50C H 0.0398 0.4140 0.5003 0.123 Uiso 0.60(6) 1 calc PR C 1
C45B C 0.0897(16) 0.349(7) 0.4149(9) 0.079(6) Uani 0.40(6) 1 d PDU C 2
H45C H 0.0701 0.3132 0.3963 0.095 Uiso 0.40(6) 1 calc PR C 2
H45D H 0.0882 0.4138 0.4062 0.095 Uiso 0.40(6) 1 calc PR C 2
C46B C 0.1268(12) 0.309(4) 0.4181(13) 0.080(6) Uani 0.40(6) 1 d PDU C 2
H46D H 0.1452 0.3272 0.4417 0.120 Uiso 0.40(6) 1 calc PR C 2
H46E H 0.1340 0.3328 0.3982 0.120 Uiso 0.40(6) 1 calc PR C 2
H46F H 0.1252 0.2412 0.4166 0.120 Uiso 0.40(6) 1 calc PR C 2
C47B C 0.0731(17) 0.2249(18) 0.4652(17) 0.092(6) Uani 0.40(6) 1 d PDU C 2
H47C H 0.0940 0.1879 0.4639 0.110 Uiso 0.40(6) 1 calc PR C 2
H47D H 0.0725 0.2177 0.4901 0.110 Uiso 0.40(6) 1 calc PR C 2
C48B C 0.0377(19) 0.186(3) 0.4378(16) 0.092(6) Uani 0.40(6) 1 d PDU C 2
H48D H 0.0169 0.2244 0.4380 0.138 Uiso 0.40(6) 1 calc PR C 2
H48E H 0.0342 0.1224 0.4443 0.138 Uiso 0.40(6) 1 calc PR C 2
H48F H 0.0391 0.1876 0.4132 0.138 Uiso 0.40(6) 1 calc PR C 2
C49B C 0.0356(14) 0.401(8) 0.4387(14) 0.082(6) Uani 0.40(6) 1 d PDU C 2
H49C H 0.0385 0.4645 0.4304 0.099 Uiso 0.40(6) 1 calc PR C 2
H49D H 0.0204 0.3651 0.4171 0.099 Uiso 0.40(6) 1 calc PR C 2
C50B C 0.0156(10) 0.407(5) 0.4657(17) 0.082(6) Uani 0.40(6) 1 d PDU C 2
H50D H 0.0055 0.3457 0.4678 0.123 Uiso 0.40(6) 1 calc PR C 2
H50E H -0.0043 0.4521 0.4570 0.123 Uiso 0.40(6) 1 calc PR C 2
H50F H 0.0329 0.4260 0.4897 0.123 Uiso 0.40(6) 1 calc PR C 2
C51 C 0.0959(4) 0.5910(10) 0.4282(3) 0.055(4) Uani 1 1 d . C .
H51A H 0.1011 0.5403 0.4137 0.066 Uiso 1 1 calc R . .
H51B H 0.0692 0.5899 0.4235 0.066 Uiso 1 1 calc R . .
C52 C 0.1050(4) 0.6825(9) 0.4140(3) 0.053(4) Uani 1 1 d . . .
H52A H 0.1029 0.7332 0.4299 0.080 Uiso 1 1 calc R C .
H52B H 0.0878 0.6931 0.3891 0.080 Uiso 1 1 calc R . .
H52C H 0.1301 0.6803 0.4140 0.080 Uiso 1 1 calc R . .
C53 C 0.1021(4) 0.6539(9) 0.4984(3) 0.049(3) Uani 1 1 d . C .
H53A H 0.1187 0.6611 0.5241 0.059 Uiso 1 1 calc R . .
H53B H 0.1012 0.7139 0.4858 0.059 Uiso 1 1 calc R . .
C54 C 0.0633(4) 0.6302(12) 0.4977(5) 0.080(5) Uani 1 1 d . . .
H54A H 0.0471 0.6177 0.4724 0.120 Uiso 1 1 calc R C .
H54B H 0.0536 0.6826 0.5073 0.120 Uiso 1 1 calc R . .
H54C H 0.0645 0.5751 0.5127 0.120 Uiso 1 1 calc R . .
C55 C 0.1669(3) 0.6035(9) 0.4838(3) 0.044(3) Uani 1 1 d . C .
H55A H 0.1663 0.6693 0.4764 0.053 Uiso 1 1 calc R . .
H55B H 0.1816 0.5996 0.5102 0.053 Uiso 1 1 calc R . .
C56 C 0.1855(4) 0.5467(12) 0.4628(4) 0.066(4) Uani 1 1 d . . .
H56A H 0.1870 0.4818 0.4707 0.099 Uiso 1 1 calc R C .
H56B H 0.2103 0.5709 0.4676 0.099 Uiso 1 1 calc R . .
H56C H 0.1712 0.5506 0.4366 0.099 Uiso 1 1 calc R . .
C57A C 0.0179(13) 0.0779(17) 0.5500(5) 0.063(6) Uani 0.59(4) 1 d PDU D 1
H57A H 0.0436 0.0558 0.5571 0.076 Uiso 0.59(4) 1 calc PR D 1
H57B H 0.0016 0.0229 0.5437 0.076 Uiso 0.59(4) 1 calc PR D 1
C58A C 0.0091(10) 0.139(2) 0.5164(3) 0.063(6) Uani 0.59(4) 1 d PDU D 1
H58A H -0.0166 0.1593 0.5085 0.076 Uiso 0.59(4) 1 calc PR D 1
H58B H 0.0131 0.1042 0.4966 0.076 Uiso 0.59(4) 1 calc PR D 1
H58C H 0.0252 0.1937 0.5223 0.076 Uiso 0.59(4) 1 calc PR D 1
C59A C -0.0363(3) 0.168(2) 0.5700(17) 0.098(6) Uani 0.59(4) 1 d PDU D 1
H59A H -0.0445 0.1863 0.5902 0.117 Uiso 0.59(4) 1 calc PR D 1
H59B H -0.0391 0.2228 0.5539 0.117 Uiso 0.59(4) 1 calc PR D 1
C60A C -0.0608(4) 0.091(3) 0.5482(12) 0.099(7) Uani 0.59(4) 1 d PDU D 1
H60A H -0.0556 0.0335 0.5627 0.118 Uiso 0.59(4) 1 calc PR D 1
H60B H -0.0561 0.0805 0.5255 0.118 Uiso 0.59(4) 1 calc PR D 1
H60C H -0.0866 0.1078 0.5423 0.118 Uiso 0.59(4) 1 calc PR D 1
C61A C 0.0175(16) 0.0413(14) 0.6212(9) 0.077(6) Uani 0.59(4) 1 d PDU D 1
H61A H -0.0005 -0.0078 0.6091 0.092 Uiso 0.59(4) 1 calc PR D 1
H61B H 0.0424 0.0145 0.6275 0.092 Uiso 0.59(4) 1 calc PR D 1
C62A C 0.0119(10) 0.070(2) 0.6563(5) 0.077(6) Uani 0.59(4) 1 d PDU D 1
H62A H 0.0231 0.1310 0.6640 0.093 Uiso 0.59(4) 1 calc PR D 1
H62B H 0.0235 0.0243 0.6755 0.093 Uiso 0.59(4) 1 calc PR D 1
H62C H -0.0145 0.0732 0.6519 0.093 Uiso 0.59(4) 1 calc PR D 1
C57B C 0.0254(19) 0.064(3) 0.5575(10) 0.064(6) Uani 0.41(4) 1 d PDU D 2
H57C H 0.0510 0.0428 0.5698 0.076 Uiso 0.41(4) 1 calc PR D 2
H57D H 0.0094 0.0087 0.5513 0.076 Uiso 0.41(4) 1 calc PR D 2
C58B C 0.0227(14) 0.114(3) 0.5222(7) 0.064(6) Uani 0.41(4) 1 d PDU D 2
H58D H 0.0260 0.1805 0.5268 0.076 Uiso 0.41(4) 1 calc PR D 2
H58E H -0.0015 0.1020 0.5036 0.076 Uiso 0.41(4) 1 calc PR D 2
H58F H 0.0418 0.0903 0.5136 0.076 Uiso 0.41(4) 1 calc PR D 2
C59B C -0.0362(3) 0.169(3) 0.569(3) 0.098(7) Uani 0.41(4) 1 d PDU D 2
H59C H -0.0418 0.2134 0.5858 0.117 Uiso 0.41(4) 1 calc PR D 2
H59D H -0.0406 0.2002 0.5457 0.117 Uiso 0.41(4) 1 calc PR D 2
C60B C -0.0621(4) 0.086(4) 0.5631(18) 0.098(7) Uani 0.41(4) 1 d PDU D 2
H60D H -0.0623 0.0519 0.5415 0.118 Uiso 0.41(4) 1 calc PR D 2
H60E H -0.0870 0.1087 0.5594 0.118 Uiso 0.41(4) 1 calc PR D 2
H60F H -0.0538 0.0456 0.5845 0.118 Uiso 0.41(4) 1 calc PR D 2
C61B C 0.012(2) 0.057(3) 0.6254(14) 0.076(6) Uani 0.41(4) 1 d PDU D 2
H61C H -0.0038 0.0037 0.6143 0.092 Uiso 0.41(4) 1 calc PR D 2
H61D H 0.0374 0.0332 0.6378 0.092 Uiso 0.41(4) 1 calc PR D 2
C62B C -0.0010(15) 0.101(3) 0.6538(8) 0.077(6) Uani 0.41(4) 1 d PDU D 2
H62D H 0.0194 0.1349 0.6718 0.092 Uiso 0.41(4) 1 calc PR D 2
H62E H -0.0099 0.0531 0.6661 0.092 Uiso 0.41(4) 1 calc PR D 2
H62F H -0.0210 0.1450 0.6417 0.092 Uiso 0.41(4) 1 calc PR D 2
C63A C 0.0925(5) 0.4682(13) 0.6093(5) 0.066(5) Uani 0.533(12) 1 d PDU D 1
H63A H 0.1044 0.5231 0.6239 0.079 Uiso 0.533(12) 1 calc PR D 1
H63B H 0.1070 0.4502 0.5942 0.079 Uiso 0.533(12) 1 calc PR D 1
C64A C 0.0540(6) 0.4946(15) 0.5843(6) 0.067(5) Uani 0.533(12) 1 d PDU D 1
H64A H 0.0427 0.4422 0.5683 0.080 Uiso 0.533(12) 1 calc PR D 1
H64B H 0.0553 0.5482 0.5694 0.080 Uiso 0.533(12) 1 calc PR D 1
H64C H 0.0391 0.5104 0.5991 0.080 Uiso 0.533(12) 1 calc PR D 1
C65A C 0.0865(6) 0.4302(10) 0.6791(4) 0.055(4) Uani 0.533(12) 1 d PDU D 1
H65A H 0.1058 0.4777 0.6890 0.066 Uiso 0.533(12) 1 calc PR D 1
H65B H 0.0625 0.4625 0.6702 0.066 Uiso 0.533(12) 1 calc PR D 1
C66A C 0.0873(8) 0.3641(17) 0.7097(3) 0.056(4) Uani 0.533(12) 1 d PDU D 1
H66A H 0.0666 0.3207 0.7007 0.067 Uiso 0.533(12) 1 calc PR D 1
H66B H 0.0854 0.3996 0.7303 0.067 Uiso 0.533(12) 1 calc PR D 1
H66C H 0.1105 0.3293 0.7177 0.067 Uiso 0.533(12) 1 calc PR D 1
C67A C 0.14189(19) 0.3427(11) 0.6531(7) 0.038(4) Uani 0.533(12) 1 d PDU D 1
H67A H 0.1487 0.2988 0.6739 0.046 Uiso 0.533(12) 1 calc PR D 1
H67B H 0.1455 0.3106 0.6323 0.046 Uiso 0.533(12) 1 calc PR D 1
C68A C 0.1675(2) 0.4259(16) 0.6638(8) 0.041(4) Uani 0.533(12) 1 d PDU D 1
H68A H 0.1548 0.4808 0.6504 0.049 Uiso 0.533(12) 1 calc PR D 1
H68B H 0.1894 0.4135 0.6576 0.049 Uiso 0.533(12) 1 calc PR D 1
H68C H 0.1749 0.4369 0.6901 0.049 Uiso 0.533(12) 1 calc PR D 1
C63B C 0.0763(9) 0.4916(9) 0.6310(6) 0.066(5) Uani 0.467(12) 1 d PDU D 2
H63C H 0.0533 0.4970 0.6363 0.079 Uiso 0.467(12) 1 calc PR D 2
H63D H 0.0945 0.5343 0.6477 0.079 Uiso 0.467(12) 1 calc PR D 2
C64B C 0.0688(10) 0.5217(13) 0.5918(6) 0.067(5) Uani 0.467(12) 1 d PDU D 2
H64D H 0.0644 0.5888 0.5896 0.080 Uiso 0.467(12) 1 calc PR D 2
H64E H 0.0471 0.4892 0.5754 0.080 Uiso 0.467(12) 1 calc PR D 2
H64F H 0.0901 0.5066 0.5850 0.080 Uiso 0.467(12) 1 calc PR D 2
C65B C 0.1060(5) 0.3662(19) 0.69008(17) 0.057(4) Uani 0.467(12) 1 d PDU D 2
H65C H 0.1252 0.3183 0.6998 0.068 Uiso 0.467(12) 1 calc PR D 2
H65D H 0.1166 0.4265 0.7009 0.068 Uiso 0.467(12) 1 calc PR D 2
C66B C 0.0739(7) 0.343(2) 0.7021(4) 0.057(4) Uani 0.467(12) 1 d PDU D 2
H66D H 0.0528 0.3824 0.6887 0.069 Uiso 0.467(12) 1 calc PR D 2
H66E H 0.0810 0.3545 0.7284 0.069 Uiso 0.467(12) 1 calc PR D 2
H66F H 0.0672 0.2778 0.6968 0.069 Uiso 0.467(12) 1 calc PR D 2
C67B C 0.1394(3) 0.3663(16) 0.6384(7) 0.039(4) Uani 0.467(12) 1 d PDU D 2
H67C H 0.1512 0.3079 0.6502 0.047 Uiso 0.467(12) 1 calc PR D 2
H67D H 0.1373 0.3637 0.6124 0.047 Uiso 0.467(12) 1 calc PR D 2
C68B C 0.1640(4) 0.4473(19) 0.6567(10) 0.041(4) Uani 0.467(12) 1 d PDU D 2
H68D H 0.1566 0.4714 0.6765 0.050 Uiso 0.467(12) 1 calc PR D 2
H68E H 0.1616 0.4965 0.6387 0.050 Uiso 0.467(12) 1 calc PR D 2
H68F H 0.1896 0.4264 0.6668 0.050 Uiso 0.467(12) 1 calc PR D 2
C69 C 0.1381(6) 0.1419(13) 0.7318(6) 0.104(5) Uani 1 1 d U E 1
H69A H 0.1517 0.1925 0.7482 0.125 Uiso 1 1 calc R E 1
H69B H 0.1256 0.1684 0.7072 0.125 Uiso 1 1 calc R E 1
C70 C 0.1107(6) 0.1030(13) 0.7456(6) 0.105(5) Uani 1 1 d U E 1
H70A H 0.0961 0.0561 0.7284 0.158 Uiso 1 1 calc R E 1
H70B H 0.0945 0.1526 0.7480 0.158 Uiso 1 1 calc R E 1
H70C H 0.1232 0.0742 0.7695 0.158 Uiso 1 1 calc R E 1
C71 C 0.1942(5) 0.0181(15) 0.7761(5) 0.102(5) Uani 1 1 d U E 1
H71A H 0.2044 0.0745 0.7906 0.122 Uiso 1 1 calc R E 1
H71B H 0.1763 -0.0103 0.7857 0.122 Uiso 1 1 calc R E 1
C72 C 0.2262(5) -0.0525(14) 0.7800(5) 0.103(5) Uani 1 1 d U E 1
H72A H 0.2160 -0.1098 0.7668 0.155 Uiso 1 1 calc R E 1
H72B H 0.2393 -0.0665 0.8059 0.155 Uiso 1 1 calc R E 1
H72C H 0.2434 -0.0251 0.7696 0.155 Uiso 1 1 calc R E 1
C73 C 0.2008(7) 0.1228(15) 0.7133(7) 0.137(7) Uani 1 1 d U E 1
H73A H 0.2197 0.0833 0.7090 0.164 Uiso 1 1 calc R E 1
H73B H 0.1854 0.1487 0.6893 0.164 Uiso 1 1 calc R E 1
C74 C 0.2194(7) 0.1993(15) 0.7365(7) 0.141(7) Uani 1 1 d U E 1
H74A H 0.2012 0.2407 0.7404 0.211 Uiso 1 1 calc R E 1
H74B H 0.2339 0.2337 0.7247 0.211 Uiso 1 1 calc R E 1
H74C H 0.2357 0.1751 0.7601 0.211 Uiso 1 1 calc R E 1
C75A C 0.1528(5) -0.2818(11) 0.6543(5) 0.059(4) Uani 0.565(12) 1 d PDU E 1
H75A H 0.1406 -0.3310 0.6364 0.071 Uiso 0.565(12) 1 calc PR E 1
H75B H 0.1715 -0.2523 0.6461 0.071 Uiso 0.565(12) 1 calc PR E 1
C76A C 0.1719(5) -0.3261(12) 0.6915(6) 0.060(4) Uani 0.565(12) 1 d PDU E 1
H76A H 0.1860 -0.2788 0.7088 0.072 Uiso 0.565(12) 1 calc PR E 1
H76B H 0.1885 -0.3750 0.6894 0.072 Uiso 0.565(12) 1 calc PR E 1
H76C H 0.1535 -0.3531 0.7004 0.072 Uiso 0.565(12) 1 calc PR E 1
C77A C 0.1035(8) -0.1576(13) 0.6065(2) 0.076(5) Uani 0.565(12) 1 d PDU E 1
H77A H 0.0871 -0.1033 0.6032 0.091 Uiso 0.565(12) 1 calc PR E 1
H77B H 0.1253 -0.1376 0.6009 0.091 Uiso 0.565(12) 1 calc PR E 1
C78A C 0.0834(7) -0.2326(18) 0.5795(2) 0.077(5) Uani 0.565(12) 1 d PDU E 1
H78A H 0.1002 -0.2844 0.5810 0.092 Uiso 0.565(12) 1 calc PR E 1
H78B H 0.0747 -0.2070 0.5547 0.092 Uiso 0.565(12) 1 calc PR E 1
H78C H 0.0624 -0.2546 0.5854 0.092 Uiso 0.565(12) 1 calc PR E 1
C79A C 0.0762(4) -0.2401(17) 0.6579(11) 0.097(7) Uani 0.565(12) 1 d PDU E 1
H79A H 0.0702 -0.2998 0.6445 0.117 Uiso 0.565(12) 1 calc PR E 1
H79B H 0.0804 -0.2527 0.6839 0.117 Uiso 0.565(12) 1 calc PR E 1
C80A C 0.0437(3) -0.175(2) 0.6427(7) 0.098(7) Uani 0.565(12) 1 d PDU E 1
H80A H 0.0489 -0.1169 0.6568 0.118 Uiso 0.565(12) 1 calc PR E 1
H80B H 0.0217 -0.2039 0.6446 0.118 Uiso 0.565(12) 1 calc PR E 1
H80C H 0.0396 -0.1612 0.6170 0.118 Uiso 0.565(12) 1 calc PR E 1
C75B C 0.1373(5) -0.2979(11) 0.6820(7) 0.060(4) Uani 0.435(12) 1 d PDU E 2
H75C H 0.1277 -0.3009 0.7022 0.072 Uiso 0.435(12) 1 calc PR E 2
H75D H 0.1286 -0.3539 0.6666 0.072 Uiso 0.435(12) 1 calc PR E 2
C76B C 0.1791(5) -0.2993(16) 0.6980(9) 0.059(4) Uani 0.435(12) 1 d PDU E 2
H76D H 0.1889 -0.2930 0.6782 0.071 Uiso 0.435(12) 1 calc PR E 2
H76E H 0.1874 -0.3581 0.7108 0.071 Uiso 0.435(12) 1 calc PR E 2
H76F H 0.1878 -0.2476 0.7152 0.071 Uiso 0.435(12) 1 calc PR E 2
C77B C 0.1195(8) -0.223(2) 0.6091(3) 0.077(5) Uani 0.435(12) 1 d PDU E 2
H77C H 0.1448 -0.2140 0.6093 0.092 Uiso 0.435(12) 1 calc PR E 2
H77D H 0.1133 -0.2897 0.6040 0.092 Uiso 0.435(12) 1 calc PR E 2
C78B C 0.0931(9) -0.165(3) 0.5786(2) 0.077(5) Uani 0.435(12) 1 d PDU E 2
H78D H 0.0687 -0.1667 0.5805 0.092 Uiso 0.435(12) 1 calc PR E 2
H78E H 0.0916 -0.1908 0.5549 0.092 Uiso 0.435(12) 1 calc PR E 2
H78F H 0.1019 -0.1012 0.5807 0.092 Uiso 0.435(12) 1 calc PR E 2
C79B C 0.0745(6) -0.246(2) 0.6505(15) 0.098(7) Uani 0.435(12) 1 d PDU E 2
H79C H 0.0619 -0.2674 0.6251 0.117 Uiso 0.435(12) 1 calc PR E 2
H79D H 0.0789 -0.3005 0.6668 0.117 Uiso 0.435(12) 1 calc PR E 2
C80B C 0.0493(5) -0.179(3) 0.6605(10) 0.099(7) Uani 0.435(12) 1 d PDU E 2
H80D H 0.0512 -0.1171 0.6508 0.119 Uiso 0.435(12) 1 calc PR E 2
H80E H 0.0567 -0.1755 0.6871 0.119 Uiso 0.435(12) 1 calc PR E 2
H80F H 0.0239 -0.2008 0.6499 0.119 Uiso 0.435(12) 1 calc PR E 2
Pt6 Pt 0.100401(13) 0.23162(4) 0.054217(13) 0.04153(12) Uani 1 1 d . F .
Pt7 Pt 0.188576(12) 0.55612(3) 0.146510(13) 0.03583(11) Uani 1 1 d . F .
Pt8 Pt 0.136862(13) 0.61866(3) 0.277993(13) 0.03990(12) Uani 1 1 d . F .
Pt9 Pt 0.039625(12) 0.27715(3) 0.276353(12) 0.03535(11) Uani 1 1 d . . .
Pt10 Pt -0.004679(12) 0.07819(3) 0.128698(12) 0.03519(11) Uani 1 1 d . F .
Cl6 Cl 0.10550(13) 0.1445(3) 0.00370(10) 0.0884(15) Uani 1 1 d . . .
Cl7 Cl 0.23692(10) 0.6223(3) 0.12952(10) 0.0610(9) Uani 1 1 d . . .
Cl8 Cl 0.17016(11) 0.7339(3) 0.32203(10) 0.0713(11) Uani 1 1 d . . .
Cl9 Cl 0.03607(10) 0.2274(3) 0.33409(8) 0.0577(9) Uani 1 1 d . . .
Cl10 Cl 0.05080(8) -0.0002(2) 0.16377(9) 0.0466(8) Uani 1 1 d . . .
P11 P 0.12968(11) 0.1141(2) 0.09349(10) 0.0545(9) Uani 1 1 d D . .
P12 P 0.07217(10) 0.3544(3) 0.01700(9) 0.0531(9) Uani 1 1 d D . .
P13 P 0.15230(12) 0.6828(3) 0.12150(10) 0.0676(12) Uani 1 1 d D . .
P14 P 0.22542(9) 0.4315(2) 0.17156(10) 0.0492(9) Uani 1 1 d D . .
P15 P 0.09136(10) 0.7252(2) 0.24844(9) 0.0459(8) Uani 1 1 d . . .
P16 P 0.18013(9) 0.5157(3) 0.31152(10) 0.0514(9) Uani 1 1 d . F .
P17 P -0.00487(8) 0.3849(3) 0.27151(9) 0.0423(8) Uani 1 1 d . . .
P18 P 0.08215(9) 0.1603(2) 0.28381(9) 0.0429(8) Uani 1 1 d . . .
P19 P -0.03259(9) -0.0686(2) 0.12484(9) 0.0458(8) Uani 1 1 d . . .
P20 P -0.05428(9) 0.1614(2) 0.09775(10) 0.0481(9) Uani 1 1 d . . .
C81 C 0.0642(3) 0.3617(8) 0.1337(3) 0.030(3) Uani 1 1 d . . .
C82 C 0.0890(3) 0.4327(8) 0.1470(3) 0.039(3) Uani 1 1 d . F .
C83 C 0.0859(3) 0.4658(7) 0.1800(3) 0.033(3) Uani 1 1 d . . .
C84 C 0.0598(3) 0.4095(8) 0.1868(3) 0.032(3) Uani 1 1 d . F .
C85 C 0.0459(3) 0.3453(8) 0.1584(3) 0.036(3) Uani 1 1 d . . .
C86 C 0.0678(3) 0.2925(9) 0.1102(3) 0.041(3) Uani 1 1 d . F .
C87 C 0.0962(3) 0.3102(9) 0.0955(3) 0.040(3) Uani 1 1 d . . .
C88 C 0.1212(3) 0.3827(9) 0.1102(3) 0.043(3) Uani 1 1 d . F .
H88 H 0.1401 0.3916 0.1005 0.051 Uiso 1 1 calc R . .
C89 C 0.1204(3) 0.4446(8) 0.1387(3) 0.042(3) Uani 1 1 d . . .
C90 C 0.1475(3) 0.5096(8) 0.1614(3) 0.037(3) Uani 1 1 d . F .
C91 C 0.1429(3) 0.5418(8) 0.1944(3) 0.037(3) Uani 1 1 d . . .
H91 H 0.1607 0.5837 0.2094 0.044 Uiso 1 1 calc R F .
C92 C 0.1134(3) 0.5156(9) 0.2063(3) 0.043(3) Uani 1 1 d . F .
C93 C 0.1087(3) 0.5200(8) 0.2411(3) 0.035(3) Uani 1 1 d . . .
C94 C 0.0842(3) 0.4597(8) 0.2486(3) 0.034(3) Uani 1 1 d . F .
H94 H 0.0834 0.4607 0.2726 0.040 Uiso 1 1 calc R . .
C95 C 0.0601(3) 0.3959(8) 0.2226(3) 0.037(3) Uani 1 1 d . . .
C96 C 0.0418(3) 0.3112(8) 0.2276(3) 0.038(3) Uani 1 1 d . F .
C97 C 0.0269(3) 0.2503(8) 0.1971(3) 0.035(3) Uani 1 1 d . . .
H97 H 0.0136 0.1977 0.2001 0.042 Uiso 1 1 calc R F .
C98 C 0.0306(3) 0.2621(8) 0.1626(3) 0.036(3) Uani 1 1 d . F .
C99 C 0.0270(3) 0.1959(8) 0.1334(3) 0.039(3) Uani 1 1 d . . .
C100 C 0.0447(3) 0.2120(8) 0.1084(3) 0.036(3) Uani 1 1 d . F .
H100 H 0.0415 0.1682 0.0893 0.043 Uiso 1 1 calc R . .
C101 C 0.1310(6) 0.1197(15) 0.1406(2) 0.057(5) Uani 0.596(13) 1 d PDU F 1
H10A H 0.1393 0.1823 0.1505 0.068 Uiso 0.596(13) 1 calc PR F 1
H10B H 0.1058 0.1107 0.1406 0.068 Uiso 0.596(13) 1 calc PR F 1
C102 C 0.1562(8) 0.048(2) 0.1656(4) 0.057(5) Uani 0.596(13) 1 d PDU F 1
H10C H 0.1505 -0.0136 0.1543 0.086 Uiso 0.596(13) 1 calc PR F 1
H10D H 0.1526 0.0474 0.1891 0.086 Uiso 0.596(13) 1 calc PR F 1
H10E H 0.1818 0.0633 0.1696 0.086 Uiso 0.596(13) 1 calc PR F 1
C103 C 0.1158(4) -0.0038(8) 0.0773(7) 0.072(5) Uani 0.596(13) 1 d PDU F 1
H10F H 0.1195 -0.0130 0.0538 0.086 Uiso 0.596(13) 1 calc PR F 1
H10G H 0.1319 -0.0483 0.0952 0.086 Uiso 0.596(13) 1 calc PR F 1
C104 C 0.0760(5) -0.0250(12) 0.0720(8) 0.073(5) Uani 0.596(13) 1 d PDU F 1
H10H H 0.0712 -0.0084 0.0942 0.109 Uiso 0.596(13) 1 calc PR F 1
H10I H 0.0712 -0.0913 0.0670 0.109 Uiso 0.596(13) 1 calc PR F 1
H10J H 0.0597 0.0111 0.0513 0.109 Uiso 0.596(13) 1 calc PR F 1
C105 C 0.17923(18) 0.109(2) 0.1036(5) 0.092(7) Uani 0.596(13) 1 d PDU F 1
H10K H 0.1913 0.1587 0.1213 0.111 Uiso 0.596(13) 1 calc PR F 1
H10L H 0.1886 0.0488 0.1153 0.111 Uiso 0.596(13) 1 calc PR F 1
C106 C 0.1898(5) 0.120(2) 0.0700(7) 0.092(7) Uani 0.596(13) 1 d PDU F 1
H10M H 0.1810 0.0665 0.0539 0.139 Uiso 0.596(13) 1 calc PR F 1
H10N H 0.2166 0.1244 0.0775 0.139 Uiso 0.596(13) 1 calc PR F 1
H10O H 0.1786 0.1769 0.0569 0.139 Uiso 0.596(13) 1 calc PR F 1
C201 C 0.1422(12) 0.137(2) 0.1423(3) 0.057(5) Uani 0.404(13) 1 d PDU F 2
H20A H 0.1655 0.1726 0.1510 0.068 Uiso 0.404(13) 1 calc PR F 2
H20B H 0.1229 0.1762 0.1460 0.068 Uiso 0.404(13) 1 calc PR F 2
C202 C 0.1469(14) 0.050(3) 0.1653(5) 0.057(5) Uani 0.404(13) 1 d PDU F 2
H20C H 0.1245 0.0120 0.1559 0.086 Uiso 0.404(13) 1 calc PR F 2
H20D H 0.1513 0.0668 0.1908 0.086 Uiso 0.404(13) 1 calc PR F 2
H20E H 0.1678 0.0139 0.1641 0.086 Uiso 0.404(13) 1 calc PR F 2
C203 C 0.0941(7) 0.0271(18) 0.0887(6) 0.073(5) Uani 0.404(13) 1 d PDU F 2
H20F H 0.1061 -0.0331 0.0980 0.087 Uiso 0.404(13) 1 calc PR F 2
H20G H 0.0798 0.0454 0.1040 0.087 Uiso 0.404(13) 1 calc PR F 2
C204 C 0.0679(6) 0.014(2) 0.0495(8) 0.073(5) Uani 0.404(13) 1 d PDU F 2
H20H H 0.0790 0.0403 0.0327 0.110 Uiso 0.404(13) 1 calc PR F 2
H20I H 0.0448 0.0462 0.0462 0.110 Uiso 0.404(13) 1 calc PR F 2
H20J H 0.0632 -0.0520 0.0444 0.110 Uiso 0.404(13) 1 calc PR F 2
C205 C 0.1642(7) 0.053(2) 0.0805(12) 0.092(7) Uani 0.404(13) 1 d PDU F 2
H20K H 0.1708 -0.0055 0.0947 0.110 Uiso 0.404(13) 1 calc PR F 2
H20L H 0.1535 0.0361 0.0543 0.110 Uiso 0.404(13) 1 calc PR F 2
C206 C 0.1990(6) 0.109(3) 0.0869(14) 0.092(7) Uani 0.404(13) 1 d PDU F 2
H20M H 0.1929 0.1661 0.0723 0.138 Uiso 0.404(13) 1 calc PR F 2
H20N H 0.2164 0.0724 0.0796 0.138 Uiso 0.404(13) 1 calc PR F 2
H20O H 0.2101 0.1251 0.1128 0.138 Uiso 0.404(13) 1 calc PR F 2
C107 C 0.1010(11) 0.4561(14) 0.0197(17) 0.091(6) Uani 0.57(3) 1 d PDU F 1
H10P H 0.0854 0.5074 0.0057 0.109 Uiso 0.57(3) 1 calc PR F 1
H10Q H 0.1119 0.4761 0.0455 0.109 Uiso 0.57(3) 1 calc PR F 1
C108 C 0.1317(7) 0.439(2) 0.0050(10) 0.092(6) Uani 0.57(3) 1 d PDU F 1
H10R H 0.1357 0.3722 0.0039 0.139 Uiso 0.57(3) 1 calc PR F 1
H10S H 0.1544 0.4684 0.0213 0.139 Uiso 0.57(3) 1 calc PR F 1
H10T H 0.1250 0.4656 -0.0195 0.139 Uiso 0.57(3) 1 calc PR F 1
C109 C 0.0571(8) 0.3342(18) -0.03225(18) 0.065(5) Uani 0.57(3) 1 d PDU F 1
H10U H 0.0788 0.3364 -0.0398 0.078 Uiso 0.57(3) 1 calc PR F 1
H10V H 0.0464 0.2713 -0.0376 0.078 Uiso 0.57(3) 1 calc PR F 1
C110 C 0.0289(8) 0.404(2) -0.0547(3) 0.065(5) Uani 0.57(3) 1 d PDU F 1
H11A H 0.0067 0.4002 -0.0484 0.098 Uiso 0.57(3) 1 calc PR F 1
H11B H 0.0226 0.3911 -0.0808 0.098 Uiso 0.57(3) 1 calc PR F 1
H11C H 0.0392 0.4671 -0.0494 0.098 Uiso 0.57(3) 1 calc PR F 1
C111 C 0.0333(8) 0.400(2) 0.0276(16) 0.056(5) Uani 0.57(3) 1 d PDU F 1
H11D H 0.0416 0.4147 0.0540 0.067 Uiso 0.57(3) 1 calc PR F 1
H11E H 0.0248 0.4582 0.0138 0.067 Uiso 0.57(3) 1 calc PR F 1
C112 C 0.0011(5) 0.333(2) 0.0183(12) 0.056(5) Uani 0.57(3) 1 d PDU F 1
H11F H -0.0109 0.3286 -0.0083 0.083 Uiso 0.57(3) 1 calc PR F 1
H11G H -0.0166 0.3552 0.0290 0.083 Uiso 0.57(3) 1 calc PR F 1
H11H H 0.0100 0.2713 0.0282 0.083 Uiso 0.57(3) 1 calc PR F 1
C207 C 0.1074(10) 0.443(3) 0.023(2) 0.091(6) Uani 0.43(3) 1 d PDU F 2
H20P H 0.0987 0.4873 0.0022 0.110 Uiso 0.43(3) 1 calc PR F 2
H20Q H 0.1107 0.4783 0.0456 0.110 Uiso 0.43(3) 1 calc PR F 2
C208 C 0.1443(5) 0.404(3) 0.0250(13) 0.092(6) Uani 0.43(3) 1 d PDU F 2
H20R H 0.1520 0.3558 0.0439 0.137 Uiso 0.43(3) 1 calc PR F 2
H20S H 0.1626 0.4535 0.0311 0.137 Uiso 0.43(3) 1 calc PR F 2
H20T H 0.1420 0.3767 0.0014 0.137 Uiso 0.43(3) 1 calc PR F 2
C209 C 0.0476(12) 0.3263(18) -0.0311(2) 0.065(5) Uani 0.43(3) 1 d PDU F 2
H20U H 0.0610 0.2764 -0.0384 0.078 Uiso 0.43(3) 1 calc PR F 2
H20V H 0.0230 0.3021 -0.0339 0.078 Uiso 0.43(3) 1 calc PR F 2
C210 C 0.0432(12) 0.409(2) -0.0566(3) 0.065(5) Uani 0.43(3) 1 d PDU F 2
H21C H 0.0172 0.4157 -0.0719 0.098 Uiso 0.43(3) 1 calc PR F 2
H21D H 0.0576 0.3980 -0.0723 0.098 Uiso 0.43(3) 1 calc PR F 2
H21E H 0.0518 0.4650 -0.0422 0.098 Uiso 0.43(3) 1 calc PR F 2
C211 C 0.0368(10) 0.420(2) 0.027(2) 0.055(5) Uani 0.43(3) 1 d PDU F 2
H21F H 0.0471 0.4426 0.0526 0.066 Uiso 0.43(3) 1 calc PR F 2
H21G H 0.0301 0.4749 0.0109 0.066 Uiso 0.43(3) 1 calc PR F 2
C212 C 0.0023(7) 0.364(3) 0.0222(16) 0.055(5) Uani 0.43(3) 1 d PDU F 2
H21H H -0.0092 0.3455 -0.0034 0.083 Uiso 0.43(3) 1 calc PR F 2
H21I H -0.0150 0.4017 0.0294 0.083 Uiso 0.43(3) 1 calc PR F 2
H21J H 0.0088 0.3083 0.0376 0.083 Uiso 0.43(3) 1 calc PR F 2
C113 C 0.1542(10) 0.6903(17) 0.0756(4) 0.084(6) Uani 0.539(10) 1 d PDU G 1
H11I H 0.1801 0.6844 0.0774 0.101 Uiso 0.539(10) 1 calc PR G 1
H11J H 0.1404 0.6375 0.0609 0.101 Uiso 0.539(10) 1 calc PR G 1
C114 C 0.1386(8) 0.7801(19) 0.0558(5) 0.085(6) Uani 0.539(10) 1 d PDU G 1
H11K H 0.1168 0.7979 0.0613 0.127 Uiso 0.539(10) 1 calc PR G 1
H11L H 0.1318 0.7710 0.0294 0.127 Uiso 0.539(10) 1 calc PR G 1
H11M H 0.1571 0.8292 0.0640 0.127 Uiso 0.539(10) 1 calc PR G 1
C115 C 0.1038(2) 0.6500(13) 0.1073(8) 0.073(5) Uani 0.539(10) 1 d PDU G 1
H11N H 0.0991 0.5982 0.0896 0.088 Uiso 0.539(10) 1 calc PR G 1
H11O H 0.0987 0.6274 0.1289 0.088 Uiso 0.539(10) 1 calc PR G 1
C116 C 0.0776(2) 0.7290(18) 0.0898(7) 0.074(5) Uani 0.539(10) 1 d PDU G 1
H11P H 0.0857 0.7854 0.1044 0.111 Uiso 0.539(10) 1 calc PR G 1
H11Q H 0.0528 0.7126 0.0888 0.111 Uiso 0.539(10) 1 calc PR G 1
H11R H 0.0773 0.7398 0.0650 0.111 Uiso 0.539(10) 1 calc PR G 1
C117 C 0.1534(5) 0.7670(14) 0.1568(5) 0.061(4) Uani 0.539(10) 1 d PDU G 1
H11S H 0.1352 0.8165 0.1456 0.073 Uiso 0.539(10) 1 calc PR G 1
H11T H 0.1459 0.7357 0.1755 0.073 Uiso 0.539(10) 1 calc PR G 1
C118 C 0.1909(6) 0.8112(15) 0.1753(7) 0.062(4) Uani 0.539(10) 1 d PDU G 1
H11U H 0.2092 0.7626 0.1858 0.094 Uiso 0.539(10) 1 calc PR G 1
H11V H 0.1900 0.8529 0.1947 0.094 Uiso 0.539(10) 1 calc PR G 1
H11W H 0.1977 0.8465 0.1572 0.094 Uiso 0.539(10) 1 calc PR G 1
C213 C 0.1533(12) 0.7426(15) 0.0807(5) 0.082(7) Uani 0.461(10) 1 d PDU G 2
H21K H 0.1359 0.7953 0.0753 0.099 Uiso 0.461(10) 1 calc PR G 2
H21L H 0.1782 0.7683 0.0859 0.099 Uiso 0.461(10) 1 calc PR G 2
C214 C 0.1434(9) 0.680(2) 0.0472(3) 0.083(6) Uani 0.461(10) 1 d PDU G 2
H21M H 0.1590 0.6250 0.0531 0.124 Uiso 0.461(10) 1 calc PR G 2
H21N H 0.1473 0.7143 0.0272 0.124 Uiso 0.461(10) 1 calc PR G 2
H21O H 0.1176 0.6619 0.0398 0.124 Uiso 0.461(10) 1 calc PR G 2
C215 C 0.1084(3) 0.7211(19) 0.1235(8) 0.075(5) Uani 0.461(10) 1 d PDU G 2
H21P H 0.1084 0.7103 0.1485 0.090 Uiso 0.461(10) 1 calc PR G 2
H21Q H 0.1058 0.7887 0.1187 0.090 Uiso 0.461(10) 1 calc PR G 2
C216 C 0.07547(19) 0.672(2) 0.0962(9) 0.075(5) Uani 0.461(10) 1 d PDU G 2
H21R H 0.0806 0.6579 0.0739 0.112 Uiso 0.461(10) 1 calc PR G 2
H21S H 0.0538 0.7118 0.0901 0.112 Uiso 0.461(10) 1 calc PR G 2
H21T H 0.0709 0.6139 0.1069 0.112 Uiso 0.461(10) 1 calc PR G 2
C217 C 0.1836(6) 0.7805(13) 0.1391(6) 0.063(4) Uani 0.461(10) 1 d PDU G 2
H21U H 0.2045 0.7746 0.1303 0.076 Uiso 0.461(10) 1 calc PR G 2
H21V H 0.1705 0.8388 0.1290 0.076 Uiso 0.461(10) 1 calc PR G 2
C218 C 0.1987(8) 0.7865(18) 0.1806(6) 0.062(5) Uani 0.461(10) 1 d PDU G 2
H916 H 0.1782 0.7884 0.1896 0.093 Uiso 0.461(10) 1 calc PR G 2
H917 H 0.2135 0.8430 0.1882 0.093 Uiso 0.461(10) 1 calc PR G 2
H918 H 0.2140 0.7321 0.1907 0.093 Uiso 0.461(10) 1 calc PR G 2
C119 C 0.2737(2) 0.458(3) 0.1970(10) 0.071(5) Uani 0.542(17) 1 d PDU G 1
H914 H 0.2853 0.4032 0.2121 0.085 Uiso 0.542(17) 1 calc PR G 1
H915 H 0.2864 0.4684 0.1795 0.085 Uiso 0.542(17) 1 calc PR G 1
C120 C 0.2793(8) 0.5421(17) 0.2218(11) 0.070(5) Uani 0.542(17) 1 d PDU G 1
H12A H 0.2612 0.5898 0.2095 0.105 Uiso 0.542(17) 1 calc PR G 1
H12B H 0.3041 0.5668 0.2271 0.105 Uiso 0.542(17) 1 calc PR G 1
H12C H 0.2762 0.5241 0.2446 0.105 Uiso 0.542(17) 1 calc PR G 1
C121 C 0.2206(12) 0.3464(14) 0.1356(6) 0.075(7) Uani 0.542(17) 1 d PDU G 1
H12D H 0.2378 0.2945 0.1459 0.090 Uiso 0.542(17) 1 calc PR G 1
H12E H 0.1954 0.3210 0.1271 0.090 Uiso 0.542(17) 1 calc PR G 1
C122 C 0.2282(10) 0.386(3) 0.1029(4) 0.074(7) Uani 0.542(17) 1 d PDU G 1
H12F H 0.2115 0.4381 0.0927 0.111 Uiso 0.542(17) 1 calc PR G 1
H12G H 0.2242 0.3377 0.0843 0.111 Uiso 0.542(17) 1 calc PR G 1
H12H H 0.2537 0.4077 0.1108 0.111 Uiso 0.542(17) 1 calc PR G 1
C123 C 0.2069(6) 0.3636(19) 0.2005(8) 0.079(5) Uani 0.542(17) 1 d PDU G 1
H12I H 0.2020 0.4057 0.2182 0.094 Uiso 0.542(17) 1 calc PR G 1
H12J H 0.1833 0.3359 0.1850 0.094 Uiso 0.542(17) 1 calc PR G 1
C124 C 0.2325(8) 0.2867(15) 0.2215(7) 0.079(5) Uani 0.542(17) 1 d PDU G 1
H12K H 0.2291 0.2319 0.2058 0.118 Uiso 0.542(17) 1 calc PR G 1
H12L H 0.2269 0.2708 0.2433 0.118 Uiso 0.542(17) 1 calc PR G 1
H12M H 0.2580 0.3078 0.2289 0.118 Uiso 0.542(17) 1 calc PR G 1
C219 C 0.2742(4) 0.462(4) 0.1898(10) 0.070(5) Uani 0.458(17) 1 d PDU G 2
H919 H 0.2889 0.4040 0.1942 0.084 Uiso 0.458(17) 1 calc PR G 2
H920 H 0.2801 0.4985 0.1713 0.084 Uiso 0.458(17) 1 calc PR G 2
C220 C 0.2852(8) 0.517(2) 0.2253(12) 0.070(5) Uani 0.458(17) 1 d PDU G 2
H22D H 0.2760 0.5805 0.2200 0.105 Uiso 0.458(17) 1 calc PR G 2
H22E H 0.3120 0.5178 0.2367 0.105 Uiso 0.458(17) 1 calc PR G 2
H22F H 0.2747 0.4877 0.2419 0.105 Uiso 0.458(17) 1 calc PR G 2
C221 C 0.2300(15) 0.3345(14) 0.1435(9) 0.075(7) Uani 0.458(17) 1 d PDU G 2
H22G H 0.2482 0.2900 0.1592 0.090 Uiso 0.458(17) 1 calc PR G 2
H22H H 0.2061 0.3020 0.1334 0.090 Uiso 0.458(17) 1 calc PR G 2
C222 C 0.2421(12) 0.364(3) 0.1121(6) 0.074(7) Uani 0.458(17) 1 d PDU G 2
H22I H 0.2224 0.3993 0.0943 0.111 Uiso 0.458(17) 1 calc PR G 2
H22J H 0.2474 0.3082 0.1003 0.111 Uiso 0.458(17) 1 calc PR G 2
H22K H 0.2642 0.4020 0.1216 0.111 Uiso 0.458(17) 1 calc PR G 2
C223 C 0.2226(9) 0.378(2) 0.2127(4) 0.079(5) Uani 0.458(17) 1 d PDU G 2
H22L H 0.2466 0.3487 0.2266 0.094 Uiso 0.458(17) 1 calc PR G 2
H22M H 0.2180 0.4263 0.2283 0.094 Uiso 0.458(17) 1 calc PR G 2
C224 C 0.1928(8) 0.304(2) 0.2049(8) 0.079(5) Uani 0.458(17) 1 d PDU G 2
H22N H 0.1853 0.2975 0.2262 0.118 Uiso 0.458(17) 1 calc PR G 2
H22O H 0.2022 0.2448 0.1998 0.118 Uiso 0.458(17) 1 calc PR G 2
H22P H 0.1715 0.3229 0.1836 0.118 Uiso 0.458(17) 1 calc PR G 2
C125 C 0.0667(4) 0.7147(10) 0.1984(4) 0.058(4) Uani 1 1 d . . .
H12N H 0.0589 0.7774 0.1884 0.070 Uiso 1 1 calc R . .
H12O H 0.0841 0.6911 0.1873 0.070 Uiso 1 1 calc R . .
C126 C 0.0334(4) 0.6526(10) 0.1867(4) 0.060(4) Uani 1 1 d . . .
H12P H 0.0401 0.5915 0.1981 0.090 Uiso 1 1 calc R . .
H12Q H 0.0241 0.6461 0.1601 0.090 Uiso 1 1 calc R . .
H12R H 0.0143 0.6800 0.1944 0.090 Uiso 1 1 calc R . .
C127 C 0.1067(4) 0.8466(8) 0.2530(4) 0.056(4) Uani 1 1 d . . .
H12S H 0.0852 0.8877 0.2423 0.067 Uiso 1 1 calc R . .
H12T H 0.1184 0.8623 0.2793 0.067 Uiso 1 1 calc R . .
C128 C 0.1345(4) 0.8643(10) 0.2336(4) 0.070(4) Uani 1 1 d . . .
H12U H 0.1549 0.8202 0.2427 0.105 Uiso 1 1 calc R . .
H12V H 0.1440 0.9278 0.2386 0.105 Uiso 1 1 calc R . .
H12W H 0.1222 0.8561 0.2072 0.105 Uiso 1 1 calc R . .
C129 C 0.0545(4) 0.7285(11) 0.2671(4) 0.060(4) Uani 1 1 d . . .
H929 H 0.0365 0.7765 0.2540 0.072 Uiso 1 1 calc R . .
H930 H 0.0417 0.6679 0.2625 0.072 Uiso 1 1 calc R . .
C130 C 0.0677(5) 0.7489(12) 0.3077(4) 0.079(5) Uani 1 1 d . . .
H13A H 0.0859 0.7022 0.3209 0.119 Uiso 1 1 calc R . .
H13B H 0.0468 0.7471 0.3160 0.119 Uiso 1 1 calc R . .
H13C H 0.0790 0.8106 0.3123 0.119 Uiso 1 1 calc R . .
C131 C 0.2276(4) 0.5538(14) 0.3215(5) 0.099(6) Uani 1 1 d DU . .
H931 H 0.2299 0.6188 0.3301 0.119 Uiso 0.59(4) 1 calc PR H 1
H932 H 0.2440 0.5154 0.3417 0.119 Uiso 0.59(4) 1 calc PR H 1
H933 H 0.2349 0.5983 0.3421 0.119 Uiso 0.41(4) 1 calc PR H 2
H934 H 0.2445 0.4999 0.3283 0.119 Uiso 0.41(4) 1 calc PR H 2
C132 C 0.2405(9) 0.548(3) 0.2892(7) 0.098(6) Uani 0.59(4) 1 d PDU H 1
H13F H 0.2266 0.5917 0.2703 0.147 Uiso 0.59(4) 1 calc PR H 1
H13G H 0.2365 0.4846 0.2792 0.147 Uiso 0.59(4) 1 calc PR H 1
H13H H 0.2667 0.5626 0.2973 0.147 Uiso 0.59(4) 1 calc PR H 1
C232 C 0.2292(14) 0.600(4) 0.2871(9) 0.099(6) Uani 0.41(4) 1 d PDU H 2
H23C H 0.2522 0.6347 0.2932 0.148 Uiso 0.41(4) 1 calc PR H 2
H23D H 0.2083 0.6420 0.2771 0.148 Uiso 0.41(4) 1 calc PR H 2
H23E H 0.2282 0.5521 0.2689 0.148 Uiso 0.41(4) 1 calc PR H 2
C133 C 0.1787(4) 0.5033(12) 0.3577(4) 0.073(5) Uani 1 1 d . . .
H13I H 0.1973 0.4572 0.3716 0.087 Uiso 1 1 calc R H .
H13J H 0.1849 0.5635 0.3707 0.087 Uiso 1 1 calc R . .
C134 C 0.1414(5) 0.4727(13) 0.3562(4) 0.084(5) Uani 1 1 d . H .
H13K H 0.1230 0.5185 0.3426 0.125 Uiso 1 1 calc R . .
H13L H 0.1412 0.4671 0.3811 0.125 Uiso 1 1 calc R . .
H13M H 0.1355 0.4125 0.3439 0.125 Uiso 1 1 calc R . .
C135 C 0.1786(4) 0.3990(10) 0.2930(4) 0.066(4) Uani 1 1 d . . .
H13N H 0.1537 0.3735 0.2882 0.080 Uiso 1 1 calc R H .
H13O H 0.1819 0.4039 0.2692 0.080 Uiso 1 1 calc R . .
C136 C 0.2065(4) 0.3292(13) 0.3166(5) 0.102(7) Uani 1 1 d . H .
H13P H 0.2314 0.3528 0.3215 0.154 Uiso 1 1 calc R . .
H13Q H 0.2035 0.2698 0.3036 0.154 Uiso 1 1 calc R . .
H13R H 0.2026 0.3201 0.3398 0.154 Uiso 1 1 calc R . .
C137 C -0.0138(3) 0.4779(9) 0.2383(4) 0.046(3) Uani 1 1 d . . .
H13S H -0.0290 0.5253 0.2446 0.055 Uiso 1 1 calc R . .
H13T H 0.0099 0.5074 0.2408 0.055 Uiso 1 1 calc R . .
C138 C -0.0329(4) 0.4511(12) 0.1990(4) 0.078(5) Uani 1 1 d . . .
H13U H -0.0185 0.4033 0.1923 0.118 Uiso 1 1 calc R . .
H13V H -0.0352 0.5057 0.1834 0.118 Uiso 1 1 calc R . .
H13W H -0.0574 0.4266 0.1956 0.118 Uiso 1 1 calc R . .
C139 C 0.0026(4) 0.4475(10) 0.3137(3) 0.055(4) Uani 1 1 d . . .
H939 H -0.0168 0.4952 0.3093 0.066 Uiso 1 1 calc R . .
H940 H 0.0002 0.4037 0.3322 0.066 Uiso 1 1 calc R . .
C140 C 0.0392(4) 0.4935(11) 0.3286(4) 0.071(5) Uani 1 1 d . . .
H14A H 0.0586 0.4468 0.3329 0.106 Uiso 1 1 calc R . .
H14B H 0.0418 0.5243 0.3517 0.106 Uiso 1 1 calc R . .
H14C H 0.0414 0.5395 0.3111 0.106 Uiso 1 1 calc R . .
C141 C -0.0494(4) 0.3251(11) 0.2608(4) 0.066(4) Uani 1 1 d . . .
H14D H -0.0550 0.2934 0.2370 0.079 Uiso 1 1 calc R . .
H14E H -0.0462 0.2763 0.2795 0.079 Uiso 1 1 calc R . .
C142 C -0.0811(5) 0.3798(12) 0.2590(6) 0.096(6) Uani 1 1 d . . .
H14F H -0.0850 0.4286 0.2405 0.144 Uiso 1 1 calc R . .
H14G H -0.0771 0.4081 0.2829 0.144 Uiso 1 1 calc R . .
H14H H -0.1029 0.3397 0.2522 0.144 Uiso 1 1 calc R . .
C143 C 0.1238(4) 0.1800(12) 0.3239(4) 0.066(4) Uani 1 1 d . . .
H14I H 0.1355 0.2379 0.3198 0.079 Uiso 1 1 calc R . .
H14J H 0.1164 0.1905 0.3453 0.079 Uiso 1 1 calc R . .
C144 C 0.1528(4) 0.1031(14) 0.3337(5) 0.097(6) Uani 1 1 d . . .
H14K H 0.1414 0.0442 0.3363 0.146 Uiso 1 1 calc R . .
H14L H 0.1725 0.1185 0.3568 0.146 Uiso 1 1 calc R . .
H14M H 0.1631 0.0975 0.3143 0.146 Uiso 1 1 calc R . .
C145 C 0.0646(4) 0.0484(9) 0.2933(4) 0.056(4) Uani 1 1 d . . .
H14N H 0.0831 -0.0005 0.2953 0.067 Uiso 1 1 calc R . .
H14O H 0.0610 0.0522 0.3171 0.067 Uiso 1 1 calc R . .
C146 C 0.0282(4) 0.0210(11) 0.2636(4) 0.068(4) Uani 1 1 d . . .
H14P H 0.0089 0.0639 0.2641 0.102 Uiso 1 1 calc R . .
H14Q H 0.0217 -0.0423 0.2681 0.102 Uiso 1 1 calc R . .
H14R H 0.0308 0.0240 0.2396 0.102 Uiso 1 1 calc R . .
C147 C 0.0986(4) 0.1304(9) 0.2471(3) 0.049(3) Uani 1 1 d . . .
H14S H 0.1127 0.0717 0.2537 0.058 Uiso 1 1 calc R . .
H14T H 0.0771 0.1186 0.2247 0.058 Uiso 1 1 calc R . .
C148 C 0.1230(4) 0.2037(10) 0.2384(4) 0.057(4) Uani 1 1 d . . .
H14U H 0.1103 0.2637 0.2340 0.085 Uiso 1 1 calc R . .
H14V H 0.1280 0.1850 0.2166 0.085 Uiso 1 1 calc R . .
H14W H 0.1462 0.2092 0.2591 0.085 Uiso 1 1 calc R . .
C149 C -0.0807(4) -0.0941(10) 0.0971(4) 0.056(4) Uani 1 1 d . . .
H949 H -0.0964 -0.0471 0.1028 0.067 Uiso 1 1 calc R . .
H950 H -0.0839 -0.0867 0.0710 0.067 Uiso 1 1 calc R . .
C150 C -0.0948(4) -0.1904(11) 0.1022(5) 0.082(5) Uani 1 1 d . . .
H15A H -0.0789 -0.2380 0.0977 0.124 Uiso 1 1 calc R . .
H15B H -0.1200 -0.1984 0.0849 0.124 Uiso 1 1 calc R . .
H15C H -0.0945 -0.1965 0.1272 0.124 Uiso 1 1 calc R . .
C151 C -0.0277(4) -0.1116(11) 0.1693(4) 0.066(4) Uani 1 1 d . . .
H15D H -0.0350 -0.1778 0.1671 0.079 Uiso 1 1 calc R . .
H15E H -0.0015 -0.1081 0.1852 0.079 Uiso 1 1 calc R . .
C152 C -0.0500(5) -0.0607(13) 0.1877(4) 0.084(5) Uani 1 1 d . . .
H15F H -0.0423 0.0045 0.1912 0.126 Uiso 1 1 calc R . .
H15G H -0.0461 -0.0890 0.2116 0.126 Uiso 1 1 calc R . .
H15H H -0.0761 -0.0641 0.1725 0.126 Uiso 1 1 calc R . .
C153 C -0.0083(4) -0.1508(10) 0.1061(4) 0.060(4) Uani 1 1 d . . .
H15I H 0.0169 -0.1602 0.1239 0.072 Uiso 1 1 calc R . .
H15J H -0.0211 -0.2113 0.1020 0.072 Uiso 1 1 calc R . .
C154 C -0.0062(5) -0.1157(11) 0.0699(5) 0.080(5) Uani 1 1 d . . .
H15K H -0.0311 -0.1117 0.0516 0.121 Uiso 1 1 calc R . .
H15L H 0.0085 -0.1586 0.0614 0.121 Uiso 1 1 calc R . .
H15M H 0.0052 -0.0541 0.0736 0.121 Uiso 1 1 calc R . .
C155 C -0.0465(4) 0.2845(9) 0.0923(4) 0.066(4) Uani 1 1 d . . .
H15N H -0.0360 0.3131 0.1168 0.079 Uiso 1 1 calc R . .
H15O H -0.0280 0.2904 0.0804 0.079 Uiso 1 1 calc R . .
C156 C -0.0813(4) 0.3400(11) 0.0694(6) 0.108(8) Uani 1 1 d . . .
H15P H -0.0898 0.3185 0.0440 0.163 Uiso 1 1 calc R . .
H15Q H -0.0753 0.4062 0.0703 0.163 Uiso 1 1 calc R . .
H15R H -0.1007 0.3301 0.0796 0.163 Uiso 1 1 calc R . .
C157 C -0.0784(4) 0.1213(11) 0.0510(4) 0.062(4) Uani 1 1 d . . .
H15S H -0.0852 0.0553 0.0516 0.074 Uiso 1 1 calc R . .
H15T H -0.1014 0.1574 0.0402 0.074 Uiso 1 1 calc R . .
C158 C -0.0556(5) 0.1310(15) 0.0268(5) 0.106(7) Uani 1 1 d . . .
H15U H -0.0497 0.1965 0.0251 0.159 Uiso 1 1 calc R . .
H15V H -0.0695 0.1071 0.0023 0.159 Uiso 1 1 calc R . .
H15W H -0.0328 0.0955 0.0373 0.159 Uiso 1 1 calc R . .
C159 C -0.0891(4) 0.1615(11) 0.1184(4) 0.068(4) Uani 1 1 d . . .
H959 H -0.1117 0.1907 0.1013 0.082 Uiso 1 1 calc R . .
H960 H -0.0951 0.0966 0.1224 0.082 Uiso 1 1 calc R . .
C160 C -0.0771(4) 0.2138(13) 0.1551(5) 0.091(6) Uani 1 1 d . . .
H16A H -0.0504 0.2094 0.1671 0.136 Uiso 1 1 calc R . .
H16B H -0.0891 0.1861 0.1708 0.136 Uiso 1 1 calc R . .
H16C H -0.0843 0.2791 0.1507 0.136 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 640 0.0033 0.0016
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
H H 1240 0.0000 0.0000
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
Cl Cl 40 0.1484 0.1585
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
P P 80 0.1023 0.0942
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
Pt Pt 40 -1.7033 8.3905
; International Tables for Crystallography (1992).
Vol. C, Tables 4.2.6.8 and 6.1.1.4
;
loop_
_diffrn_standard_refln_index_h
_diffrn_standard_refln_index_k
_diffrn_standard_refln_index_l
? ? ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C7 Pt1 P2 91.2(3) . . ?
C7 Pt1 P1 89.9(3) . . ?
P2 Pt1 P1 174.83(14) . . ?
C7 Pt1 Cl1 178.9(4) . . ?
P2 Pt1 Cl1 88.49(14) . . ?
P1 Pt1 Cl1 90.25(14) . . ?
C10 Pt2 P3 89.9(3) . . ?
C10 Pt2 P4 92.5(3) . . ?
P3 Pt2 P4 170.39(17) . . ?
C10 Pt2 Cl2 179.2(4) . . ?
P3 Pt2 Cl2 89.50(14) . . ?
P4 Pt2 Cl2 88.15(13) . . ?
C13 Pt3 P5 88.0(3) . . ?
C13 Pt3 P6 172.8(3) . . ?
P5 Pt3 P6 99.18(12) . . ?
C13 Pt3 Cl3 87.4(3) . . ?
P5 Pt3 Cl3 172.96(13) . . ?
P6 Pt3 Cl3 85.40(11) . . ?
C16 Pt4 P8 91.3(4) . . ?
C16 Pt4 P7 87.0(4) . . ?
P8 Pt4 P7 175.25(13) . . ?
C16 Pt4 Cl4 178.2(4) . . ?
P8 Pt4 Cl4 90.40(12) . . ?
P7 Pt4 Cl4 91.24(12) . . ?
C19 Pt5 P9 93.0(3) . . ?
C19 Pt5 P10 87.1(3) . . ?
P9 Pt5 P10 178.96(15) . . ?
C19 Pt5 Cl5 175.9(4) . . ?
P9 Pt5 Cl5 90.70(12) . . ?
P10 Pt5 Cl5 89.26(13) . . ?
C23 P1 C21 103.1(8) . . ?
C23 P1 C25 103.7(7) . . ?
C21 P1 C25 101.6(8) . . ?
C23 P1 Pt1 114.8(6) . . ?
C21 P1 Pt1 112.0(6) . . ?
C25 P1 Pt1 119.6(4) . . ?
C27B P2 C29B 107(4) . . ?
C27B P2 C31B 93(3) . . ?
C29B P2 C31B 106(2) . . ?
C27A P2 C29A 103(2) . . ?
C27B P2 C29A 98(3) . . ?
C27A P2 C31A 113(2) . . ?
C29A P2 C31A 103.0(9) . . ?
C27A P2 Pt1 114.9(11) . . ?
C27B P2 Pt1 119.2(14) . . ?
C29B P2 Pt1 115(3) . . ?
C31B P2 Pt1 114.1(17) . . ?
C29A P2 Pt1 111(2) . . ?
C31A P2 Pt1 111.1(11) . . ?
C37A P3 C33A 107.5(16) . . ?
C35B P3 C33B 129(5) . . ?
C35B P3 C37B 108(3) . . ?
C33B P3 C37B 80(4) . . ?
C37A P3 C35A 99.5(7) . . ?
C33A P3 C35A 105.2(18) . . ?
C37A P3 Pt2 116.5(10) . . ?
C35B P3 Pt2 108(3) . . ?
C33A P3 Pt2 116.4(7) . . ?
C33B P3 Pt2 119(3) . . ?
C37B P3 Pt2 104(2) . . ?
C35A P3 Pt2 109.9(10) . . ?
C39 P4 C43 104.0(7) . . ?
C39 P4 C41 104.7(6) . . ?
C43 P4 C41 103.2(8) . . ?
C39 P4 Pt2 114.1(5) . . ?
C43 P4 Pt2 109.5(5) . . ?
C41 P4 Pt2 119.7(5) . . ?
C45B P5 C47B 105(4) . . ?
C45A P5 C47A 103(3) . . ?
C45B P5 C49B 95(2) . . ?
C47B P5 C49B 107(4) . . ?
C45A P5 C49A 113.9(15) . . ?
C47A P5 C49A 97(3) . . ?
C45A P5 Pt3 114(2) . . ?
C45B P5 Pt3 117(3) . . ?
C47B P5 Pt3 116.4(16) . . ?
C47A P5 Pt3 117.1(9) . . ?
C49B P5 Pt3 114(3) . . ?
C49A P5 Pt3 111(2) . . ?
C53 P6 C55 104.9(6) . . ?
C53 P6 C51 101.8(6) . . ?
C55 P6 C51 103.0(6) . . ?
C53 P6 Pt3 109.4(4) . . ?
C55 P6 Pt3 110.8(4) . . ?
C51 P6 Pt3 125.0(5) . . ?
C57B P7 C59B 111(4) . . ?
C59A P7 C61A 108(3) . . ?
C59A P7 C57A 101(2) . . ?
C61A P7 C57A 102.1(10) . . ?
C57B P7 C61B 104.3(13) . . ?
C59B P7 C61B 101(4) . . ?
C57B P7 Pt4 114(2) . . ?
C59A P7 Pt4 114.9(9) . . ?
C59B P7 Pt4 114.8(14) . . ?
C61A P7 Pt4 113.9(17) . . ?
C57A P7 Pt4 115.4(15) . . ?
C61B P7 Pt4 111(3) . . ?
C65A P8 C67A 109.1(10) . . ?
C67B P8 C63B 109.5(13) . . ?
C67B P8 C65B 98.6(11) . . ?
C63B P8 C65B 101.8(11) . . ?
C65A P8 C63A 103.8(10) . . ?
C67A P8 C63A 97.6(9) . . ?
C65A P8 Pt4 115.4(7) . . ?
C67B P8 Pt4 118.7(7) . . ?
C67A P8 Pt4 116.5(6) . . ?
C63B P8 Pt4 115.5(10) . . ?
C65B P8 Pt4 110.0(7) . . ?
C63A P8 Pt4 112.3(7) . . ?
C71 P9 C73 111.3(11) . . ?
C71 P9 C69 102.7(10) . . ?
C73 P9 C69 97.1(10) . . ?
C71 P9 Pt5 115.0(7) . . ?
C73 P9 Pt5 115.0(6) . . ?
C69 P9 Pt5 113.8(7) . . ?
C79B P10 C77B 100.0(18) . . ?
C79A P10 C75A 115.7(11) . . ?
C79A P10 C77A 102.3(14) . . ?
C75A P10 C77A 99.8(11) . . ?
C79B P10 C75B 83.5(16) . . ?
C77B P10 C75B 104.5(13) . . ?
C79A P10 Pt5 115.7(12) . . ?
C79B P10 Pt5 123.5(11) . . ?
C77B P10 Pt5 129.4(11) . . ?
C75A P10 Pt5 111.8(7) . . ?
C77A P10 Pt5 109.6(6) . . ?
C75B P10 Pt5 104.7(9) . . ?
C6 C1 C5 124.7(12) . . ?
C6 C1 C2 126.4(12) . . ?
C5 C1 C2 104.6(9) . . ?
C3 C2 C9 127.3(12) . . ?
C3 C2 C1 107.7(10) . . ?
C9 C2 C1 118.8(11) . . ?
C4 C3 C2 109.1(10) . . ?
C4 C3 C12 126.8(11) . . ?
C2 C3 C12 119.6(12) . . ?
C5 C4 C3 109.1(10) . . ?
C5 C4 C15 124.1(12) . . ?
C3 C4 C15 121.8(12) . . ?
C4 C5 C18 125.1(12) . . ?
C4 C5 C1 109.5(10) . . ?
C18 C5 C1 120.7(12) . . ?
C1 C6 C7 113.3(13) . . ?
C1 C6 C20 113.7(12) . . ?
C7 C6 C20 132.6(13) . . ?
C6 C7 C8 122.3(13) . . ?
C6 C7 Pt1 119.2(11) . . ?
C8 C7 Pt1 118.5(9) . . ?
C9 C8 C7 119.9(11) . . ?
C9 C8 H8 120.0 . . ?
C7 C8 H8 120.0 . . ?
C2 C9 C10 113.7(12) . . ?
C2 C9 C8 116.8(12) . . ?
C10 C9 C8 128.7(12) . . ?
C9 C10 C11 119.0(13) . . ?
C9 C10 Pt2 119.1(10) . . ?
C11 C10 Pt2 121.8(10) . . ?
C12 C11 C10 124.5(12) . . ?
C12 C11 H11 117.7 . . ?
C10 C11 H11 117.7 . . ?
C11 C12 C13 134.5(13) . . ?
C11 C12 C3 114.9(11) . . ?
C13 C12 C3 109.7(11) . . ?
C14 C13 C12 122.8(12) . . ?
C14 C13 Pt3 123.2(9) . . ?
C12 C13 Pt3 114.0(10) . . ?
C15 C14 C13 123.9(11) . . ?
C15 C14 H14 118.0 . . ?
C13 C14 H14 118.0 . . ?
C14 C15 C4 112.7(11) . . ?
C14 C15 C16 132.4(12) . . ?
C4 C15 C16 114.3(12) . . ?
C15 C16 C17 119.3(12) . . ?
C15 C16 Pt4 119.0(10) . . ?
C17 C16 Pt4 121.7(9) . . ?
C18 C17 C16 123.6(11) . . ?
C18 C17 H17 118.2 . . ?
C16 C17 H17 118.2 . . ?
C19 C18 C5 116.8(12) . . ?
C19 C18 C17 130.6(12) . . ?
C5 C18 C17 112.3(11) . . ?
C18 C19 C20 120.1(11) . . ?
C18 C19 Pt5 118.7(9) . . ?
C20 C19 Pt5 121.1(9) . . ?
C6 C20 C19 122.4(12) . . ?
C6 C20 H20 118.8 . . ?
C19 C20 H20 118.8 . . ?
C22 C21 P1 115.4(13) . . ?
C22 C21 H21A 108.4 . . ?
P1 C21 H21A 108.4 . . ?
C22 C21 H21B 108.4 . . ?
P1 C21 H21B 108.4 . . ?
H21A C21 H21B 107.5 . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C24 C23 P1 113.4(11) . . ?
C24 C23 H23A 108.9 . . ?
P1 C23 H23A 108.9 . . ?
C24 C23 H23B 108.9 . . ?
P1 C23 H23B 108.9 . . ?
H23A C23 H23B 107.7 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 P1 117.6(12) . . ?
C26 C25 H25A 107.9 . . ?
P1 C25 H25A 107.9 . . ?
C26 C25 H25B 107.9 . . ?
P1 C25 H25B 107.9 . . ?
H25A C25 H25B 107.2 . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C28A C27A P2 113.6(4) . . ?
C28A C27A H27A 108.8 . . ?
P2 C27A H27A 108.8 . . ?
C28A C27A H27B 108.8 . . ?
P2 C27A H27B 108.8 . . ?
H27A C27A H27B 107.7 . . ?
C27A C28A H28A 109.5 . . ?
C27A C28A H28B 109.5 . . ?
H28A C28A H28B 109.5 . . ?
C27A C28A H28C 109.5 . . ?
H28A C28A H28C 109.5 . . ?
H28B C28A H28C 109.5 . . ?
C30A C29A P2 113.4(4) . . ?
C30A C29A H29A 108.9 . . ?
P2 C29A H29A 108.9 . . ?
C30A C29A H29B 108.9 . . ?
P2 C29A H29B 108.9 . . ?
H29A C29A H29B 107.7 . . ?
C29A C30A H30A 109.5 . . ?
C29A C30A H30B 109.5 . . ?
H30A C30A H30B 109.5 . . ?
C29A C30A H30C 109.5 . . ?
H30A C30A H30C 109.5 . . ?
H30B C30A H30C 109.5 . . ?
C32A C31A P2 113.4(4) . . ?
C32A C31A H31A 108.9 . . ?
P2 C31A H31A 108.9 . . ?
C32A C31A H31B 108.9 . . ?
P2 C31A H31B 108.9 . . ?
H31A C31A H31B 107.7 . . ?
C31A C32A H32A 109.5 . . ?
C31A C32A H32B 109.5 . . ?
H32A C32A H32B 109.5 . . ?
C31A C32A H32C 109.5 . . ?
H32A C32A H32C 109.5 . . ?
H32B C32A H32C 109.5 . . ?
C28B C27B P2 113.6(4) . . ?
C28B C27B H27C 108.9 . . ?
P2 C27B H27C 108.9 . . ?
C28B C27B H27D 108.9 . . ?
P2 C27B H27D 108.9 . . ?
H27C C27B H27D 107.7 . . ?
C27B C28B H28D 109.5 . . ?
C27B C28B H28E 109.5 . . ?
H28D C28B H28E 109.5 . . ?
C27B C28B H28F 109.5 . . ?
H28D C28B H28F 109.5 . . ?
H28E C28B H28F 109.5 . . ?
C30B C29B P2 113.5(4) . . ?
C30B C29B H29C 108.9 . . ?
P2 C29B H29C 108.9 . . ?
C30B C29B H29D 108.9 . . ?
P2 C29B H29D 108.9 . . ?
H29C C29B H29D 107.7 . . ?
C29B C30B H30D 109.5 . . ?
C29B C30B H30E 109.5 . . ?
H30D C30B H30E 109.5 . . ?
C29B C30B H30F 109.5 . . ?
H30D C30B H30F 109.5 . . ?
H30E C30B H30F 109.5 . . ?
C32B C31B P2 113.5(4) . . ?
C32B C31B H31C 108.9 . . ?
P2 C31B H31C 108.9 . . ?
C32B C31B H31D 108.9 . . ?
P2 C31B H31D 108.9 . . ?
H31C C31B H31D 107.7 . . ?
C31B C32B H32D 109.5 . . ?
C31B C32B H32E 109.5 . . ?
H32D C32B H32E 109.5 . . ?
C31B C32B H32F 109.5 . . ?
H32D C32B H32F 109.5 . . ?
H32E C32B H32F 109.5 . . ?
C34A C33A P3 113.5(4) . . ?
C34A C33A H33A 108.9 . . ?
P3 C33A H33A 108.9 . . ?
C34A C33A H33B 108.9 . . ?
P3 C33A H33B 108.9 . . ?
H33A C33A H33B 107.7 . . ?
C33A C34A H34A 109.5 . . ?
C33A C34A H34B 109.5 . . ?
H34A C34A H34B 109.5 . . ?
C33A C34A H34C 109.5 . . ?
H34A C34A H34C 109.5 . . ?
H34B C34A H34C 109.5 . . ?
C36A C35A P3 113.6(4) . . ?
C36A C35A H35A 108.8 . . ?
P3 C35A H35A 108.8 . . ?
C36A C35A H35B 108.8 . . ?
P3 C35A H35B 108.8 . . ?
H35A C35A H35B 107.7 . . ?
C35A C36A H36A 109.5 . . ?
C35A C36A H36B 109.5 . . ?
H36A C36A H36B 109.5 . . ?
C35A C36A H36C 109.5 . . ?
H36A C36A H36C 109.5 . . ?
H36B C36A H36C 109.5 . . ?
C38A C37A P3 113.3(4) . . ?
C38A C37A H37A 108.9 . . ?
P3 C37A H37A 108.9 . . ?
C38A C37A H37B 108.9 . . ?
P3 C37A H37B 108.9 . . ?
H37A C37A H37B 107.7 . . ?
C37A C38A H38A 109.5 . . ?
C37A C38A H38B 109.5 . . ?
H38A C38A H38B 109.5 . . ?
C37A C38A H38C 109.5 . . ?
H38A C38A H38C 109.5 . . ?
H38B C38A H38C 109.5 . . ?
C34B C33B P3 113.5(4) . . ?
C34B C33B H33C 108.9 . . ?
P3 C33B H33C 108.9 . . ?
C34B C33B H33D 108.9 . . ?
P3 C33B H33D 108.9 . . ?
H33C C33B H33D 107.7 . . ?
C33B C34B H34D 109.5 . . ?
C33B C34B H34E 109.5 . . ?
H34D C34B H34E 109.5 . . ?
C33B C34B H34F 109.5 . . ?
H34D C34B H34F 109.5 . . ?
H34E C34B H34F 109.5 . . ?
C36B C35B P3 113.4(4) . . ?
C36B C35B H35C 108.9 . . ?
P3 C35B H35C 108.9 . . ?
C36B C35B H35D 108.9 . . ?
P3 C35B H35D 108.9 . . ?
H35C C35B H35D 107.7 . . ?
C35B C36B H36D 109.5 . . ?
C35B C36B H36E 109.5 . . ?
H36D C36B H36E 109.5 . . ?
C35B C36B H36F 109.5 . . ?
H36D C36B H36F 109.5 . . ?
H36E C36B H36F 109.5 . . ?
C38B C37B P3 113.5(4) . . ?
C38B C37B H37C 108.9 . . ?
P3 C37B H37C 108.9 . . ?
C38B C37B H37D 108.9 . . ?
P3 C37B H37D 108.9 . . ?
H37C C37B H37D 107.7 . . ?
C37B C38B H38D 109.5 . . ?
C37B C38B H38E 109.5 . . ?
H38D C38B H38E 109.5 . . ?
C37B C38B H38F 109.5 . . ?
H38D C38B H38F 109.5 . . ?
H38E C38B H38F 109.5 . . ?
C40 C39 P4 116.3(10) . . ?
C40 C39 H39A 108.2 . . ?
P4 C39 H39A 108.2 . . ?
C40 C39 H39B 108.2 . . ?
P4 C39 H39B 108.2 . . ?
H39A C39 H39B 107.4 . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C42 C41 P4 115.3(10) . . ?
C42 C41 H41A 108.5 . . ?
P4 C41 H41A 108.5 . . ?
C42 C41 H41B 108.5 . . ?
P4 C41 H41B 108.5 . . ?
H41A C41 H41B 107.5 . . ?
C41 C42 H42A 109.5 . . ?
C41 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C41 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 P4 113.7(11) . . ?
C44 C43 H43A 108.8 . . ?
P4 C43 H43A 108.8 . . ?
C44 C43 H43B 108.8 . . ?
P4 C43 H43B 108.8 . . ?
H43A C43 H43B 107.7 . . ?
C43 C44 H44A 109.5 . . ?
C43 C44 H44B 109.5 . . ?
H44A C44 H44B 109.5 . . ?
C43 C44 H44C 109.5 . . ?
H44A C44 H44C 109.5 . . ?
H44B C44 H44C 109.5 . . ?
C46A C45A P5 113.6(4) . . ?
C46A C45A H45A 108.8 . . ?
P5 C45A H45A 108.8 . . ?
C46A C45A H45B 108.8 . . ?
P5 C45A H45B 108.8 . . ?
H45A C45A H45B 107.7 . . ?
C45A C46A H46A 109.5 . . ?
C45A C46A H46B 109.5 . . ?
H46A C46A H46B 109.5 . . ?
C45A C46A H46C 109.5 . . ?
H46A C46A H46C 109.5 . . ?
H46B C46A H46C 109.5 . . ?
C48A C47A P5 113.5(4) . . ?
C48A C47A H47A 108.9 . . ?
P5 C47A H47A 108.9 . . ?
C48A C47A H47B 108.9 . . ?
P5 C47A H47B 108.9 . . ?
H47A C47A H47B 107.7 . . ?
C47A C48A H48A 109.5 . . ?
C47A C48A H48B 109.5 . . ?
H48A C48A H48B 109.5 . . ?
C47A C48A H48C 109.5 . . ?
H48A C48A H48C 109.5 . . ?
H48B C48A H48C 109.5 . . ?
C50A C49A P5 113.4(4) . . ?
C50A C49A H49A 108.9 . . ?
P5 C49A H49A 108.9 . . ?
C50A C49A H49B 108.9 . . ?
P5 C49A H49B 108.9 . . ?
H49A C49A H49B 107.7 . . ?
C49A C50A H50A 109.5 . . ?
C49A C50A H50B 109.5 . . ?
H50A C50A H50B 109.5 . . ?
C49A C50A H50C 109.5 . . ?
H50A C50A H50C 109.5 . . ?
H50B C50A H50C 109.5 . . ?
C46B C45B P5 113.6(4) . . ?
C46B C45B H45C 108.8 . . ?
P5 C45B H45C 108.8 . . ?
C46B C45B H45D 108.8 . . ?
P5 C45B H45D 108.8 . . ?
H45C C45B H45D 107.7 . . ?
C45B C46B H46D 109.5 . . ?
C45B C46B H46E 109.5 . . ?
H46D C46B H46E 109.5 . . ?
C45B C46B H46F 109.5 . . ?
H46D C46B H46F 109.5 . . ?
H46E C46B H46F 109.5 . . ?
C48B C47B P5 113.5(4) . . ?
C48B C47B H47C 108.9 . . ?
P5 C47B H47C 108.9 . . ?
C48B C47B H47D 108.9 . . ?
P5 C47B H47D 108.9 . . ?
H47C C47B H47D 107.7 . . ?
C47B C48B H48D 109.5 . . ?
C47B C48B H48E 109.5 . . ?
H48D C48B H48E 109.5 . . ?
C47B C48B H48F 109.5 . . ?
H48D C48B H48F 109.5 . . ?
H48E C48B H48F 109.5 . . ?
C50B C49B P5 113.5(4) . . ?
C50B C49B H49C 108.9 . . ?
P5 C49B H49C 108.9 . . ?
C50B C49B H49D 108.9 . . ?
P5 C49B H49D 108.9 . . ?
H49C C49B H49D 107.7 . . ?
C49B C50B H50D 109.5 . . ?
C49B C50B H50E 109.5 . . ?
H50D C50B H50E 109.5 . . ?
C49B C50B H50F 109.5 . . ?
H50D C50B H50F 109.5 . . ?
H50E C50B H50F 109.5 . . ?
C52 C51 P6 116.5(10) . . ?
C52 C51 H51A 108.2 . . ?
P6 C51 H51A 108.2 . . ?
C52 C51 H51B 108.2 . . ?
P6 C51 H51B 108.2 . . ?
H51A C51 H51B 107.3 . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C54 C53 P6 112.6(10) . . ?
C54 C53 H53A 109.1 . . ?
P6 C53 H53A 109.1 . . ?
C54 C53 H53B 109.1 . . ?
P6 C53 H53B 109.1 . . ?
H53A C53 H53B 107.8 . . ?
C53 C54 H54A 109.5 . . ?
C53 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C53 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C56 C55 P6 113.5(9) . . ?
C56 C55 H55A 108.9 . . ?
P6 C55 H55A 108.9 . . ?
C56 C55 H55B 108.9 . . ?
P6 C55 H55B 108.9 . . ?
H55A C55 H55B 107.7 . . ?
C55 C56 H56A 109.5 . . ?
C55 C56 H56B 109.5 . . ?
H56A C56 H56B 109.5 . . ?
C55 C56 H56C 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?
C58A C57A P7 113.5(4) . . ?
C58A C57A H57A 108.9 . . ?
P7 C57A H57A 108.9 . . ?
C58A C57A H57B 108.9 . . ?
P7 C57A H57B 108.9 . . ?
H57A C57A H57B 107.7 . . ?
C57A C58A H58A 109.5 . . ?
C57A C58A H58B 109.5 . . ?
H58A C58A H58B 109.5 . . ?
C57A C58A H58C 109.5 . . ?
H58A C58A H58C 109.5 . . ?
H58B C58A H58C 109.5 . . ?
C60A C59A P7 113.6(4) . . ?
C60A C59A H59A 108.8 . . ?
P7 C59A H59A 108.8 . . ?
C60A C59A H59B 108.8 . . ?
P7 C59A H59B 108.8 . . ?
H59A C59A H59B 107.7 . . ?
C59A C60A H60A 109.5 . . ?
C59A C60A H60B 109.5 . . ?
H60A C60A H60B 109.5 . . ?
C59A C60A H60C 109.5 . . ?
H60A C60A H60C 109.5 . . ?
H60B C60A H60C 109.5 . . ?
C62A C61A P7 113.6(4) . . ?
C62A C61A H61A 108.8 . . ?
P7 C61A H61A 108.8 . . ?
C62A C61A H61B 108.8 . . ?
P7 C61A H61B 108.8 . . ?
H61A C61A H61B 107.7 . . ?
C61A C62A H62A 109.5 . . ?
C61A C62A H62B 109.5 . . ?
H62A C62A H62B 109.5 . . ?
C61A C62A H62C 109.5 . . ?
H62A C62A H62C 109.5 . . ?
H62B C62A H62C 109.5 . . ?
C58B C57B P7 113.5(4) . . ?
C58B C57B H57C 108.9 . . ?
P7 C57B H57C 108.9 . . ?
C58B C57B H57D 108.9 . . ?
P7 C57B H57D 108.9 . . ?
H57C C57B H57D 107.7 . . ?
C57B C58B H58D 109.5 . . ?
C57B C58B H58E 109.5 . . ?
H58D C58B H58E 109.5 . . ?
C57B C58B H58F 109.5 . . ?
H58D C58B H58F 109.5 . . ?
H58E C58B H58F 109.5 . . ?
C60B C59B P7 113.6(4) . . ?
C60B C59B H59C 108.8 . . ?
P7 C59B H59C 108.8 . . ?
C60B C59B H59D 108.8 . . ?
P7 C59B H59D 108.9 . . ?
H59C C59B H59D 107.7 . . ?
C59B C60B H60D 109.5 . . ?
C59B C60B H60E 109.5 . . ?
H60D C60B H60E 109.5 . . ?
C59B C60B H60F 109.5 . . ?
H60D C60B H60F 109.5 . . ?
H60E C60B H60F 109.5 . . ?
C62B C61B P7 113.5(4) . . ?
C62B C61B H61C 108.9 . . ?
P7 C61B H61C 108.9 . . ?
C62B C61B H61D 108.9 . . ?
P7 C61B H61D 108.9 . . ?
H61C C61B H61D 107.7 . . ?
C61B C62B H62D 109.5 . . ?
C61B C62B H62E 109.5 . . ?
H62D C62B H62E 109.5 . . ?
C61B C62B H62F 109.5 . . ?
H62D C62B H62F 109.5 . . ?
H62E C62B H62F 109.5 . . ?
C64A C63A P8 113.5(4) . . ?
C64A C63A H63A 108.9 . . ?
P8 C63A H63A 108.9 . . ?
C64A C63A H63B 108.9 . . ?
P8 C63A H63B 108.9 . . ?
H63A C63A H63B 107.7 . . ?
C63A C64A H64A 109.5 . . ?
C63A C64A H64B 109.5 . . ?
H64A C64A H64B 109.5 . . ?
C63A C64A H64C 109.5 . . ?
H64A C64A H64C 109.5 . . ?
H64B C64A H64C 109.5 . . ?
C66A C65A P8 113.6(4) . . ?
C66A C65A H65A 108.9 . . ?
P8 C65A H65A 108.9 . . ?
C66A C65A H65B 108.9 . . ?
P8 C65A H65B 108.9 . . ?
H65A C65A H65B 107.7 . . ?
C65A C66A H66A 109.5 . . ?
C65A C66A H66B 109.5 . . ?
H66A C66A H66B 109.5 . . ?
C65A C66A H66C 109.5 . . ?
H66A C66A H66C 109.5 . . ?
H66B C66A H66C 109.5 . . ?
C68A C67A P8 113.7(4) . . ?
C68A C67A H67A 108.8 . . ?
P8 C67A H67A 108.8 . . ?
C68A C67A H67B 108.8 . . ?
P8 C67A H67B 108.8 . . ?
H67A C67A H67B 107.7 . . ?
C67A C68A H68A 109.5 . . ?
C67A C68A H68B 109.5 . . ?
H68A C68A H68B 109.5 . . ?
C67A C68A H68C 109.5 . . ?
H68A C68A H68C 109.5 . . ?
H68B C68A H68C 109.5 . . ?
C64B C63B P8 113.3(4) . . ?
C64B C63B H63C 108.9 . . ?
P8 C63B H63C 108.9 . . ?
C64B C63B H63D 108.9 . . ?
P8 C63B H63D 108.9 . . ?
H63C C63B H63D 107.7 . . ?
C63B C64B H64D 109.5 . . ?
C63B C64B H64E 109.5 . . ?
H64D C64B H64E 109.5 . . ?
C63B C64B H64F 109.5 . . ?
H64D C64B H64F 109.5 . . ?
H64E C64B H64F 109.5 . . ?
C66B C65B P8 113.6(4) . . ?
C66B C65B H65C 108.8 . . ?
P8 C65B H65C 108.8 . . ?
C66B C65B H65D 108.8 . . ?
P8 C65B H65D 108.8 . . ?
H65C C65B H65D 107.7 . . ?
C65B C66B H66D 109.5 . . ?
C65B C66B H66E 109.5 . . ?
H66D C66B H66E 109.5 . . ?
C65B C66B H66F 109.5 . . ?
H66D C66B H66F 109.5 . . ?
H66E C66B H66F 109.5 . . ?
C68B C67B P8 113.7(4) . . ?
C68B C67B H67C 108.8 . . ?
P8 C67B H67C 108.8 . . ?
C68B C67B H67D 108.8 . . ?
P8 C67B H67D 108.8 . . ?
H67C C67B H67D 107.7 . . ?
C67B C68B H68D 109.5 . . ?
C67B C68B H68E 109.5 . . ?
H68D C68B H68E 109.5 . . ?
C67B C68B H68F 109.5 . . ?
H68D C68B H68F 109.5 . . ?
H68E C68B H68F 109.5 . . ?
C70 C69 P9 110.5(14) . . ?
C70 C69 H69A 109.5 . . ?
P9 C69 H69A 109.5 . . ?
C70 C69 H69B 109.5 . . ?
P9 C69 H69B 109.5 . . ?
H69A C69 H69B 108.1 . . ?
C69 C70 H70A 109.5 . . ?
C69 C70 H70B 109.5 . . ?
H70A C70 H70B 109.5 . . ?
C69 C70 H70C 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C72 C71 P9 109.9(13) . . ?
C72 C71 H71A 109.7 . . ?
P9 C71 H71A 109.7 . . ?
C72 C71 H71B 109.7 . . ?
P9 C71 H71B 109.7 . . ?
H71A C71 H71B 108.2 . . ?
C71 C72 H72A 109.5 . . ?
C71 C72 H72B 109.5 . . ?
H72A C72 H72B 109.5 . . ?
C71 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
C74 C73 P9 117.5(17) . . ?
C74 C73 H73A 107.9 . . ?
P9 C73 H73A 107.9 . . ?
C74 C73 H73B 107.9 . . ?
P9 C73 H73B 107.9 . . ?
H73A C73 H73B 107.2 . . ?
C73 C74 H74A 109.5 . . ?
C73 C74 H74B 109.5 . . ?
H74A C74 H74B 109.5 . . ?
C73 C74 H74C 109.5 . . ?
H74A C74 H74C 109.5 . . ?
H74B C74 H74C 109.5 . . ?
C76A C75A P10 113.3(4) . . ?
C76A C75A H75A 108.9 . . ?
P10 C75A H75A 108.9 . . ?
C76A C75A H75B 108.9 . . ?
P10 C75A H75B 108.9 . . ?
H75A C75A H75B 107.7 . . ?
C75A C76A H76A 109.5 . . ?
C75A C76A H76B 109.5 . . ?
H76A C76A H76B 109.5 . . ?
C75A C76A H76C 109.5 . . ?
H76A C76A H76C 109.5 . . ?
H76B C76A H76C 109.5 . . ?
C78A C77A P10 113.6(4) . . ?
C78A C77A H77A 108.8 . . ?
P10 C77A H77A 108.8 . . ?
C78A C77A H77B 108.8 . . ?
P10 C77A H77B 108.8 . . ?
H77A C77A H77B 107.7 . . ?
C77A C78A H78A 109.5 . . ?
C77A C78A H78B 109.5 . . ?
H78A C78A H78B 109.5 . . ?
C77A C78A H78C 109.5 . . ?
H78A C78A H78C 109.5 . . ?
H78B C78A H78C 109.5 . . ?
C80A C79A P10 113.5(4) . . ?
C80A C79A H79A 108.9 . . ?
P10 C79A H79A 108.9 . . ?
C80A C79A H79B 108.9 . . ?
P10 C79A H79B 108.9 . . ?
H79A C79A H79B 107.7 . . ?
C79A C80A H80A 109.5 . . ?
C79A C80A H80B 109.5 . . ?
H80A C80A H80B 109.5 . . ?
C79A C80A H80C 109.5 . . ?
H80A C80A H80C 109.5 . . ?
H80B C80A H80C 109.5 . . ?
C76B C75B P10 113.3(4) . . ?
C76B C75B H75C 108.9 . . ?
P10 C75B H75C 108.9 . . ?
C76B C75B H75D 108.9 . . ?
P10 C75B H75D 108.9 . . ?
H75C C75B H75D 107.7 . . ?
C75B C76B H76D 109.5 . . ?
C75B C76B H76E 109.5 . . ?
H76D C76B H76E 109.5 . . ?
C75B C76B H76F 109.5 . . ?
H76D C76B H76F 109.5 . . ?
H76E C76B H76F 109.5 . . ?
C78B C77B P10 113.4(4) . . ?
C78B C77B H77C 108.9 . . ?
P10 C77B H77C 108.9 . . ?
C78B C77B H77D 108.9 . . ?
P10 C77B H77D 108.9 . . ?
H77C C77B H77D 107.7 . . ?
C77B C78B H78D 109.5 . . ?
C77B C78B H78E 109.5 . . ?
H78D C78B H78E 109.5 . . ?
C77B C78B H78F 109.5 . . ?
H78D C78B H78F 109.5 . . ?
H78E C78B H78F 109.5 . . ?
C80B C79B P10 113.5(4) . . ?
C80B C79B H79C 108.9 . . ?
P10 C79B H79C 108.9 . . ?
C80B C79B H79D 108.9 . . ?
P10 C79B H79D 108.9 . . ?
H79C C79B H79D 107.7 . . ?
C79B C80B H80D 109.5 . . ?
C79B C80B H80E 109.5 . . ?
H80D C80B H80E 109.5 . . ?
C79B C80B H80F 109.5 . . ?
H80D C80B H80F 109.5 . . ?
H80E C80B H80F 109.5 . . ?
C87 Pt6 P11 92.3(3) . . ?
C87 Pt6 P12 85.4(3) . . ?
P11 Pt6 P12 177.33(13) . . ?
C87 Pt6 Cl6 177.5(3) . . ?
P11 Pt6 Cl6 89.92(14) . . ?
P12 Pt6 Cl6 92.38(14) . . ?
C90 Pt7 P14 93.2(3) . . ?
C90 Pt7 P13 87.5(4) . . ?
P14 Pt7 P13 179.13(15) . . ?
C90 Pt7 Cl7 176.2(3) . . ?
P14 Pt7 Cl7 89.81(13) . . ?
P13 Pt7 Cl7 89.43(15) . . ?
C93 Pt8 P16 93.1(3) . . ?
C93 Pt8 P15 89.2(3) . . ?
P16 Pt8 P15 174.87(13) . . ?
C93 Pt8 Cl8 179.4(3) . . ?
P16 Pt8 Cl8 86.42(13) . . ?
P15 Pt8 Cl8 91.23(13) . . ?
C96 Pt9 P17 92.4(3) . . ?
C96 Pt9 P18 91.6(3) . . ?
P17 Pt9 P18 175.10(12) . . ?
C96 Pt9 Cl9 176.9(4) . . ?
P17 Pt9 Cl9 89.16(12) . . ?
P18 Pt9 Cl9 86.70(12) . . ?
C99 Pt10 P20 88.9(3) . . ?
C99 Pt10 P19 171.4(3) . . ?
P20 Pt10 P19 99.03(12) . . ?
C99 Pt10 Cl10 87.0(3) . . ?
P20 Pt10 Cl10 175.66(12) . . ?
P19 Pt10 Cl10 85.10(12) . . ?
C205 P11 C201 115(2) . . ?
C101 P11 C103 106.8(12) . . ?
C101 P11 C105 97.7(10) . . ?
C103 P11 C105 101.4(11) . . ?
C205 P11 C203 104.2(15) . . ?
C201 P11 C203 98.2(14) . . ?
C101 P11 Pt6 118.1(6) . . ?
C205 P11 Pt6 114.2(14) . . ?
C201 P11 Pt6 116.8(11) . . ?
C103 P11 Pt6 116.0(9) . . ?
C105 P11 Pt6 114.1(8) . . ?
C203 P11 Pt6 105.0(10) . . ?
C111 P12 C107 103.9(10) . . ?
C211 P12 C209 100(3) . . ?
C111 P12 C109 108(2) . . ?
C107 P12 C109 99(2) . . ?
C211 P12 C207 101.5(14) . . ?
C209 P12 C207 112(3) . . ?
C111 P12 Pt6 112.3(19) . . ?
C107 P12 Pt6 115.7(19) . . ?
C211 P12 Pt6 119(3) . . ?
C209 P12 Pt6 115.9(10) . . ?
C109 P12 Pt6 116.5(7) . . ?
C207 P12 Pt6 106.8(19) . . ?
C215 P13 C213 101.9(17) . . ?
C113 P13 C117 134.9(12) . . ?
C215 P13 C217 105.2(12) . . ?
C213 P13 C217 75.3(11) . . ?
C113 P13 C115 96.5(15) . . ?
C117 P13 C115 98.4(11) . . ?
C215 P13 Pt7 131.6(11) . . ?
C213 P13 Pt7 123.0(13) . . ?
C113 P13 Pt7 103.4(7) . . ?
C117 P13 Pt7 111.1(8) . . ?
C217 P13 Pt7 102.9(9) . . ?
C115 P13 Pt7 109.6(6) . . ?
C221 P14 C223 104.7(16) . . ?
C121 P14 C119 111.3(16) . . ?
C221 P14 C219 96(2) . . ?
C223 P14 C219 97.8(18) . . ?
C121 P14 C123 99.4(15) . . ?
C119 P14 C123 109.2(18) . . ?
C221 P14 Pt7 121.6(14) . . ?
C121 P14 Pt7 108.7(11) . . ?
C223 P14 Pt7 119.1(14) . . ?
C119 P14 Pt7 116.0(14) . . ?
C219 P14 Pt7 113(2) . . ?
C123 P14 Pt7 111.1(7) . . ?
C129 P15 C127 102.2(7) . . ?
C129 P15 C125 103.8(6) . . ?
C127 P15 C125 102.1(7) . . ?
C129 P15 Pt8 112.8(5) . . ?
C127 P15 Pt8 114.7(5) . . ?
C125 P15 Pt8 119.3(5) . . ?
C135 P16 C131 104.5(8) . . ?
C135 P16 C133 107.0(8) . . ?
C131 P16 C133 101.6(8) . . ?
C135 P16 Pt8 117.3(5) . . ?
C131 P16 Pt8 114.3(7) . . ?
C133 P16 Pt8 110.8(5) . . ?
C139 P17 C137 102.2(6) . . ?
C139 P17 C141 105.8(7) . . ?
C137 P17 C141 104.9(6) . . ?
C139 P17 Pt9 113.0(4) . . ?
C137 P17 Pt9 120.7(4) . . ?
C141 P17 Pt9 108.9(5) . . ?
C147 P18 C143 105.0(6) . . ?
C147 P18 C145 102.2(6) . . ?
C143 P18 C145 104.0(7) . . ?
C147 P18 Pt9 120.8(4) . . ?
C143 P18 Pt9 111.8(5) . . ?
C145 P18 Pt9 111.4(5) . . ?
C151 P19 C153 106.0(7) . . ?
C151 P19 C149 103.7(6) . . ?
C153 P19 C149 101.5(7) . . ?
C151 P19 Pt10 111.1(5) . . ?
C153 P19 Pt10 108.3(5) . . ?
C149 P19 Pt10 124.6(5) . . ?
C159 P20 C155 103.5(8) . . ?
C159 P20 C157 104.4(7) . . ?
C155 P20 C157 103.7(7) . . ?
C159 P20 Pt10 113.6(5) . . ?
C155 P20 Pt10 116.0(4) . . ?
C157 P20 Pt10 114.3(5) . . ?
C82 C81 C86 123.9(11) . . ?
C82 C81 C85 108.9(10) . . ?
C86 C81 C85 121.7(11) . . ?
C81 C82 C89 124.3(11) . . ?
C81 C82 C83 108.5(10) . . ?
C89 C82 C83 122.6(11) . . ?
C92 C83 C84 125.5(11) . . ?
C92 C83 C82 123.4(11) . . ?
C84 C83 C82 106.3(10) . . ?
C83 C84 C85 109.5(10) . . ?
C83 C84 C95 121.3(10) . . ?
C85 C84 C95 124.3(10) . . ?
C98 C85 C84 122.9(11) . . ?
C98 C85 C81 125.1(11) . . ?
C84 C85 C81 106.8(10) . . ?
C81 C86 C87 114.0(11) . . ?
C81 C86 C100 113.4(10) . . ?
C87 C86 C100 132.2(11) . . ?
C88 C87 C86 119.3(11) . . ?
C88 C87 Pt6 120.0(8) . . ?
C86 C87 Pt6 120.7(9) . . ?
C87 C88 C89 125.1(11) . . ?
C87 C88 H88 117.4 . . ?
C89 C88 H88 117.4 . . ?
C82 C89 C88 111.7(11) . . ?
C82 C89 C90 116.6(11) . . ?
C88 C89 C90 131.4(12) . . ?
C91 C90 C89 117.2(10) . . ?
C91 C90 Pt7 121.3(8) . . ?
C89 C90 Pt7 121.4(9) . . ?
C92 C91 C90 125.1(10) . . ?
C92 C91 H91 117.4 . . ?
C90 C91 H91 117.4 . . ?
C83 C92 C91 113.2(11) . . ?
C83 C92 C93 113.3(10) . . ?
C91 C92 C93 133.0(11) . . ?
C94 C93 C92 120.0(10) . . ?
C94 C93 Pt8 121.2(8) . . ?
C92 C93 Pt8 118.8(8) . . ?
C93 C94 C95 124.7(10) . . ?
C93 C94 H94 117.7 . . ?
C95 C94 H94 117.7 . . ?
C84 C95 C94 112.7(10) . . ?
C84 C95 C96 114.6(10) . . ?
C94 C95 C96 131.6(11) . . ?
C97 C96 C95 118.2(10) . . ?
C97 C96 Pt9 120.3(9) . . ?
C95 C96 Pt9 121.4(8) . . ?
C98 C97 C96 125.1(11) . . ?
C98 C97 H97 117.4 . . ?
C96 C97 H97 117.4 . . ?
C85 C98 C97 114.4(11) . . ?
C85 C98 C99 113.7(10) . . ?
C97 C98 C99 130.8(11) . . ?
C100 C99 C98 120.3(11) . . ?
C100 C99 Pt10 119.9(8) . . ?
C98 C99 Pt10 119.7(8) . . ?
C99 C100 C86 123.1(10) . . ?
C99 C100 H100 118.5 . . ?
C86 C100 H100 118.5 . . ?
C102 C101 P11 113.6(4) . . ?
C102 C101 H10A 108.8 . . ?
P11 C101 H10A 108.8 . . ?
C102 C101 H10B 108.8 . . ?
P11 C101 H10B 108.8 . . ?
H10A C101 H10B 107.7 . . ?
C101 C102 H10C 109.5 . . ?
C101 C102 H10D 109.5 . . ?
H10C C102 H10D 109.5 . . ?
C101 C102 H10E 109.5 . . ?
H10C C102 H10E 109.5 . . ?
H10D C102 H10E 109.5 . . ?
C104 C103 P11 113.3(4) . . ?
C104 C103 H10F 108.9 . . ?
P11 C103 H10F 108.9 . . ?
C104 C103 H10G 108.9 . . ?
P11 C103 H10G 108.9 . . ?
H10F C103 H10G 107.7 . . ?
C103 C104 H10H 109.5 . . ?
C103 C104 H10I 109.5 . . ?
H10H C104 H10I 109.5 . . ?
C103 C104 H10J 109.5 . . ?
H10H C104 H10J 109.5 . . ?
H10I C104 H10J 109.5 . . ?
C106 C105 P11 113.5(4) . . ?
C106 C105 H10K 108.9 . . ?
P11 C105 H10K 108.9 . . ?
C106 C105 H10L 108.9 . . ?
P11 C105 H10L 108.9 . . ?
H10K C105 H10L 107.7 . . ?
C105 C106 H10M 109.5 . . ?
C105 C106 H10N 109.5 . . ?
H10M C106 H10N 109.5 . . ?
C105 C106 H10O 109.5 . . ?
H10M C106 H10O 109.5 . . ?
H10N C106 H10O 109.5 . . ?
C202 C201 P11 113.6(4) . . ?
C202 C201 H20A 108.8 . . ?
P11 C201 H20A 108.8 . . ?
C202 C201 H20B 108.8 . . ?
P11 C201 H20B 108.8 . . ?
H20A C201 H20B 107.7 . . ?
C201 C202 H20C 109.5 . . ?
C201 C202 H20D 109.5 . . ?
H20C C202 H20D 109.5 . . ?
C201 C202 H20E 109.5 . . ?
H20C C202 H20E 109.5 . . ?
H20D C202 H20E 109.5 . . ?
C204 C203 P11 113.5(4) . . ?
C204 C203 H20F 108.9 . . ?
P11 C203 H20F 108.9 . . ?
C204 C203 H20G 108.9 . . ?
P11 C203 H20G 108.9 . . ?
H20F C203 H20G 107.7 . . ?
C203 C204 H20H 109.5 . . ?
C203 C204 H20I 109.5 . . ?
H20H C204 H20I 109.5 . . ?
C203 C204 H20J 109.5 . . ?
H20H C204 H20J 109.5 . . ?
H20I C204 H20J 109.5 . . ?
C206 C205 P11 113.4(4) . . ?
C206 C205 H20K 108.9 . . ?
P11 C205 H20K 108.9 . . ?
C206 C205 H20L 108.9 . . ?
P11 C205 H20L 108.9 . . ?
H20K C205 H20L 107.7 . . ?
C205 C206 H20M 109.5 . . ?
C205 C206 H20N 109.5 . . ?
H20M C206 H20N 109.5 . . ?
C205 C206 H20O 109.5 . . ?
H20M C206 H20O 109.5 . . ?
H20N C206 H20O 109.5 . . ?
C108 C107 P12 113.5(4) . . ?
C108 C107 H10P 108.9 . . ?
P12 C107 H10P 108.9 . . ?
C108 C107 H10Q 108.9 . . ?
P12 C107 H10Q 108.9 . . ?
H10P C107 H10Q 107.7 . . ?
C107 C108 H10R 109.5 . . ?
C107 C108 H10S 109.5 . . ?
H10R C108 H10S 109.5 . . ?
C107 C108 H10T 109.5 . . ?
H10R C108 H10T 109.5 . . ?
H10S C108 H10T 109.5 . . ?
C110 C109 P12 113.5(4) . . ?
C110 C109 H10U 108.9 . . ?
P12 C109 H10U 108.9 . . ?
C110 C109 H10V 108.9 . . ?
P12 C109 H10V 108.9 . . ?
H10U C109 H10V 107.7 . . ?
C109 C110 H11A 109.5 . . ?
C109 C110 H11B 109.5 . . ?
H11A C110 H11B 109.5 . . ?
C109 C110 H11C 109.5 . . ?
H11A C110 H11C 109.5 . . ?
H11B C110 H11C 109.5 . . ?
C112 C111 P12 113.4(4) . . ?
C112 C111 H11D 108.9 . . ?
P12 C111 H11D 108.9 . . ?
C112 C111 H11E 108.9 . . ?
P12 C111 H11E 108.9 . . ?
H11D C111 H11E 107.7 . . ?
C111 C112 H11F 109.5 . . ?
C111 C112 H11G 109.5 . . ?
H11F C112 H11G 109.5 . . ?
C111 C112 H11H 109.5 . . ?
H11F C112 H11H 109.5 . . ?
H11G C112 H11H 109.5 . . ?
C208 C207 P12 113.4(19) . . ?
C208 C207 H20P 108.9 . . ?
P12 C207 H20P 108.9 . . ?
C208 C207 H20Q 108.9 . . ?
P12 C207 H20Q 108.9 . . ?
H20P C207 H20Q 107.7 . . ?
C207 C208 H20R 109.5 . . ?
C207 C208 H20S 109.5 . . ?
H20R C208 H20S 109.5 . . ?
C207 C208 H20T 109.5 . . ?
H20R C208 H20T 109.5 . . ?
H20S C208 H20T 109.5 . . ?
C210 C209 P12 113.5(4) . . ?
C210 C209 H20U 108.9 . . ?
P12 C209 H20U 108.9 . . ?
C210 C209 H20V 108.9 . . ?
P12 C209 H20V 108.9 . . ?
H20U C209 H20V 107.7 . . ?
C209 C210 H21C 109.5 . . ?
C209 C210 H21D 109.5 . . ?
H21C C210 H21D 109.5 . . ?
C209 C210 H21E 109.5 . . ?
H21C C210 H21E 109.5 . . ?
H21D C210 H21E 109.5 . . ?
C212 C211 P12 113.4(4) . . ?
C212 C211 H21F 108.9 . . ?
P12 C211 H21F 108.9 . . ?
C212 C211 H21G 108.9 . . ?
P12 C211 H21G 108.9 . . ?
H21F C211 H21G 107.7 . . ?
C211 C212 H21H 109.5 . . ?
C211 C212 H21I 109.5 . . ?
H21H C212 H21I 109.5 . . ?
C211 C212 H21J 109.5 . . ?
H21H C212 H21J 109.5 . . ?
H21I C212 H21J 109.5 . . ?
C114 C113 P13 113.7(4) . . ?
C114 C113 H11I 108.8 . . ?
P13 C113 H11I 108.8 . . ?
C114 C113 H11J 108.8 . . ?
P13 C113 H11J 108.8 . . ?
H11I C113 H11J 107.7 . . ?
C113 C114 H11K 109.5 . . ?
C113 C114 H11L 109.5 . . ?
H11K C114 H11L 109.5 . . ?
C113 C114 H11M 109.5 . . ?
H11K C114 H11M 109.5 . . ?
H11L C114 H11M 109.5 . . ?
C116 C115 P13 113.5(4) . . ?
C116 C115 H11N 108.9 . . ?
P13 C115 H11N 108.9 . . ?
C116 C115 H11O 108.9 . . ?
P13 C115 H11O 108.9 . . ?
H11N C115 H11O 107.7 . . ?
C115 C116 H11P 109.5 . . ?
C115 C116 H11Q 109.5 . . ?
H11P C116 H11Q 109.5 . . ?
C115 C116 H11R 109.5 . . ?
H11P C116 H11R 109.5 . . ?
H11Q C116 H11R 109.5 . . ?
C118 C117 P13 113.4(4) . . ?
C118 C117 H11S 108.9 . . ?
P13 C117 H11S 108.9 . . ?
C118 C117 H11T 108.9 . . ?
P13 C117 H11T 108.9 . . ?
H11S C117 H11T 107.7 . . ?
C117 C118 H11U 109.5 . . ?
C117 C118 H11V 109.5 . . ?
H11U C118 H11V 109.5 . . ?
C117 C118 H11W 109.5 . . ?
H11U C118 H11W 109.5 . . ?
H11V C118 H11W 109.5 . . ?
C214 C213 P13 113.5(4) . . ?
C214 C213 H21K 108.9 . . ?
P13 C213 H21K 108.9 . . ?
C214 C213 H21L 108.9 . . ?
P13 C213 H21L 108.9 . . ?
H21K C213 H21L 107.7 . . ?
C213 C214 H21M 109.5 . . ?
C213 C214 H21N 109.5 . . ?
H21M C214 H21N 109.5 . . ?
C213 C214 H21O 109.5 . . ?
H21M C214 H21O 109.5 . . ?
H21N C214 H21O 109.5 . . ?
C216 C215 P13 113.4(4) . . ?
C216 C215 H21P 108.9 . . ?
P13 C215 H21P 108.9 . . ?
C216 C215 H21Q 108.9 . . ?
P13 C215 H21Q 108.9 . . ?
H21P C215 H21Q 107.7 . . ?
C215 C216 H21R 109.5 . . ?
C215 C216 H21S 109.5 . . ?
H21R C216 H21S 109.5 . . ?
C215 C216 H21T 109.5 . . ?
H21R C216 H21T 109.5 . . ?
H21S C216 H21T 109.5 . . ?
C218 C217 P13 113.4(4) . . ?
C218 C217 H21U 108.9 . . ?
P13 C217 H21U 108.9 . . ?
C218 C217 H21V 108.9 . . ?
P13 C217 H21V 108.9 . . ?
H21U C217 H21V 107.7 . . ?
C217 C218 H916 109.5 . . ?
C217 C218 H917 109.5 . . ?
H916 C218 H917 109.5 . . ?
C217 C218 H918 109.5 . . ?
H916 C218 H918 109.5 . . ?
H917 C218 H918 109.5 . . ?
C120 C119 P14 113.5(4) . . ?
C120 C119 H914 108.9 . . ?
P14 C119 H914 108.9 . . ?
C120 C119 H915 108.9 . . ?
P14 C119 H915 108.9 . . ?
H914 C119 H915 107.7 . . ?
C119 C120 H12A 109.5 . . ?
C119 C120 H12B 109.5 . . ?
H12A C120 H12B 109.5 . . ?
C119 C120 H12C 109.5 . . ?
H12A C120 H12C 109.5 . . ?
H12B C120 H12C 109.5 . . ?
C122 C121 P14 113.5(4) . . ?
C122 C121 H12D 108.9 . . ?
P14 C121 H12D 108.9 . . ?
C122 C121 H12E 108.9 . . ?
P14 C121 H12E 108.9 . . ?
H12D C121 H12E 107.7 . . ?
C121 C122 H12F 109.5 . . ?
C121 C122 H12G 109.5 . . ?
H12F C122 H12G 109.5 . . ?
C121 C122 H12H 109.5 . . ?
H12F C122 H12H 109.5 . . ?
H12G C122 H12H 109.5 . . ?
C124 C123 P14 113.5(4) . . ?
C124 C123 H12I 108.9 . . ?
P14 C123 H12I 108.9 . . ?
C124 C123 H12J 108.9 . . ?
P14 C123 H12J 108.9 . . ?
H12I C123 H12J 107.7 . . ?
C123 C124 H12K 109.5 . . ?
C123 C124 H12L 109.5 . . ?
H12K C124 H12L 109.5 . . ?
C123 C124 H12M 109.5 . . ?
H12K C124 H12M 109.5 . . ?
H12L C124 H12M 109.5 . . ?
C220 C219 P14 113.5(4) . . ?
C220 C219 H919 108.9 . . ?
P14 C219 H919 108.9 . . ?
C220 C219 H920 108.9 . . ?
P14 C219 H920 108.9 . . ?
H919 C219 H920 107.7 . . ?
C219 C220 H22D 109.5 . . ?
C219 C220 H22E 109.5 . . ?
H22D C220 H22E 109.5 . . ?
C219 C220 H22F 109.5 . . ?
H22D C220 H22F 109.5 . . ?
H22E C220 H22F 109.5 . . ?
C222 C221 P14 113.5(4) . . ?
C222 C221 H22G 108.9 . . ?
P14 C221 H22G 108.9 . . ?
C222 C221 H22H 108.9 . . ?
P14 C221 H22H 108.9 . . ?
H22G C221 H22H 107.7 . . ?
C221 C222 H22I 109.5 . . ?
C221 C222 H22J 109.5 . . ?
H22I C222 H22J 109.5 . . ?
C221 C222 H22K 109.5 . . ?
H22I C222 H22K 109.5 . . ?
H22J C222 H22K 109.5 . . ?
C224 C223 P14 113.6(4) . . ?
C224 C223 H22L 108.9 . . ?
P14 C223 H22L 108.9 . . ?
C224 C223 H22M 108.9 . . ?
P14 C223 H22M 108.9 . . ?
H22L C223 H22M 107.7 . . ?
C223 C224 H22N 109.5 . . ?
C223 C224 H22O 109.5 . . ?
H22N C224 H22O 109.5 . . ?
C223 C224 H22P 109.5 . . ?
H22N C224 H22P 109.5 . . ?
H22O C224 H22P 109.5 . . ?
C126 C125 P15 115.9(10) . . ?
C126 C125 H12N 108.3 . . ?
P15 C125 H12N 108.3 . . ?
C126 C125 H12O 108.3 . . ?
P15 C125 H12O 108.3 . . ?
H12N C125 H12O 107.4 . . ?
C125 C126 H12P 109.5 . . ?
C125 C126 H12Q 109.5 . . ?
H12P C126 H12Q 109.5 . . ?
C125 C126 H12R 109.5 . . ?
H12P C126 H12R 109.5 . . ?
H12Q C126 H12R 109.5 . . ?
C128 C127 P15 111.7(9) . . ?
C128 C127 H12S 109.3 . . ?
P15 C127 H12S 109.3 . . ?
C128 C127 H12T 109.3 . . ?
P15 C127 H12T 109.3 . . ?
H12S C127 H12T 107.9 . . ?
C127 C128 H12U 109.5 . . ?
C127 C128 H12V 109.5 . . ?
H12U C128 H12V 109.5 . . ?
C127 C128 H12W 109.5 . . ?
H12U C128 H12W 109.5 . . ?
H12V C128 H12W 109.5 . . ?
C130 C129 P15 113.8(10) . . ?
C130 C129 H929 108.8 . . ?
P15 C129 H929 108.8 . . ?
C130 C129 H930 108.8 . . ?
P15 C129 H930 108.8 . . ?
H929 C129 H930 107.7 . . ?
C129 C130 H13A 109.5 . . ?
C129 C130 H13B 109.5 . . ?
H13A C130 H13B 109.5 . . ?
C129 C130 H13C 109.5 . . ?
H13A C130 H13C 109.5 . . ?
H13B C130 H13C 109.5 . . ?
C132 C131 C232 32.8(19) . . ?
C132 C131 P16 114.4(16) . . ?
C232 C131 P16 107(2) . . ?
C132 C131 H931 108.7 . . ?
C232 C131 H931 81.9 . . ?
P16 C131 H931 108.7 . . ?
C132 C131 H932 108.7 . . ?
C232 C131 H932 136.9 . . ?
P16 C131 H932 108.7 . . ?
H931 C131 H932 107.6 . . ?
C132 C131 H933 129.0 . . ?
C232 C131 H933 110.2 . . ?
P16 C131 H933 110.2 . . ?
H931 C131 H933 31.1 . . ?
H932 C131 H933 78.1 . . ?
C132 C131 H934 78.1 . . ?
C232 C131 H934 110.2 . . ?
P16 C131 H934 110.2 . . ?
H931 C131 H934 132.8 . . ?
H932 C131 H934 33.8 . . ?
H933 C131 H934 108.5 . . ?
C131 C132 H13F 109.5 . . ?
C131 C132 H13G 109.5 . . ?
H13F C132 H13G 109.5 . . ?
C131 C132 H13H 109.5 . . ?
H13F C132 H13H 109.5 . . ?
H13G C132 H13H 109.5 . . ?
C131 C232 H23C 109.5 . . ?
C131 C232 H23D 109.5 . . ?
H23C C232 H23D 109.5 . . ?
C131 C232 H23E 109.5 . . ?
H23C C232 H23E 109.5 . . ?
H23D C232 H23E 109.5 . . ?
C134 C133 P16 111.0(10) . . ?
C134 C133 H13I 109.4 . . ?
P16 C133 H13I 109.4 . . ?
C134 C133 H13J 109.4 . . ?
P16 C133 H13J 109.4 . . ?
H13I C133 H13J 108.0 . . ?
C133 C134 H13K 109.5 . . ?
C133 C134 H13L 109.5 . . ?
H13K C134 H13L 109.5 . . ?
C133 C134 H13M 109.5 . . ?
H13K C134 H13M 109.5 . . ?
H13L C134 H13M 109.5 . . ?
C136 C135 P16 116.9(11) . . ?
C136 C135 H13N 108.1 . . ?
P16 C135 H13N 108.1 . . ?
C136 C135 H13O 108.1 . . ?
P16 C135 H13O 108.1 . . ?
H13N C135 H13O 107.3 . . ?
C135 C136 H13P 109.5 . . ?
C135 C136 H13Q 109.5 . . ?
H13P C136 H13Q 109.5 . . ?
C135 C136 H13R 109.5 . . ?
H13P C136 H13R 109.5 . . ?
H13Q C136 H13R 109.5 . . ?
C138 C137 P17 116.3(10) . . ?
C138 C137 H13S 108.2 . . ?
P17 C137 H13S 108.2 . . ?
C138 C137 H13T 108.2 . . ?
P17 C137 H13T 108.2 . . ?
H13S C137 H13T 107.4 . . ?
C137 C138 H13U 109.5 . . ?
C137 C138 H13V 109.5 . . ?
H13U C138 H13V 109.5 . . ?
C137 C138 H13W 109.5 . . ?
H13U C138 H13W 109.5 . . ?
H13V C138 H13W 109.5 . . ?
C140 C139 P17 113.6(9) . . ?
C140 C139 H939 108.8 . . ?
P17 C139 H939 108.8 . . ?
C140 C139 H940 108.8 . . ?
P17 C139 H940 108.8 . . ?
H939 C139 H940 107.7 . . ?
C139 C140 H14A 109.5 . . ?
C139 C140 H14B 109.5 . . ?
H14A C140 H14B 109.5 . . ?
C139 C140 H14C 109.5 . . ?
H14A C140 H14C 109.5 . . ?
H14B C140 H14C 109.5 . . ?
C142 C141 P17 118.3(13) . . ?
C142 C141 H14D 107.7 . . ?
P17 C141 H14D 107.7 . . ?
C142 C141 H14E 107.7 . . ?
P17 C141 H14E 107.7 . . ?
H14D C141 H14E 107.1 . . ?
C141 C142 H14F 109.5 . . ?
C141 C142 H14G 109.5 . . ?
H14F C142 H14G 109.5 . . ?
C141 C142 H14H 109.5 . . ?
H14F C142 H14H 109.5 . . ?
H14G C142 H14H 109.5 . . ?
C144 C143 P18 116.9(12) . . ?
C144 C143 H14I 108.1 . . ?
P18 C143 H14I 108.1 . . ?
C144 C143 H14J 108.1 . . ?
P18 C143 H14J 108.1 . . ?
H14I C143 H14J 107.3 . . ?
C143 C144 H14K 109.5 . . ?
C143 C144 H14L 109.5 . . ?
H14K C144 H14L 109.5 . . ?
C143 C144 H14M 109.5 . . ?
H14K C144 H14M 109.5 . . ?
H14L C144 H14M 109.5 . . ?
C146 C145 P18 112.5(10) . . ?
C146 C145 H14N 109.1 . . ?
P18 C145 H14N 109.1 . . ?
C146 C145 H14O 109.1 . . ?
P18 C145 H14O 109.1 . . ?
H14N C145 H14O 107.8 . . ?
C145 C146 H14P 109.5 . . ?
C145 C146 H14Q 109.5 . . ?
H14P C146 H14Q 109.5 . . ?
C145 C146 H14R 109.5 . . ?
H14P C146 H14R 109.5 . . ?
H14Q C146 H14R 109.5 . . ?
C148 C147 P18 115.5(9) . . ?
C148 C147 H14S 108.4 . . ?
P18 C147 H14S 108.4 . . ?
C148 C147 H14T 108.4 . . ?
P18 C147 H14T 108.4 . . ?
H14S C147 H14T 107.5 . . ?
C147 C148 H14U 109.5 . . ?
C147 C148 H14V 109.5 . . ?
H14U C148 H14V 109.5 . . ?
C147 C148 H14W 109.5 . . ?
H14U C148 H14W 109.5 . . ?
H14V C148 H14W 109.5 . . ?
C150 C149 P19 116.2(11) . . ?
C150 C149 H949 108.2 . . ?
P19 C149 H949 108.2 . . ?
C150 C149 H950 108.2 . . ?
P19 C149 H950 108.2 . . ?
H949 C149 H950 107.4 . . ?
C149 C150 H15A 109.5 . . ?
C149 C150 H15B 109.5 . . ?
H15A C150 H15B 109.5 . . ?
C149 C150 H15C 109.5 . . ?
H15A C150 H15C 109.5 . . ?
H15B C150 H15C 109.5 . . ?
C152 C151 P19 114.7(12) . . ?
C152 C151 H15D 108.6 . . ?
P19 C151 H15D 108.6 . . ?
C152 C151 H15E 108.6 . . ?
P19 C151 H15E 108.6 . . ?
H15D C151 H15E 107.6 . . ?
C151 C152 H15F 109.5 . . ?
C151 C152 H15G 109.5 . . ?
H15F C152 H15G 109.5 . . ?
C151 C152 H15H 109.5 . . ?
H15F C152 H15H 109.5 . . ?
H15G C152 H15H 109.5 . . ?
C154 C153 P19 111.2(11) . . ?
C154 C153 H15I 109.4 . . ?
P19 C153 H15I 109.4 . . ?
C154 C153 H15J 109.4 . . ?
P19 C153 H15J 109.4 . . ?
H15I C153 H15J 108.0 . . ?
C153 C154 H15K 109.5 . . ?
C153 C154 H15L 109.5 . . ?
H15K C154 H15L 109.5 . . ?
C153 C154 H15M 109.5 . . ?
H15K C154 H15M 109.5 . . ?
H15L C154 H15M 109.5 . . ?
C156 C155 P20 114.8(10) . . ?
C156 C155 H15N 108.6 . . ?
P20 C155 H15N 108.6 . . ?
C156 C155 H15O 108.6 . . ?
P20 C155 H15O 108.6 . . ?
H15N C155 H15O 107.5 . . ?
C155 C156 H15P 109.5 . . ?
C155 C156 H15Q 109.5 . . ?
H15P C156 H15Q 109.5 . . ?
C155 C156 H15R 109.5 . . ?
H15P C156 H15R 109.5 . . ?
H15Q C156 H15R 109.5 . . ?
C158 C157 P20 112.9(10) . . ?
C158 C157 H15S 109.0 . . ?
P20 C157 H15S 109.0 . . ?
C158 C157 H15T 109.0 . . ?
P20 C157 H15T 109.0 . . ?
H15S C157 H15T 107.8 . . ?
C157 C158 H15U 109.5 . . ?
C157 C158 H15V 109.5 . . ?
H15U C158 H15V 109.5 . . ?
C157 C158 H15W 109.5 . . ?
H15U C158 H15W 109.5 . . ?
H15V C158 H15W 109.5 . . ?
C160 C159 P20 113.0(10) . . ?
C160 C159 H959 109.0 . . ?
P20 C159 H959 109.0 . . ?
C160 C159 H960 109.0 . . ?
P20 C159 H960 109.0 . . ?
H959 C159 H960 107.8 . . ?
C159 C160 H16A 109.5 . . ?
C159 C160 H16B 109.5 . . ?
H16A C160 H16B 109.5 . . ?
C159 C160 H16C 109.5 . . ?
H16A C160 H16C 109.5 . . ?
H16B C160 H16C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C7 2.087(14) . ?
Pt1 P2 2.286(4) . ?
Pt1 P1 2.315(4) . ?
Pt1 Cl1 2.417(4) . ?
Pt2 C10 2.029(15) . ?
Pt2 P3 2.277(4) . ?
Pt2 P4 2.303(3) . ?
Pt2 Cl2 2.404(3) . ?
Pt3 C13 2.096(14) . ?
Pt3 P5 2.216(3) . ?
Pt3 P6 2.345(3) . ?
Pt3 Cl3 2.373(3) . ?
Pt4 C16 1.993(14) . ?
Pt4 P8 2.294(3) . ?
Pt4 P7 2.302(3) . ?
Pt4 Cl4 2.413(3) . ?
Pt5 C19 2.031(13) . ?
Pt5 P9 2.284(4) . ?
Pt5 P10 2.292(4) . ?
Pt5 Cl5 2.407(3) . ?
P1 C23 1.801(15) . ?
P1 C21 1.813(17) . ?
P1 C25 1.836(14) . ?
P2 C27A 1.826(5) . ?
P2 C27B 1.827(5) . ?
P2 C29B 1.827(5) . ?
P2 C31B 1.827(5) . ?
P2 C29A 1.828(5) . ?
P2 C31A 1.828(5) . ?
P3 C37A 1.825(5) . ?
P3 C35B 1.827(5) . ?
P3 C33A 1.827(5) . ?
P3 C33B 1.827(5) . ?
P3 C37B 1.828(5) . ?
P3 C35A 1.828(5) . ?
P4 C39 1.812(12) . ?
P4 C43 1.814(16) . ?
P4 C41 1.834(13) . ?
P5 C45A 1.825(5) . ?
P5 C45B 1.826(5) . ?
P5 C47B 1.827(5) . ?
P5 C47A 1.827(5) . ?
P5 C49B 1.827(5) . ?
P5 C49A 1.828(5) . ?
P6 C53 1.808(12) . ?
P6 C55 1.813(12) . ?
P6 C51 1.828(12) . ?
P7 C57B 1.827(5) . ?
P7 C59A 1.827(5) . ?
P7 C59B 1.827(5) . ?
P7 C61A 1.827(5) . ?
P7 C57A 1.827(5) . ?
P7 C61B 1.827(5) . ?
P8 C65A 1.824(5) . ?
P8 C67B 1.825(5) . ?
P8 C67A 1.826(5) . ?
P8 C63B 1.827(5) . ?
P8 C65B 1.828(5) . ?
P8 C63A 1.829(5) . ?
P9 C71 1.775(17) . ?
P9 C73 1.83(2) . ?
P9 C69 1.905(18) . ?
P10 C79A 1.826(5) . ?
P10 C79B 1.826(5) . ?
P10 C77B 1.826(5) . ?
P10 C75A 1.827(5) . ?
P10 C77A 1.829(5) . ?
P10 C75B 1.830(5) . ?
C1 C6 1.393(16) . ?
C1 C5 1.424(16) . ?
C1 C2 1.437(17) . ?
C2 C3 1.378(15) . ?
C2 C9 1.399(16) . ?
C3 C4 1.371(17) . ?
C3 C12 1.433(17) . ?
C4 C5 1.349(17) . ?
C4 C15 1.426(16) . ?
C5 C18 1.420(16) . ?
C6 C7 1.403(17) . ?
C6 C20 1.446(17) . ?
C7 C8 1.464(18) . ?
C8 C9 1.446(16) . ?
C8 H8 0.9500 . ?
C9 C10 1.438(18) . ?
C10 C11 1.447(17) . ?
C11 C12 1.391(16) . ?
C11 H11 0.9500 . ?
C12 C13 1.430(17) . ?
C13 C14 1.426(16) . ?
C14 C15 1.399(17) . ?
C14 H14 0.9500 . ?
C15 C16 1.431(18) . ?
C16 C17 1.479(18) . ?
C17 C18 1.420(17) . ?
C17 H17 0.9500 . ?
C18 C19 1.411(17) . ?
C19 C20 1.462(18) . ?
C20 H20 0.9500 . ?
C21 C22 1.50(2) . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 C24 1.51(2) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.47(2) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27A C28A 1.521(6) . ?
C27A H27A 0.9900 . ?
C27A H27B 0.9900 . ?
C28A H28A 0.9800 . ?
C28A H28B 0.9800 . ?
C28A H28C 0.9800 . ?
C29A C30A 1.521(6) . ?
C29A H29A 0.9900 . ?
C29A H29B 0.9900 . ?
C30A H30A 0.9800 . ?
C30A H30B 0.9800 . ?
C30A H30C 0.9800 . ?
C31A C32A 1.521(6) . ?
C31A H31A 0.9900 . ?
C31A H31B 0.9900 . ?
C32A H32A 0.9800 . ?
C32A H32B 0.9800 . ?
C32A H32C 0.9800 . ?
C27B C28B 1.521(6) . ?
C27B H27C 0.9900 . ?
C27B H27D 0.9900 . ?
C28B H28D 0.9800 . ?
C28B H28E 0.9800 . ?
C28B H28F 0.9800 . ?
C29B C30B 1.521(6) . ?
C29B H29C 0.9900 . ?
C29B H29D 0.9900 . ?
C30B H30D 0.9800 . ?
C30B H30E 0.9800 . ?
C30B H30F 0.9800 . ?
C31B C32B 1.521(6) . ?
C31B H31C 0.9900 . ?
C31B H31D 0.9900 . ?
C32B H32D 0.9800 . ?
C32B H32E 0.9800 . ?
C32B H32F 0.9800 . ?
C33A C34A 1.521(6) . ?
C33A H33A 0.9900 . ?
C33A H33B 0.9900 . ?
C34A H34A 0.9800 . ?
C34A H34B 0.9800 . ?
C34A H34C 0.9800 . ?
C35A C36A 1.519(6) . ?
C35A H35A 0.9900 . ?
C35A H35B 0.9900 . ?
C36A H36A 0.9800 . ?
C36A H36B 0.9800 . ?
C36A H36C 0.9800 . ?
C37A C38A 1.523(6) . ?
C37A H37A 0.9900 . ?
C37A H37B 0.9900 . ?
C38A H38A 0.9800 . ?
C38A H38B 0.9800 . ?
C38A H38C 0.9800 . ?
C33B C34B 1.521(6) . ?
C33B H33C 0.9900 . ?
C33B H33D 0.9900 . ?
C34B H34D 0.9800 . ?
C34B H34E 0.9800 . ?
C34B H34F 0.9800 . ?
C35B C36B 1.521(6) . ?
C35B H35C 0.9900 . ?
C35B H35D 0.9900 . ?
C36B H36D 0.9800 . ?
C36B H36E 0.9800 . ?
C36B H36F 0.9800 . ?
C37B C38B 1.521(6) . ?
C37B H37C 0.9900 . ?
C37B H37D 0.9900 . ?
C38B H38D 0.9800 . ?
C38B H38E 0.9800 . ?
C38B H38F 0.9800 . ?
C39 C40 1.531(19) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 C42 1.49(2) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.50(2) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 H44C 0.9800 . ?
C45A C46A 1.520(6) . ?
C45A H45A 0.9900 . ?
C45A H45B 0.9900 . ?
C46A H46A 0.9800 . ?
C46A H46B 0.9800 . ?
C46A H46C 0.9800 . ?
C47A C48A 1.521(6) . ?
C47A H47A 0.9900 . ?
C47A H47B 0.9900 . ?
C48A H48A 0.9800 . ?
C48A H48B 0.9800 . ?
C48A H48C 0.9800 . ?
C49A C50A 1.521(6) . ?
C49A H49A 0.9900 . ?
C49A H49B 0.9900 . ?
C50A H50A 0.9800 . ?
C50A H50B 0.9800 . ?
C50A H50C 0.9800 . ?
C45B C46B 1.520(6) . ?
C45B H45C 0.9900 . ?
C45B H45D 0.9900 . ?
C46B H46D 0.9800 . ?
C46B H46E 0.9800 . ?
C46B H46F 0.9800 . ?
C47B C48B 1.521(6) . ?
C47B H47C 0.9900 . ?
C47B H47D 0.9900 . ?
C48B H48D 0.9800 . ?
C48B H48E 0.9800 . ?
C48B H48F 0.9800 . ?
C49B C50B 1.521(6) . ?
C49B H49C 0.9900 . ?
C49B H49D 0.9900 . ?
C50B H50D 0.9800 . ?
C50B H50E 0.9800 . ?
C50B H50F 0.9800 . ?
C51 C52 1.520(18) . ?
C51 H51A 0.9900 . ?
C51 H51B 0.9900 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 C54 1.538(18) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C55 C56 1.516(17) . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C56 H56A 0.9800 . ?
C56 H56B 0.9800 . ?
C56 H56C 0.9800 . ?
C57A C58A 1.521(6) . ?
C57A H57A 0.9900 . ?
C57A H57B 0.9900 . ?
C58A H58A 0.9800 . ?
C58A H58B 0.9800 . ?
C58A H58C 0.9800 . ?
C59A C60A 1.521(6) . ?
C59A H59A 0.9900 . ?
C59A H59B 0.9900 . ?
C60A H60A 0.9800 . ?
C60A H60B 0.9800 . ?
C60A H60C 0.9800 . ?
C61A C62A 1.520(6) . ?
C61A H61A 0.9900 . ?
C61A H61B 0.9900 . ?
C62A H62A 0.9800 . ?
C62A H62B 0.9800 . ?
C62A H62C 0.9800 . ?
C57B C58B 1.521(6) . ?
C57B H57C 0.9900 . ?
C57B H57D 0.9900 . ?
C58B H58D 0.9800 . ?
C58B H58E 0.9800 . ?
C58B H58F 0.9800 . ?
C59B C60B 1.521(6) . ?
C59B H59C 0.9900 . ?
C59B H59D 0.9900 . ?
C60B H60D 0.9800 . ?
C60B H60E 0.9800 . ?
C60B H60F 0.9800 . ?
C61B C62B 1.521(6) . ?
C61B H61C 0.9900 . ?
C61B H61D 0.9900 . ?
C62B H62D 0.9800 . ?
C62B H62E 0.9800 . ?
C62B H62F 0.9800 . ?
C63A C64A 1.520(6) . ?
C63A H63A 0.9900 . ?
C63A H63B 0.9900 . ?
C64A H64A 0.9800 . ?
C64A H64B 0.9800 . ?
C64A H64C 0.9800 . ?
C65A C66A 1.521(6) . ?
C65A H65A 0.9900 . ?
C65A H65B 0.9900 . ?
C66A H66A 0.9800 . ?
C66A H66B 0.9800 . ?
C66A H66C 0.9800 . ?
C67A C68A 1.520(6) . ?
C67A H67A 0.9900 . ?
C67A H67B 0.9900 . ?
C68A H68A 0.9800 . ?
C68A H68B 0.9800 . ?
C68A H68C 0.9800 . ?
C63B C64B 1.522(6) . ?
C63B H63C 0.9900 . ?
C63B H63D 0.9900 . ?
C64B H64D 0.9800 . ?
C64B H64E 0.9800 . ?
C64B H64F 0.9800 . ?
C65B C66B 1.519(6) . ?
C65B H65C 0.9900 . ?
C65B H65D 0.9900 . ?
C66B H66D 0.9800 . ?
C66B H66E 0.9800 . ?
C66B H66F 0.9800 . ?
C67B C68B 1.520(6) . ?
C67B H67C 0.9900 . ?
C67B H67D 0.9900 . ?
C68B H68D 0.9800 . ?
C68B H68E 0.9800 . ?
C68B H68F 0.9800 . ?
C69 C70 1.47(2) . ?
C69 H69A 0.9900 . ?
C69 H69B 0.9900 . ?
C70 H70A 0.9800 . ?
C70 H70B 0.9800 . ?
C70 H70C 0.9800 . ?
C71 C72 1.57(3) . ?
C71 H71A 0.9900 . ?
C71 H71B 0.9900 . ?
C72 H72A 0.9800 . ?
C72 H72B 0.9800 . ?
C72 H72C 0.9800 . ?
C73 C74 1.45(2) . ?
C73 H73A 0.9900 . ?
C73 H73B 0.9900 . ?
C74 H74A 0.9800 . ?
C74 H74B 0.9800 . ?
C74 H74C 0.9800 . ?
C75A C76A 1.522(6) . ?
C75A H75A 0.9900 . ?
C75A H75B 0.9900 . ?
C76A H76A 0.9800 . ?
C76A H76B 0.9800 . ?
C76A H76C 0.9800 . ?
C77A C78A 1.520(6) . ?
C77A H77A 0.9900 . ?
C77A H77B 0.9900 . ?
C78A H78A 0.9800 . ?
C78A H78B 0.9800 . ?
C78A H78C 0.9800 . ?
C79A C80A 1.520(6) . ?
C79A H79A 0.9900 . ?
C79A H79B 0.9900 . ?
C80A H80A 0.9800 . ?
C80A H80B 0.9800 . ?
C80A H80C 0.9800 . ?
C75B C76B 1.521(6) . ?
C75B H75C 0.9900 . ?
C75B H75D 0.9900 . ?
C76B H76D 0.9800 . ?
C76B H76E 0.9800 . ?
C76B H76F 0.9800 . ?
C77B C78B 1.521(6) . ?
C77B H77C 0.9900 . ?
C77B H77D 0.9900 . ?
C78B H78D 0.9800 . ?
C78B H78E 0.9800 . ?
C78B H78F 0.9800 . ?
C79B C80B 1.520(6) . ?
C79B H79C 0.9900 . ?
C79B H79D 0.9900 . ?
C80B H80D 0.9800 . ?
C80B H80E 0.9800 . ?
C80B H80F 0.9800 . ?
Pt6 C87 2.029(13) . ?
Pt6 P11 2.299(4) . ?
Pt6 P12 2.307(4) . ?
Pt6 Cl6 2.409(3) . ?
Pt7 C90 2.000(11) . ?
Pt7 P14 2.290(3) . ?
Pt7 P13 2.304(4) . ?
Pt7 Cl7 2.406(3) . ?
Pt8 C93 2.047(11) . ?
Pt8 P16 2.278(4) . ?
Pt8 P15 2.319(4) . ?
Pt8 Cl8 2.413(3) . ?
Pt9 C96 2.000(12) . ?
Pt9 P17 2.285(3) . ?
Pt9 P18 2.307(3) . ?
Pt9 Cl9 2.421(3) . ?
Pt10 C99 2.066(12) . ?
Pt10 P20 2.230(3) . ?
Pt10 P19 2.359(3) . ?
Pt10 Cl10 2.392(3) . ?
P11 C101 1.826(5) . ?
P11 C205 1.826(5) . ?
P11 C201 1.826(5) . ?
P11 C103 1.827(5) . ?
P11 C105 1.828(5) . ?
P11 C203 1.828(5) . ?
P12 C111 1.827(5) . ?
P12 C107 1.827(5) . ?
P12 C211 1.827(5) . ?
P12 C209 1.827(5) . ?
P12 C109 1.827(5) . ?
P12 C207 1.83(3) . ?
P13 C215 1.826(5) . ?
P13 C213 1.826(5) . ?
P13 C113 1.827(5) . ?
P13 C117 1.828(5) . ?
P13 C217 1.830(5) . ?
P13 C115 1.830(5) . ?
P14 C221 1.827(5) . ?
P14 C121 1.827(5) . ?
P14 C223 1.827(5) . ?
P14 C119 1.827(5) . ?
P14 C219 1.827(5) . ?
P14 C123 1.828(5) . ?
P15 C129 1.827(14) . ?
P15 C127 1.838(13) . ?
P15 C125 1.854(14) . ?
P16 C135 1.825(15) . ?
P16 C131 1.831(16) . ?
P16 C133 1.838(15) . ?
P17 C139 1.811(13) . ?
P17 C137 1.811(13) . ?
P17 C141 1.847(14) . ?
P18 C147 1.820(12) . ?
P18 C143 1.833(13) . ?
P18 C145 1.841(14) . ?
P19 C151 1.794(14) . ?
P19 C153 1.828(13) . ?
P19 C149 1.838(13) . ?
P20 C159 1.810(14) . ?
P20 C155 1.827(13) . ?
P20 C157 1.829(14) . ?
C81 C82 1.376(16) . ?
C81 C86 1.398(15) . ?
C81 C85 1.408(15) . ?
C82 C89 1.385(16) . ?
C82 C83 1.423(16) . ?
C83 C92 1.392(15) . ?
C83 C84 1.398(15) . ?
C84 C85 1.400(16) . ?
C84 C95 1.410(15) . ?
C85 C98 1.376(15) . ?
C86 C87 1.439(16) . ?
C86 C100 1.453(16) . ?
C87 C88 1.405(17) . ?
C88 C89 1.437(16) . ?
C88 H88 0.9500 . ?
C89 C90 1.454(16) . ?
C90 C91 1.445(16) . ?
C91 C92 1.432(15) . ?
C91 H91 0.9500 . ?
C92 C93 1.441(16) . ?
C93 C94 1.397(16) . ?
C94 C95 1.443(15) . ?
C94 H94 0.9500 . ?
C95 C96 1.462(16) . ?
C96 C97 1.430(15) . ?
C97 C98 1.416(15) . ?
C97 H97 0.9500 . ?
C98 C99 1.456(16) . ?
C99 C100 1.406(16) . ?
C100 H100 0.9500 . ?
C101 C102 1.521(6) . ?
C101 H10A 0.9900 . ?
C101 H10B 0.9900 . ?
C102 H10C 0.9800 . ?
C102 H10D 0.9800 . ?
C102 H10E 0.9800 . ?
C103 C104 1.522(6) . ?
C103 H10F 0.9900 . ?
C103 H10G 0.9900 . ?
C104 H10H 0.9800 . ?
C104 H10I 0.9800 . ?
C104 H10J 0.9800 . ?
C105 C106 1.520(6) . ?
C105 H10K 0.9900 . ?
C105 H10L 0.9900 . ?
C106 H10M 0.9800 . ?
C106 H10N 0.9800 . ?
C106 H10O 0.9800 . ?
C201 C202 1.521(6) . ?
C201 H20A 0.9900 . ?
C201 H20B 0.9900 . ?
C202 H20C 0.9800 . ?
C202 H20D 0.9800 . ?
C202 H20E 0.9800 . ?
C203 C204 1.520(6) . ?
C203 H20F 0.9900 . ?
C203 H20G 0.9900 . ?
C204 H20H 0.9800 . ?
C204 H20I 0.9800 . ?
C204 H20J 0.9800 . ?
C205 C206 1.521(6) . ?
C205 H20K 0.9900 . ?
C205 H20L 0.9900 . ?
C206 H20M 0.9800 . ?
C206 H20N 0.9800 . ?
C206 H20O 0.9800 . ?
C107 C108 1.521(6) . ?
C107 H10P 0.9900 . ?
C107 H10Q 0.9900 . ?
C108 H10R 0.9800 . ?
C108 H10S 0.9800 . ?
C108 H10T 0.9800 . ?
C109 C110 1.522(6) . ?
C109 H10U 0.9900 . ?
C109 H10V 0.9900 . ?
C110 H11A 0.9800 . ?
C110 H11B 0.9800 . ?
C110 H11C 0.9800 . ?
C111 C112 1.521(6) . ?
C111 H11D 0.9900 . ?
C111 H11E 0.9900 . ?
C112 H11F 0.9800 . ?
C112 H11G 0.9800 . ?
C112 H11H 0.9800 . ?
C207 C208 1.521(6) . ?
C207 H20P 0.9900 . ?
C207 H20Q 0.9900 . ?
C208 H20R 0.9800 . ?
C208 H20S 0.9800 . ?
C208 H20T 0.9800 . ?
C209 C210 1.521(6) . ?
C209 H20U 0.9900 . ?
C209 H20V 0.9900 . ?
C210 H21C 0.9800 . ?
C210 H21D 0.9800 . ?
C210 H21E 0.9800 . ?
C211 C212 1.521(6) . ?
C211 H21F 0.9900 . ?
C211 H21G 0.9900 . ?
C212 H21H 0.9800 . ?
C212 H21I 0.9800 . ?
C212 H21J 0.9800 . ?
C113 C114 1.520(6) . ?
C113 H11I 0.9900 . ?
C113 H11J 0.9900 . ?
C114 H11K 0.9800 . ?
C114 H11L 0.9800 . ?
C114 H11M 0.9800 . ?
C115 C116 1.520(6) . ?
C115 H11N 0.9900 . ?
C115 H11O 0.9900 . ?
C116 H11P 0.9800 . ?
C116 H11Q 0.9800 . ?
C116 H11R 0.9800 . ?
C117 C118 1.522(6) . ?
C117 H11S 0.9900 . ?
C117 H11T 0.9900 . ?
C118 H11U 0.9800 . ?
C118 H11V 0.9800 . ?
C118 H11W 0.9800 . ?
C213 C214 1.521(6) . ?
C213 H21K 0.9900 . ?
C213 H21L 0.9900 . ?
C214 H21M 0.9800 . ?
C214 H21N 0.9800 . ?
C214 H21O 0.9800 . ?
C215 C216 1.522(6) . ?
C215 H21P 0.9900 . ?
C215 H21Q 0.9900 . ?
C216 H21R 0.9800 . ?
C216 H21S 0.9800 . ?
C216 H21T 0.9800 . ?
C217 C218 1.521(6) . ?
C217 H21U 0.9900 . ?
C217 H21V 0.9900 . ?
C218 H916 0.9800 . ?
C218 H917 0.9800 . ?
C218 H918 0.9800 . ?
C119 C120 1.521(6) . ?
C119 H914 0.9900 . ?
C119 H915 0.9900 . ?
C120 H12A 0.9800 . ?
C120 H12B 0.9800 . ?
C120 H12C 0.9800 . ?
C121 C122 1.521(6) . ?
C121 H12D 0.9900 . ?
C121 H12E 0.9900 . ?
C122 H12F 0.9800 . ?
C122 H12G 0.9800 . ?
C122 H12H 0.9800 . ?
C123 C124 1.521(6) . ?
C123 H12I 0.9900 . ?
C123 H12J 0.9900 . ?
C124 H12K 0.9800 . ?
C124 H12L 0.9800 . ?
C124 H12M 0.9800 . ?
C219 C220 1.521(6) . ?
C219 H919 0.9900 . ?
C219 H920 0.9900 . ?
C220 H22D 0.9800 . ?
C220 H22E 0.9800 . ?
C220 H22F 0.9800 . ?
C221 C222 1.521(6) . ?
C221 H22G 0.9900 . ?
C221 H22H 0.9900 . ?
C222 H22I 0.9800 . ?
C222 H22J 0.9800 . ?
C222 H22K 0.9800 . ?
C223 C224 1.520(6) . ?
C223 H22L 0.9900 . ?
C223 H22M 0.9900 . ?
C224 H22N 0.9800 . ?
C224 H22O 0.9800 . ?
C224 H22P 0.9800 . ?
C125 C126 1.506(18) . ?
C125 H12N 0.9900 . ?
C125 H12O 0.9900 . ?
C126 H12P 0.9800 . ?
C126 H12Q 0.9800 . ?
C126 H12R 0.9800 . ?
C127 C128 1.549(19) . ?
C127 H12S 0.9900 . ?
C127 H12T 0.9900 . ?
C128 H12U 0.9800 . ?
C128 H12V 0.9800 . ?
C128 H12W 0.9800 . ?
C129 C130 1.514(19) . ?
C129 H929 0.9900 . ?
C129 H930 0.9900 . ?
C130 H13A 0.9800 . ?
C130 H13B 0.9800 . ?
C130 H13C 0.9800 . ?
C131 C132 1.520(6) . ?
C131 C232 1.522(6) . ?
C131 H931 0.9900 . ?
C131 H932 0.9900 . ?
C131 H933 0.9900 . ?
C131 H934 0.9900 . ?
C132 H13F 0.9800 . ?
C132 H13G 0.9800 . ?
C132 H13H 0.9800 . ?
C232 H23C 0.9800 . ?
C232 H23D 0.9800 . ?
C232 H23E 0.9800 . ?
C133 C134 1.50(2) . ?
C133 H13I 0.9900 . ?
C133 H13J 0.9900 . ?
C134 H13K 0.9800 . ?
C134 H13L 0.9800 . ?
C134 H13M 0.9800 . ?
C135 C136 1.53(2) . ?
C135 H13N 0.9900 . ?
C135 H13O 0.9900 . ?
C136 H13P 0.9800 . ?
C136 H13Q 0.9800 . ?
C136 H13R 0.9800 . ?
C137 C138 1.504(19) . ?
C137 H13S 0.9900 . ?
C137 H13T 0.9900 . ?
C138 H13U 0.9800 . ?
C138 H13V 0.9800 . ?
C138 H13W 0.9800 . ?
C139 C140 1.491(19) . ?
C139 H939 0.9900 . ?
C139 H940 0.9900 . ?
C140 H14A 0.9800 . ?
C140 H14B 0.9800 . ?
C140 H14C 0.9800 . ?
C141 C142 1.45(2) . ?
C141 H14D 0.9900 . ?
C141 H14E 0.9900 . ?
C142 H14F 0.9800 . ?
C142 H14G 0.9800 . ?
C142 H14H 0.9800 . ?
C143 C144 1.53(2) . ?
C143 H14I 0.9900 . ?
C143 H14J 0.9900 . ?
C144 H14K 0.9800 . ?
C144 H14L 0.9800 . ?
C144 H14M 0.9800 . ?
C145 C146 1.530(19) . ?
C145 H14N 0.9900 . ?
C145 H14O 0.9900 . ?
C146 H14P 0.9800 . ?
C146 H14Q 0.9800 . ?
C146 H14R 0.9800 . ?
C147 C148 1.538(18) . ?
C147 H14S 0.9900 . ?
C147 H14T 0.9900 . ?
C148 H14U 0.9800 . ?
C148 H14V 0.9800 . ?
C148 H14W 0.9800 . ?
C149 C150 1.532(19) . ?
C149 H949 0.9900 . ?
C149 H950 0.9900 . ?
C150 H15A 0.9800 . ?
C150 H15B 0.9800 . ?
C150 H15C 0.9800 . ?
C151 C152 1.50(2) . ?
C151 H15D 0.9900 . ?
C151 H15E 0.9900 . ?
C152 H15F 0.9800 . ?
C152 H15G 0.9800 . ?
C152 H15H 0.9800 . ?
C153 C154 1.53(2) . ?
C153 H15I 0.9900 . ?
C153 H15J 0.9900 . ?
C154 H15K 0.9800 . ?
C154 H15L 0.9800 . ?
C154 H15M 0.9800 . ?
C155 C156 1.554(19) . ?
C155 H15N 0.9900 . ?
C155 H15O 0.9900 . ?
C156 H15P 0.9800 . ?
C156 H15Q 0.9800 . ?
C156 H15R 0.9800 . ?
C157 C158 1.52(2) . ?
C157 H15S 0.9900 . ?
C157 H15T 0.9900 . ?
C158 H15U 0.9800 . ?
C158 H15V 0.9800 . ?
C158 H15W 0.9800 . ?
C159 C160 1.54(2) . ?
C159 H959 0.9900 . ?
C159 H960 0.9900 . ?
C160 H16A 0.9800 . ?
C160 H16B 0.9800 . ?
C160 H16C 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C7 Pt1 P1 C23 -150.2(7) . . . . ?
P2 Pt1 P1 C23 106.7(16) . . . . ?
Cl1 Pt1 P1 C23 30.9(6) . . . . ?
C7 Pt1 P1 C21 92.7(7) . . . . ?
P2 Pt1 P1 C21 -10.4(17) . . . . ?
Cl1 Pt1 P1 C21 -86.3(6) . . . . ?
C7 Pt1 P1 C25 -26.0(7) . . . . ?
P2 Pt1 P1 C25 -129.1(15) . . . . ?
Cl1 Pt1 P1 C25 155.1(6) . . . . ?
C7 Pt1 P2 C27A 14(2) . . . . ?
P1 Pt1 P2 C27A 118(3) . . . . ?
Cl1 Pt1 P2 C27A -167(2) . . . . ?
C7 Pt1 P2 C27B 18(4) . . . . ?
P1 Pt1 P2 C27B 121(4) . . . . ?
Cl1 Pt1 P2 C27B -163(4) . . . . ?
C7 Pt1 P2 C29B 146.7(18) . . . . ?
P1 Pt1 P2 C29B -110(2) . . . . ?
Cl1 Pt1 P2 C29B -34.4(18) . . . . ?
C7 Pt1 P2 C31B -90.9(18) . . . . ?
P1 Pt1 P2 C31B 12(2) . . . . ?
Cl1 Pt1 P2 C31B 88.1(17) . . . . ?
C7 Pt1 P2 C29A 130.3(12) . . . . ?
P1 Pt1 P2 C29A -126.6(18) . . . . ?
Cl1 Pt1 P2 C29A -50.7(11) . . . . ?
C7 Pt1 P2 C31A -115.7(9) . . . . ?
P1 Pt1 P2 C31A -12.7(18) . . . . ?
Cl1 Pt1 P2 C31A 63.2(8) . . . . ?
C10 Pt2 P3 C37A -127.6(7) . . . . ?
P4 Pt2 P3 C37A 127.6(10) . . . . ?
Cl2 Pt2 P3 C37A 51.8(6) . . . . ?
C10 Pt2 P3 C35B 149.2(18) . . . . ?
P4 Pt2 P3 C35B 44(2) . . . . ?
Cl2 Pt2 P3 C35B -31.3(17) . . . . ?
C10 Pt2 P3 C33A 0.9(19) . . . . ?
P4 Pt2 P3 C33A -104(2) . . . . ?
Cl2 Pt2 P3 C33A -179.7(19) . . . . ?
C10 Pt2 P3 C33B -10(5) . . . . ?
P4 Pt2 P3 C33B -115(5) . . . . ?
Cl2 Pt2 P3 C33B 169(5) . . . . ?
C10 Pt2 P3 C37B -96(2) . . . . ?
P4 Pt2 P3 C37B 159(2) . . . . ?
Cl2 Pt2 P3 C37B 83(2) . . . . ?
C10 Pt2 P3 C35A 120.3(8) . . . . ?
P4 Pt2 P3 C35A 15.6(12) . . . . ?
Cl2 Pt2 P3 C35A -60.2(7) . . . . ?
C10 Pt2 P4 C39 115.4(6) . . . . ?
P3 Pt2 P4 C39 -140.0(9) . . . . ?
Cl2 Pt2 P4 C39 -64.1(5) . . . . ?
C10 Pt2 P4 C43 -128.5(7) . . . . ?
P3 Pt2 P4 C43 -23.9(11) . . . . ?
Cl2 Pt2 P4 C43 52.0(6) . . . . ?
C10 Pt2 P4 C41 -9.8(7) . . . . ?
P3 Pt2 P4 C41 94.8(10) . . . . ?
Cl2 Pt2 P4 C41 170.7(6) . . . . ?
C13 Pt3 P5 C45A -119.4(14) . . . . ?
P6 Pt3 P5 C45A 61.2(14) . . . . ?
Cl3 Pt3 P5 C45A -168.6(17) . . . . ?
C13 Pt3 P5 C45B -129(2) . . . . ?
P6 Pt3 P5 C45B 52(2) . . . . ?
Cl3 Pt3 P5 C45B -178(19) . . . . ?
C13 Pt3 P5 C47B -4(3) . . . . ?
P6 Pt3 P5 C47B 177(3) . . . . ?
Cl3 Pt3 P5 C47B -53(3) . . . . ?
C13 Pt3 P5 C47A 1(2) . . . . ?
P6 Pt3 P5 C47A -179(2) . . . . ?
Cl3 Pt3 P5 C47A -49(3) . . . . ?
C13 Pt3 P5 C49B 121(2) . . . . ?
P6 Pt3 P5 C49B -58(2) . . . . ?
Cl3 Pt3 P5 C49B 72(3) . . . . ?
C13 Pt3 P5 C49A 110.3(17) . . . . ?
P6 Pt3 P5 C49A -69.2(17) . . . . ?
Cl3 Pt3 P5 C49A 61(2) . . . . ?
C13 Pt3 P6 C53 -59(3) . . . . ?
P5 Pt3 P6 C53 116.0(5) . . . . ?
Cl3 Pt3 P6 C53 -58.6(5) . . . . ?
C13 Pt3 P6 C55 56(3) . . . . ?
P5 Pt3 P6 C55 -128.9(4) . . . . ?
Cl3 Pt3 P6 C55 56.5(4) . . . . ?
C13 Pt3 P6 C51 180(100) . . . . ?
P5 Pt3 P6 C51 -4.8(6) . . . . ?
Cl3 Pt3 P6 C51 -179.4(6) . . . . ?
C16 Pt4 P7 C57B -28.0(14) . . . . ?
P8 Pt4 P7 C57B -97(2) . . . . ?
Cl4 Pt4 P7 C57B 152.3(14) . . . . ?
C16 Pt4 P7 C59A -158(3) . . . . ?
P8 Pt4 P7 C59A 133(3) . . . . ?
Cl4 Pt4 P7 C59A 22(2) . . . . ?
C16 Pt4 P7 C59B -157(4) . . . . ?
P8 Pt4 P7 C59B 134(4) . . . . ?
Cl4 Pt4 P7 C59B 23(4) . . . . ?
C16 Pt4 P7 C61A 76.6(13) . . . . ?
P8 Pt4 P7 C61A 7(2) . . . . ?
Cl4 Pt4 P7 C61A -103.2(13) . . . . ?
C16 Pt4 P7 C57A -41.2(11) . . . . ?
P8 Pt4 P7 C57A -110.7(18) . . . . ?
Cl4 Pt4 P7 C57A 139.1(10) . . . . ?
C16 Pt4 P7 C61B 89.0(17) . . . . ?
P8 Pt4 P7 C61B 19(2) . . . . ?
Cl4 Pt4 P7 C61B -90.7(16) . . . . ?
C16 Pt4 P8 C65A -141.4(8) . . . . ?
P7 Pt4 P8 C65A -72.0(17) . . . . ?
Cl4 Pt4 P8 C65A 38.2(7) . . . . ?
C16 Pt4 P8 C67B 11.4(11) . . . . ?
P7 Pt4 P8 C67B 80.8(19) . . . . ?
Cl4 Pt4 P8 C67B -169.0(11) . . . . ?
C16 Pt4 P8 C67A -11.5(10) . . . . ?
P7 Pt4 P8 C67A 57.8(18) . . . . ?
Cl4 Pt4 P8 C67A 168.1(9) . . . . ?
C16 Pt4 P8 C63B 144.5(9) . . . . ?
P7 Pt4 P8 C63B -146.1(16) . . . . ?
Cl4 Pt4 P8 C63B -35.9(8) . . . . ?
C16 Pt4 P8 C65B -101.0(9) . . . . ?
P7 Pt4 P8 C65B -31.6(17) . . . . ?
Cl4 Pt4 P8 C65B 78.6(8) . . . . ?
C16 Pt4 P8 C63A 99.9(9) . . . . ?
P7 Pt4 P8 C63A 169.2(16) . . . . ?
Cl4 Pt4 P8 C63A -80.5(8) . . . . ?
C19 Pt5 P9 C71 -142.7(9) . . . . ?
P10 Pt5 P9 C71 -52(8) . . . . ?
Cl5 Pt5 P9 C71 35.6(8) . . . . ?
C19 Pt5 P9 C73 -11.4(11) . . . . ?
P10 Pt5 P9 C73 79(8) . . . . ?
Cl5 Pt5 P9 C73 166.8(10) . . . . ?
C19 Pt5 P9 C69 99.3(8) . . . . ?
P10 Pt5 P9 C69 -170(100) . . . . ?
Cl5 Pt5 P9 C69 -82.5(7) . . . . ?
C19 Pt5 P10 C79A -143.1(10) . . . . ?
P9 Pt5 P10 C79A 126(8) . . . . ?
Cl5 Pt5 P10 C79A 38.6(9) . . . . ?
C19 Pt5 P10 C79B -138(2) . . . . ?
P9 Pt5 P10 C79B 131(8) . . . . ?
Cl5 Pt5 P10 C79B 43.5(19) . . . . ?
C19 Pt5 P10 C77B 6.4(11) . . . . ?
P9 Pt5 P10 C77B -84(8) . . . . ?
Cl5 Pt5 P10 C77B -171.9(10) . . . . ?
C19 Pt5 P10 C75A 81.6(7) . . . . ?
P9 Pt5 P10 C75A -9(8) . . . . ?
Cl5 Pt5 P10 C75A -96.7(6) . . . . ?
C19 Pt5 P10 C77A -28.1(11) . . . . ?
P9 Pt5 P10 C77A -119(8) . . . . ?
Cl5 Pt5 P10 C77A 153.6(11) . . . . ?
C19 Pt5 P10 C75B 129.8(9) . . . . ?
P9 Pt5 P10 C75B 39(8) . . . . ?
Cl5 Pt5 P10 C75B -48.5(9) . . . . ?
C6 C1 C2 C3 -157.2(11) . . . . ?
C5 C1 C2 C3 0.1(12) . . . . ?
C6 C1 C2 C9 -2.8(17) . . . . ?
C5 C1 C2 C9 154.4(10) . . . . ?
C9 C2 C3 C4 -152.2(11) . . . . ?
C1 C2 C3 C4 -0.7(13) . . . . ?
C9 C2 C3 C12 5.5(17) . . . . ?
C1 C2 C3 C12 157.0(10) . . . . ?
C2 C3 C4 C5 1.1(14) . . . . ?
C12 C3 C4 C5 -154.6(11) . . . . ?
C2 C3 C4 C15 157.2(11) . . . . ?
C12 C3 C4 C15 1.5(19) . . . . ?
C3 C4 C5 C18 154.5(12) . . . . ?
C15 C4 C5 C18 -1(2) . . . . ?
C3 C4 C5 C1 -1.0(14) . . . . ?
C15 C4 C5 C1 -156.5(11) . . . . ?
C6 C1 C5 C4 158.3(12) . . . . ?
C2 C1 C5 C4 0.6(13) . . . . ?
C6 C1 C5 C18 1.5(19) . . . . ?
C2 C1 C5 C18 -156.2(11) . . . . ?
C5 C1 C6 C7 -164.3(11) . . . . ?
C2 C1 C6 C7 -11.4(17) . . . . ?
C5 C1 C6 C20 8.5(18) . . . . ?
C2 C1 C6 C20 161.4(11) . . . . ?
C1 C6 C7 C8 15.4(17) . . . . ?
C20 C6 C7 C8 -155.6(14) . . . . ?
C1 C6 C7 Pt1 -164.0(8) . . . . ?
C20 C6 C7 Pt1 25.0(19) . . . . ?
P2 Pt1 C7 C6 -104.2(9) . . . . ?
P1 Pt1 C7 C6 80.8(9) . . . . ?
Cl1 Pt1 C7 C6 180(100) . . . . ?
P2 Pt1 C7 C8 76.3(9) . . . . ?
P1 Pt1 C7 C8 -98.6(9) . . . . ?
Cl1 Pt1 C7 C8 1(21) . . . . ?
C6 C7 C8 C9 -6.1(17) . . . . ?
Pt1 C7 C8 C9 173.3(8) . . . . ?
C3 C2 C9 C10 -8.6(16) . . . . ?
C1 C2 C9 C10 -157.3(10) . . . . ?
C3 C2 C9 C8 161.6(11) . . . . ?
C1 C2 C9 C8 12.8(15) . . . . ?
C7 C8 C9 C2 -8.7(16) . . . . ?
C7 C8 C9 C10 159.7(11) . . . . ?
C2 C9 C10 C11 2.2(15) . . . . ?
C8 C9 C10 C11 -166.5(11) . . . . ?
C2 C9 C10 Pt2 179.1(8) . . . . ?
C8 C9 C10 Pt2 10.4(16) . . . . ?
P3 Pt2 C10 C9 85.1(9) . . . . ?
P4 Pt2 C10 C9 -104.2(9) . . . . ?
Cl2 Pt2 C10 C9 40(27) . . . . ?
P3 Pt2 C10 C11 -98.0(9) . . . . ?
P4 Pt2 C10 C11 72.7(9) . . . . ?
Cl2 Pt2 C10 C11 -143(26) . . . . ?
C9 C10 C11 C12 7.3(18) . . . . ?
Pt2 C10 C11 C12 -169.6(9) . . . . ?
C10 C11 C12 C13 156.8(13) . . . . ?
C10 C11 C12 C3 -10.4(17) . . . . ?
C4 C3 C12 C11 157.6(12) . . . . ?
C2 C3 C12 C11 4.2(16) . . . . ?
C4 C3 C12 C13 -12.7(17) . . . . ?
C2 C3 C12 C13 -166.1(10) . . . . ?
C11 C12 C13 C14 -155.9(13) . . . . ?
C3 C12 C13 C14 11.7(16) . . . . ?
C11 C12 C13 Pt3 24.0(18) . . . . ?
C3 C12 C13 Pt3 -168.3(7) . . . . ?
P5 Pt3 C13 C14 -88.6(9) . . . . ?
P6 Pt3 C13 C14 87(3) . . . . ?
Cl3 Pt3 C13 C14 86.0(9) . . . . ?
P5 Pt3 C13 C12 91.4(8) . . . . ?
P6 Pt3 C13 C12 -93(3) . . . . ?
Cl3 Pt3 C13 C12 -93.9(8) . . . . ?
C12 C13 C14 C15 -0.2(18) . . . . ?
Pt3 C13 C14 C15 179.8(9) . . . . ?
C13 C14 C15 C4 -11.4(16) . . . . ?
C13 C14 C15 C16 158.9(13) . . . . ?
C5 C4 C15 C14 163.3(11) . . . . ?
C3 C4 C15 C14 10.8(16) . . . . ?
C5 C4 C15 C16 -8.9(18) . . . . ?
C3 C4 C15 C16 -161.4(11) . . . . ?
C14 C15 C16 C17 -160.9(12) . . . . ?
C4 C15 C16 C17 9.2(16) . . . . ?
C14 C15 C16 Pt4 19.2(19) . . . . ?
C4 C15 C16 Pt4 -170.6(8) . . . . ?
P8 Pt4 C16 C15 -78.7(10) . . . . ?
P7 Pt4 C16 C15 105.7(10) . . . . ?
Cl4 Pt4 C16 C15 115(13) . . . . ?
P8 Pt4 C16 C17 101.5(10) . . . . ?
P7 Pt4 C16 C17 -74.1(10) . . . . ?
Cl4 Pt4 C16 C17 -65(13) . . . . ?
C15 C16 C17 C18 -0.7(18) . . . . ?
Pt4 C16 C17 C18 179.2(9) . . . . ?
C4 C5 C18 C19 -164.7(12) . . . . ?
C1 C5 C18 C19 -11.7(17) . . . . ?
C4 C5 C18 C17 9.6(18) . . . . ?
C1 C5 C18 C17 162.6(11) . . . . ?
C16 C17 C18 C19 164.8(12) . . . . ?
C16 C17 C18 C5 -8.5(17) . . . . ?
C5 C18 C19 C20 11.4(17) . . . . ?
C17 C18 C19 C20 -161.7(13) . . . . ?
C5 C18 C19 Pt5 -166.6(8) . . . . ?
C17 C18 C19 Pt5 20.3(18) . . . . ?
P9 Pt5 C19 C18 -86.7(9) . . . . ?
P10 Pt5 C19 C18 94.3(9) . . . . ?
Cl5 Pt5 C19 C18 119(5) . . . . ?
P9 Pt5 C19 C20 95.3(9) . . . . ?
P10 Pt5 C19 C20 -83.6(9) . . . . ?
Cl5 Pt5 C19 C20 -59(5) . . . . ?
C1 C6 C20 C19 -8.5(17) . . . . ?
C7 C6 C20 C19 162.5(13) . . . . ?
C18 C19 C20 C6 -1.2(18) . . . . ?
Pt5 C19 C20 C6 176.7(9) . . . . ?
C23 P1 C21 C22 -68.7(15) . . . . ?
C25 P1 C21 C22 -176.0(14) . . . . ?
Pt1 P1 C21 C22 55.2(15) . . . . ?
C21 P1 C23 C24 -174.1(13) . . . . ?
C25 P1 C23 C24 -68.5(14) . . . . ?
Pt1 P1 C23 C24 63.8(14) . . . . ?
C23 P1 C25 C26 -148.3(12) . . . . ?
C21 P1 C25 C26 -41.6(13) . . . . ?
Pt1 P1 C25 C26 82.2(12) . . . . ?
C29A P2 C27A C28A 45(5) . . . . ?
C31A P2 C27A C28A -66(5) . . . . ?
Pt1 P2 C27A C28A 165(3) . . . . ?
C27A P2 C29A C30A 59(4) . . . . ?
C31A P2 C29A C30A 177(3) . . . . ?
Pt1 P2 C29A C30A -65(4) . . . . ?
C27A P2 C31A C32A -71(3) . . . . ?
C29A P2 C31A C32A 179(3) . . . . ?
Pt1 P2 C31A C32A 60(3) . . . . ?
C29B P2 C27B C28B 52(7) . . . . ?
C31B P2 C27B C28B -55(7) . . . . ?
Pt1 P2 C27B C28B -175(5) . . . . ?
C27B P2 C29B C30B 70(7) . . . . ?
C31B P2 C29B C30B 169(5) . . . . ?
Pt1 P2 C29B C30B -64(6) . . . . ?
C27B P2 C31B C32B -168(5) . . . . ?
C29B P2 C31B C32B 83(6) . . . . ?
Pt1 P2 C31B C32B -44(6) . . . . ?
C37A P3 C33A C34A -52(4) . . . . ?
C35A P3 C33A C34A 53(4) . . . . ?
Pt2 P3 C33A C34A 175(3) . . . . ?
C37A P3 C35A C36A 175(2) . . . . ?
C33A P3 C35A C36A 64(3) . . . . ?
Pt2 P3 C35A C36A -62(2) . . . . ?
C33A P3 C37A C38A -63(3) . . . . ?
C35A P3 C37A C38A -173(2) . . . . ?
Pt2 P3 C37A C38A 69(3) . . . . ?
C35B P3 C33B C34B 48(11) . . . . ?
C37B P3 C33B C34B -58(8) . . . . ?
Pt2 P3 C33B C34B -158(7) . . . . ?
C33B P3 C35B C36B 82(8) . . . . ?
C37B P3 C35B C36B 174(6) . . . . ?
Pt2 P3 C35B C36B -75(6) . . . . ?
C35B P3 C37B C38B 68(6) . . . . ?
C33B P3 C37B C38B -164(7) . . . . ?
Pt2 P3 C37B C38B -47(6) . . . . ?
C43 P4 C39 C40 48.8(13) . . . . ?
C41 P4 C39 C40 -59.2(13) . . . . ?
Pt2 P4 C39 C40 168.0(10) . . . . ?
C39 P4 C41 C42 -58.6(12) . . . . ?
C43 P4 C41 C42 -167.2(10) . . . . ?
Pt2 P4 C41 C42 70.9(11) . . . . ?
C39 P4 C43 C44 178.1(12) . . . . ?
C41 P4 C43 C44 -72.8(14) . . . . ?
Pt2 P4 C43 C44 55.7(13) . . . . ?
C47A P5 C45A C46A -61(4) . . . . ?
C49A P5 C45A C46A -165(4) . . . . ?
Pt3 P5 C45A C46A 66(4) . . . . ?
C45A P5 C47A C48A -51(5) . . . . ?
C49A P5 C47A C48A 66(5) . . . . ?
Pt3 P5 C47A C48A -177(3) . . . . ?
C45A P5 C49A C50A 172(4) . . . . ?
C47A P5 C49A C50A 65(4) . . . . ?
Pt3 P5 C49A C50A -57(4) . . . . ?
C47B P5 C45B C46B -72(6) . . . . ?
C49B P5 C45B C46B 179(7) . . . . ?
Pt3 P5 C45B C46B 59(6) . . . . ?
C45B P5 C47B C48B -68(6) . . . . ?
C49B P5 C47B C48B 32(7) . . . . ?
Pt3 P5 C47B C48B 161(5) . . . . ?
C45B P5 C49B C50B 175(6) . . . . ?
C47B P5 C49B C50B 68(6) . . . . ?
Pt3 P5 C49B C50B -62(6) . . . . ?
C53 P6 C51 C52 66.7(11) . . . . ?
C55 P6 C51 C52 -41.8(12) . . . . ?
Pt3 P6 C51 C52 -169.2(8) . . . . ?
C55 P6 C53 C54 -175.6(9) . . . . ?
C51 P6 C53 C54 77.3(10) . . . . ?
Pt3 P6 C53 C54 -56.7(10) . . . . ?
C53 P6 C55 C56 -171.5(10) . . . . ?
C51 P6 C55 C56 -65.3(11) . . . . ?
Pt3 P6 C55 C56 70.5(10) . . . . ?
C59A P7 C57A C58A 60(3) . . . . ?
C61A P7 C57A C58A 171(3) . . . . ?
Pt4 P7 C57A C58A -65(3) . . . . ?
C61A P7 C59A C60A -63(5) . . . . ?
C57A P7 C59A C60A 44(5) . . . . ?
Pt4 P7 C59A C60A 169(3) . . . . ?
C59A P7 C61A C62A -71(4) . . . . ?
C57A P7 C61A C62A -177(3) . . . . ?
Pt4 P7 C61A C62A 58(3) . . . . ?
C59B P7 C57B C58B 64(4) . . . . ?
C61B P7 C57B C58B 173(4) . . . . ?
Pt4 P7 C57B C58B -67(4) . . . . ?
C57B P7 C59B C60B 65(7) . . . . ?
C61B P7 C59B C60B -45(6) . . . . ?
Pt4 P7 C59B C60B -165(5) . . . . ?
C57B P7 C61B C62B -176(5) . . . . ?
C59B P7 C61B C62B -60(5) . . . . ?
Pt4 P7 C61B C62B 62(5) . . . . ?
C65A P8 C63A C64A -85(2) . . . . ?
C67A P8 C63A C64A 163(2) . . . . ?
Pt4 P8 C63A C64A 40(2) . . . . ?
C67A P8 C65A C66A -75(2) . . . . ?
C63A P8 C65A C66A -178.3(17) . . . . ?
Pt4 P8 C65A C66A 58.4(19) . . . . ?
C65A P8 C67A C68A -60(2) . . . . ?
C63A P8 C67A C68A 48(2) . . . . ?
Pt4 P8 C67A C68A 167.6(15) . . . . ?
C67B P8 C63B C64B 68(3) . . . . ?
C65B P8 C63B C64B 172(2) . . . . ?
Pt4 P8 C63B C64B -69(3) . . . . ?
C67B P8 C65B C66B -164(2) . . . . ?
C63B P8 C65B C66B 84(2) . . . . ?
Pt4 P8 C65B C66B -39(2) . . . . ?
C63B P8 C67B C68B 43(2) . . . . ?
C65B P8 C67B C68B -63(2) . . . . ?
Pt4 P8 C67B C68B 178.2(17) . . . . ?
C71 P9 C69 C70 -64.5(17) . . . . ?
C73 P9 C69 C70 -178.3(16) . . . . ?
Pt5 P9 C69 C70 60.3(17) . . . . ?
C73 P9 C71 C72 -71.5(17) . . . . ?
C69 P9 C71 C72 -174.5(14) . . . . ?
Pt5 P9 C71 C72 61.4(15) . . . . ?
C71 P9 C73 C74 -46(3) . . . . ?
C69 P9 C73 C74 61(2) . . . . ?
Pt5 P9 C73 C74 -178.5(18) . . . . ?
C79A P10 C75A C76A -73(2) . . . . ?
C77A P10 C75A C76A 178.5(17) . . . . ?
Pt5 P10 C75A C76A 62.7(17) . . . . ?
C79A P10 C77A C78A -53(2) . . . . ?
C75A P10 C77A C78A 66(2) . . . . ?
Pt5 P10 C77A C78A -176.1(19) . . . . ?
C75A P10 C79A C80A -157(2) . . . . ?
C77A P10 C79A C80A -49(3) . . . . ?
C75B P10 C79A C80A 172(3) . . . . ?
Pt5 P10 C79A C80A 70(3) . . . . ?
C79B P10 C75B C76B -177(3) . . . . ?
C77B P10 C75B C76B 84(3) . . . . ?
Pt5 P10 C75B C76B -54(2) . . . . ?
C79B P10 C77B C78B 73(3) . . . . ?
C75B P10 C77B C78B 159(2) . . . . ?
Pt5 P10 C77B C78B -78(3) . . . . ?
C77B P10 C79B C80B -128(4) . . . . ?
C75B P10 C79B C80B 128(4) . . . . ?
Pt5 P10 C79B C80B 25(5) . . . . ?
C87 Pt6 P11 C101 10.5(10) . . . . ?
P12 Pt6 P11 C101 40(3) . . . . ?
Cl6 Pt6 P11 C101 -170.7(10) . . . . ?
C87 Pt6 P11 C205 -145.6(12) . . . . ?
P12 Pt6 P11 C205 -117(3) . . . . ?
Cl6 Pt6 P11 C205 33.1(11) . . . . ?
C87 Pt6 P11 C201 -6.6(15) . . . . ?
P12 Pt6 P11 C201 22(3) . . . . ?
Cl6 Pt6 P11 C201 172.1(15) . . . . ?
C87 Pt6 P11 C103 139.3(7) . . . . ?
P12 Pt6 P11 C103 168(3) . . . . ?
Cl6 Pt6 P11 C103 -42.0(6) . . . . ?
C87 Pt6 P11 C105 -103.4(10) . . . . ?
P12 Pt6 P11 C105 -74(3) . . . . ?
Cl6 Pt6 P11 C105 75.3(9) . . . . ?
C87 Pt6 P11 C203 100.9(11) . . . . ?
P12 Pt6 P11 C203 130(3) . . . . ?
Cl6 Pt6 P11 C203 -80.4(10) . . . . ?
C87 Pt6 P12 C111 -44.4(11) . . . . ?
P11 Pt6 P12 C111 -74(3) . . . . ?
Cl6 Pt6 P12 C111 136.8(11) . . . . ?
C87 Pt6 P12 C107 74.7(13) . . . . ?
P11 Pt6 P12 C107 46(3) . . . . ?
Cl6 Pt6 P12 C107 -104.1(13) . . . . ?
C87 Pt6 P12 C211 -36.0(14) . . . . ?
P11 Pt6 P12 C211 -65(3) . . . . ?
Cl6 Pt6 P12 C211 145.2(14) . . . . ?
C87 Pt6 P12 C209 -156.0(16) . . . . ?
P11 Pt6 P12 C209 175(21) . . . . ?
Cl6 Pt6 P12 C209 25.2(16) . . . . ?
C87 Pt6 P12 C109 -170.2(12) . . . . ?
P11 Pt6 P12 C109 161(3) . . . . ?
Cl6 Pt6 P12 C109 11.0(12) . . . . ?
C87 Pt6 P12 C207 78(2) . . . . ?
P11 Pt6 P12 C207 49(4) . . . . ?
Cl6 Pt6 P12 C207 -101(2) . . . . ?
C90 Pt7 P13 C215 7.9(10) . . . . ?
P14 Pt7 P13 C215 -141(9) . . . . ?
Cl7 Pt7 P13 C215 -169.8(9) . . . . ?
C90 Pt7 P13 C213 -147.1(12) . . . . ?
P14 Pt7 P13 C213 64(9) . . . . ?
Cl7 Pt7 P13 C213 35.2(12) . . . . ?
C90 Pt7 P13 C113 -130.5(13) . . . . ?
P14 Pt7 P13 C113 81(9) . . . . ?
Cl7 Pt7 P13 C113 51.7(13) . . . . ?
C90 Pt7 P13 C117 79.1(8) . . . . ?
P14 Pt7 P13 C117 -70(9) . . . . ?
Cl7 Pt7 P13 C117 -98.6(7) . . . . ?
C90 Pt7 P13 C217 132.2(9) . . . . ?
P14 Pt7 P13 C217 -17(9) . . . . ?
Cl7 Pt7 P13 C217 -45.6(8) . . . . ?
C90 Pt7 P13 C115 -28.5(11) . . . . ?
P14 Pt7 P13 C115 -177(100) . . . . ?
Cl7 Pt7 P13 C115 153.8(10) . . . . ?
C90 Pt7 P14 C221 100.0(16) . . . . ?
P13 Pt7 P14 C221 -111(9) . . . . ?
Cl7 Pt7 P14 C221 -82.3(16) . . . . ?
C90 Pt7 P14 C121 96.5(12) . . . . ?
P13 Pt7 P14 C121 -115(9) . . . . ?
Cl7 Pt7 P14 C121 -85.7(12) . . . . ?
C90 Pt7 P14 C223 -33.1(9) . . . . ?
P13 Pt7 P14 C223 116(9) . . . . ?
Cl7 Pt7 P14 C223 144.6(8) . . . . ?
C90 Pt7 P14 C119 -137.3(14) . . . . ?
P13 Pt7 P14 C119 12(9) . . . . ?
Cl7 Pt7 P14 C119 40.4(13) . . . . ?
C90 Pt7 P14 C219 -146.8(12) . . . . ?
P13 Pt7 P14 C219 2(9) . . . . ?
Cl7 Pt7 P14 C219 31.0(11) . . . . ?
C90 Pt7 P14 C123 -11.9(13) . . . . ?
P13 Pt7 P14 C123 137(9) . . . . ?
Cl7 Pt7 P14 C123 165.9(13) . . . . ?
C93 Pt8 P15 C129 90.4(6) . . . . ?
P16 Pt8 P15 C129 -26.6(16) . . . . ?
Cl8 Pt8 P15 C129 -89.2(5) . . . . ?
C93 Pt8 P15 C127 -153.2(6) . . . . ?
P16 Pt8 P15 C127 89.8(15) . . . . ?
Cl8 Pt8 P15 C127 27.2(5) . . . . ?
C93 Pt8 P15 C125 -31.8(6) . . . . ?
P16 Pt8 P15 C125 -148.7(15) . . . . ?
Cl8 Pt8 P15 C125 148.7(6) . . . . ?
C93 Pt8 P16 C135 7.1(7) . . . . ?
P15 Pt8 P16 C135 123.8(15) . . . . ?
Cl8 Pt8 P16 C135 -173.4(6) . . . . ?
C93 Pt8 P16 C131 129.8(7) . . . . ?
P15 Pt8 P16 C131 -113.4(15) . . . . ?
Cl8 Pt8 P16 C131 -50.6(6) . . . . ?
C93 Pt8 P16 C133 -116.1(7) . . . . ?
P15 Pt8 P16 C133 0.6(17) . . . . ?
Cl8 Pt8 P16 C133 63.4(6) . . . . ?
C96 Pt9 P17 C139 -138.0(6) . . . . ?
P18 Pt9 P17 C139 77.2(15) . . . . ?
Cl9 Pt9 P17 C139 44.8(5) . . . . ?
C96 Pt9 P17 C137 -16.6(6) . . . . ?
P18 Pt9 P17 C137 -161.4(14) . . . . ?
Cl9 Pt9 P17 C137 166.1(5) . . . . ?
C96 Pt9 P17 C141 104.7(6) . . . . ?
P18 Pt9 P17 C141 -40.1(15) . . . . ?
Cl9 Pt9 P17 C141 -72.6(5) . . . . ?
C96 Pt9 P18 C147 -5.8(6) . . . . ?
P17 Pt9 P18 C147 139.1(14) . . . . ?
Cl9 Pt9 P18 C147 171.6(5) . . . . ?
C96 Pt9 P18 C143 118.5(6) . . . . ?
P17 Pt9 P18 C143 -96.7(15) . . . . ?
Cl9 Pt9 P18 C143 -64.2(6) . . . . ?
C96 Pt9 P18 C145 -125.6(6) . . . . ?
P17 Pt9 P18 C145 19.3(15) . . . . ?
Cl9 Pt9 P18 C145 51.8(5) . . . . ?
C99 Pt10 P19 C151 84(2) . . . . ?
P20 Pt10 P19 C151 -117.7(6) . . . . ?
Cl10 Pt10 P19 C151 60.9(6) . . . . ?
C99 Pt10 P19 C153 -32(2) . . . . ?
P20 Pt10 P19 C153 126.2(5) . . . . ?
Cl10 Pt10 P19 C153 -55.1(5) . . . . ?
C99 Pt10 P19 C149 -151(2) . . . . ?
P20 Pt10 P19 C149 7.4(6) . . . . ?
Cl10 Pt10 P19 C149 -174.0(6) . . . . ?
C99 Pt10 P20 C159 -121.9(6) . . . . ?
P19 Pt10 P20 C159 61.3(6) . . . . ?
Cl10 Pt10 P20 C159 -100.7(18) . . . . ?
C99 Pt10 P20 C155 -2.1(7) . . . . ?
P19 Pt10 P20 C155 -178.9(6) . . . . ?
Cl10 Pt10 P20 C155 19.1(19) . . . . ?
C99 Pt10 P20 C157 118.5(6) . . . . ?
P19 Pt10 P20 C157 -58.3(5) . . . . ?
Cl10 Pt10 P20 C157 139.7(17) . . . . ?
C86 C81 C82 C89 0.1(18) . . . . ?
C85 C81 C82 C89 154.1(11) . . . . ?
C86 C81 C82 C83 -156.4(11) . . . . ?
C85 C81 C82 C83 -2.4(13) . . . . ?
C81 C82 C83 C92 159.3(11) . . . . ?
C89 C82 C83 C92 2.3(18) . . . . ?
C81 C82 C83 C84 2.7(12) . . . . ?
C89 C82 C83 C84 -154.3(11) . . . . ?
C92 C83 C84 C85 -158.0(11) . . . . ?
C82 C83 C84 C85 -2.1(13) . . . . ?
C92 C83 C84 C95 -1.9(18) . . . . ?
C82 C83 C84 C95 154.0(10) . . . . ?
C83 C84 C85 C98 156.2(11) . . . . ?
C95 C84 C85 C98 1.0(18) . . . . ?
C83 C84 C85 C81 0.7(13) . . . . ?
C95 C84 C85 C81 -154.6(10) . . . . ?
C82 C81 C85 C98 -153.8(11) . . . . ?
C86 C81 C85 C98 1.0(18) . . . . ?
C82 C81 C85 C84 1.1(12) . . . . ?
C86 C81 C85 C84 155.8(10) . . . . ?
C82 C81 C86 C87 -10.6(16) . . . . ?
C85 C81 C86 C87 -161.4(10) . . . . ?
C82 C81 C86 C100 163.3(10) . . . . ?
C85 C81 C86 C100 12.4(15) . . . . ?
C81 C86 C87 C88 11.0(16) . . . . ?
C100 C86 C87 C88 -161.3(12) . . . . ?
C81 C86 C87 Pt6 -169.1(8) . . . . ?
C100 C86 C87 Pt6 18.5(17) . . . . ?
P11 Pt6 C87 C88 99.9(9) . . . . ?
P12 Pt6 C87 C88 -78.8(9) . . . . ?
Cl6 Pt6 C87 C88 -51(8) . . . . ?
P11 Pt6 C87 C86 -80.0(9) . . . . ?
P12 Pt6 C87 C86 101.3(9) . . . . ?
Cl6 Pt6 C87 C86 130(7) . . . . ?
C86 C87 C88 C89 -2.0(18) . . . . ?
Pt6 C87 C88 C89 178.2(9) . . . . ?
C81 C82 C89 C88 9.1(17) . . . . ?
C83 C82 C89 C88 162.5(11) . . . . ?
C81 C82 C89 C90 -166.2(11) . . . . ?
C83 C82 C89 C90 -12.9(17) . . . . ?
C87 C88 C89 C82 -8.1(17) . . . . ?
C87 C88 C89 C90 166.3(12) . . . . ?
C82 C89 C90 C91 11.8(16) . . . . ?
C88 C89 C90 C91 -162.5(12) . . . . ?
C82 C89 C90 Pt7 -166.1(9) . . . . ?
C88 C89 C90 Pt7 19.7(18) . . . . ?
P14 Pt7 C90 C91 96.7(9) . . . . ?
P13 Pt7 C90 C91 -82.9(9) . . . . ?
Cl7 Pt7 C90 C91 -46(6) . . . . ?
P14 Pt7 C90 C89 -85.6(9) . . . . ?
P13 Pt7 C90 C89 94.9(9) . . . . ?
Cl7 Pt7 C90 C89 131(5) . . . . ?
C89 C90 C91 C92 -0.8(18) . . . . ?
Pt7 C90 C91 C92 177.1(9) . . . . ?
C84 C83 C92 C91 160.7(11) . . . . ?
C82 C83 C92 C91 8.6(17) . . . . ?
C84 C83 C92 C93 -12.1(17) . . . . ?
C82 C83 C92 C93 -164.1(11) . . . . ?
C90 C91 C92 C83 -9.3(17) . . . . ?
C90 C91 C92 C93 161.7(13) . . . . ?
C83 C92 C93 C94 15.2(16) . . . . ?
C91 C92 C93 C94 -155.7(13) . . . . ?
C83 C92 C93 Pt8 -162.5(8) . . . . ?
C91 C92 C93 Pt8 26.6(18) . . . . ?
P16 Pt8 C93 C94 80.9(9) . . . . ?
P15 Pt8 C93 C94 -94.5(9) . . . . ?
Cl8 Pt8 C93 C94 38(35) . . . . ?
P16 Pt8 C93 C92 -101.3(9) . . . . ?
P15 Pt8 C93 C92 83.2(9) . . . . ?
Cl8 Pt8 C93 C92 -144(34) . . . . ?
C92 C93 C94 C95 -5.5(17) . . . . ?
Pt8 C93 C94 C95 172.2(8) . . . . ?
C83 C84 C95 C94 12.0(15) . . . . ?
C85 C84 C95 C94 164.5(10) . . . . ?
C83 C84 C95 C96 -157.3(10) . . . . ?
C85 C84 C95 C96 -4.8(16) . . . . ?
C93 C94 C95 C84 -8.5(16) . . . . ?
C93 C94 C95 C96 158.5(12) . . . . ?
C84 C95 C96 C97 2.1(14) . . . . ?
C94 C95 C96 C97 -164.7(11) . . . . ?
C84 C95 C96 Pt9 179.0(7) . . . . ?
C94 C95 C96 Pt9 12.2(16) . . . . ?
P17 Pt9 C96 C97 -107.4(8) . . . . ?
P18 Pt9 C96 C97 69.8(8) . . . . ?
Cl9 Pt9 C96 C97 13(6) . . . . ?
P17 Pt9 C96 C95 75.8(8) . . . . ?
P18 Pt9 C96 C95 -107.0(8) . . . . ?
Cl9 Pt9 C96 C95 -164(5) . . . . ?
C95 C96 C97 C98 4.4(16) . . . . ?
Pt9 C96 C97 C98 -172.5(8) . . . . ?
C84 C85 C98 C97 5.3(16) . . . . ?
C81 C85 C98 C97 156.3(11) . . . . ?
C84 C85 C98 C99 -164.4(10) . . . . ?
C81 C85 C98 C99 -13.4(16) . . . . ?
C96 C97 C98 C85 -8.1(16) . . . . ?
C96 C97 C98 C99 159.5(11) . . . . ?
C85 C98 C99 C100 11.9(15) . . . . ?
C97 C98 C99 C100 -155.7(12) . . . . ?
C85 C98 C99 Pt10 -167.6(8) . . . . ?
C97 C98 C99 Pt10 24.8(16) . . . . ?
P20 Pt10 C99 C100 -95.7(9) . . . . ?
P19 Pt10 C99 C100 62(3) . . . . ?
Cl10 Pt10 C99 C100 85.8(9) . . . . ?
P20 Pt10 C99 C98 83.7(8) . . . . ?
P19 Pt10 C99 C98 -118(2) . . . . ?
Cl10 Pt10 C99 C98 -94.7(8) . . . . ?
C98 C99 C100 C86 1.3(17) . . . . ?
Pt10 C99 C100 C86 -179.2(8) . . . . ?
C81 C86 C100 C99 -13.4(16) . . . . ?
C87 C86 C100 C99 159.0(12) . . . . ?
C205 P11 C101 C102 -17(3) . . . . ?
C201 P11 C101 C102 -82(7) . . . . ?
C103 P11 C101 C102 57(3) . . . . ?
C105 P11 C101 C102 -48(3) . . . . ?
C203 P11 C101 C102 86(3) . . . . ?
Pt6 P11 C101 C102 -170(2) . . . . ?
C101 P11 C103 C104 70(2) . . . . ?
C205 P11 C103 C104 -171(3) . . . . ?
C201 P11 C103 C104 81(3) . . . . ?
C105 P11 C103 C104 171(2) . . . . ?
C203 P11 C103 C104 16.3(16) . . . . ?
Pt6 P11 C103 C104 -64(2) . . . . ?
C101 P11 C105 C106 -170(2) . . . . ?
C205 P11 C105 C106 55(3) . . . . ?
C201 P11 C105 C106 -162(3) . . . . ?
C103 P11 C105 C106 81(3) . . . . ?
C203 P11 C105 C106 102(3) . . . . ?
Pt6 P11 C105 C106 -45(3) . . . . ?
C101 P11 C201 C202 58(5) . . . . ?
C205 P11 C201 C202 -65(4) . . . . ?
C103 P11 C201 C202 12(5) . . . . ?
C105 P11 C201 C202 -89(4) . . . . ?
C203 P11 C201 C202 45(4) . . . . ?
Pt6 P11 C201 C202 157(3) . . . . ?
C101 P11 C203 C204 157(3) . . . . ?
C205 P11 C203 C204 -81(3) . . . . ?
C201 P11 C203 C204 160(3) . . . . ?
C103 P11 C203 C204 -74(3) . . . . ?
C105 P11 C203 C204 -109(3) . . . . ?
Pt6 P11 C203 C204 39(3) . . . . ?
C101 P11 C205 C206 -82(4) . . . . ?
C201 P11 C205 C206 -67(4) . . . . ?
C103 P11 C205 C206 -178(4) . . . . ?
C105 P11 C205 C206 -26(2) . . . . ?
C203 P11 C205 C206 -173(3) . . . . ?
Pt6 P11 C205 C206 73(3) . . . . ?
C111 P12 C107 C108 -169(4) . . . . ?
C211 P12 C107 C108 -168(5) . . . . ?
C209 P12 C107 C108 -66(4) . . . . ?
C109 P12 C107 C108 -58(4) . . . . ?
C207 P12 C107 C108 48(21) . . . . ?
Pt6 P12 C107 C108 67(4) . . . . ?
C111 P12 C109 C110 34(3) . . . . ?
C107 P12 C109 C110 -74(3) . . . . ?
C211 P12 C109 C110 24(3) . . . . ?
C209 P12 C109 C110 71(6) . . . . ?
C207 P12 C109 C110 -83(3) . . . . ?
Pt6 P12 C109 C110 162(2) . . . . ?
C107 P12 C111 C112 166(3) . . . . ?
C211 P12 C111 C112 158(27) . . . . ?
C209 P12 C111 C112 54(3) . . . . ?
C109 P12 C111 C112 62(3) . . . . ?
C207 P12 C111 C112 172(3) . . . . ?
Pt6 P12 C111 C112 -68(3) . . . . ?
C111 P12 C207 C208 164(5) . . . . ?
C107 P12 C207 C208 -157(29) . . . . ?
C211 P12 C207 C208 166(5) . . . . ?
C209 P12 C207 C208 -87(6) . . . . ?
C109 P12 C207 C208 -81(5) . . . . ?
Pt6 P12 C207 C208 41(6) . . . . ?
C111 P12 C209 C210 84(4) . . . . ?
C107 P12 C209 C210 -24(4) . . . . ?
C211 P12 C209 C210 74(4) . . . . ?
C109 P12 C209 C210 -61(5) . . . . ?
C207 P12 C209 C210 -33(4) . . . . ?
Pt6 P12 C209 C210 -156(3) . . . . ?
C111 P12 C211 C212 -17(22) . . . . ?
C107 P12 C211 C212 171(4) . . . . ?
C209 P12 C211 C212 61(4) . . . . ?
C109 P12 C211 C212 71(4) . . . . ?
C207 P12 C211 C212 177(4) . . . . ?
Pt6 P12 C211 C212 -66(4) . . . . ?
C215 P13 C113 C114 44(3) . . . . ?
C213 P13 C113 C114 -23(4) . . . . ?
C117 P13 C113 C114 -29(4) . . . . ?
C217 P13 C113 C114 -64(3) . . . . ?
C115 P13 C113 C114 80(3) . . . . ?
Pt7 P13 C113 C114 -168(2) . . . . ?
C215 P13 C115 C116 47(2) . . . . ?
C213 P13 C115 C116 -48(2) . . . . ?
C113 P13 C115 C116 -72(2) . . . . ?
C117 P13 C115 C116 65(2) . . . . ?
C217 P13 C115 C116 33(3) . . . . ?
Pt7 P13 C115 C116 -179.1(18) . . . . ?
C215 P13 C117 C118 -167(3) . . . . ?
C213 P13 C117 C118 -74(3) . . . . ?
C113 P13 C117 C118 -72(3) . . . . ?
C217 P13 C117 C118 -24(2) . . . . ?
C115 P13 C117 C118 -180(2) . . . . ?
Pt7 P13 C117 C118 66(2) . . . . ?
C215 P13 C213 C214 -102(3) . . . . ?
C113 P13 C213 C214 18(3) . . . . ?
C117 P13 C213 C214 -166(3) . . . . ?
C217 P13 C213 C214 156(3) . . . . ?
C115 P13 C213 C214 -63(3) . . . . ?
Pt7 P13 C213 C214 60(3) . . . . ?
C213 P13 C215 C216 77(3) . . . . ?
C113 P13 C215 C216 54(3) . . . . ?
C117 P13 C215 C216 -176(3) . . . . ?
C217 P13 C215 C216 155(2) . . . . ?
C115 P13 C215 C216 -16(2) . . . . ?
Pt7 P13 C215 C216 -82(3) . . . . ?
C215 P13 C217 C218 80(3) . . . . ?
C213 P13 C217 C218 178(3) . . . . ?
C113 P13 C217 C218 -165(2) . . . . ?
C117 P13 C217 C218 46(2) . . . . ?
C115 P13 C217 C218 89(3) . . . . ?
Pt7 P13 C217 C218 -60(2) . . . . ?
C221 P14 C119 C120 176(4) . . . . ?
C121 P14 C119 C120 168(4) . . . . ?
C223 P14 C119 C120 -79(4) . . . . ?
C219 P14 C119 C120 114(22) . . . . ?
C123 P14 C119 C120 -83(4) . . . . ?
Pt7 P14 C119 C120 43(4) . . . . ?
C221 P14 C121 C122 -112(10) . . . . ?
C223 P14 C121 C122 -172(2) . . . . ?
C119 P14 C121 C122 -74(3) . . . . ?
C219 P14 C121 C122 -67(3) . . . . ?
C123 P14 C121 C122 171(2) . . . . ?
Pt7 P14 C121 C122 55(3) . . . . ?
C221 P14 C123 C124 60(3) . . . . ?
C121 P14 C123 C124 73(3) . . . . ?
C223 P14 C123 C124 -56(5) . . . . ?
C119 P14 C123 C124 -44(3) . . . . ?
C219 P14 C123 C124 -41(4) . . . . ?
Pt7 P14 C123 C124 -173(2) . . . . ?
C221 P14 C219 C220 -159(5) . . . . ?
C121 P14 C219 C220 -168(4) . . . . ?
C223 P14 C219 C220 -53(5) . . . . ?
C119 P14 C219 C220 -39(14) . . . . ?
C123 P14 C219 C220 -58(6) . . . . ?
Pt7 P14 C219 C220 73(5) . . . . ?
C121 P14 C221 C222 70(8) . . . . ?
C223 P14 C221 C222 -166(3) . . . . ?
C119 P14 C221 C222 -74(3) . . . . ?
C219 P14 C221 C222 -66(3) . . . . ?
C123 P14 C221 C222 175(3) . . . . ?
Pt7 P14 C221 C222 55(3) . . . . ?
C221 P14 C223 C224 -54(4) . . . . ?
C121 P14 C223 C224 -42(4) . . . . ?
C119 P14 C223 C224 -154(3) . . . . ?
C219 P14 C223 C224 -152(3) . . . . ?
C123 P14 C223 C224 14(4) . . . . ?
Pt7 P14 C223 C224 86(3) . . . . ?
C129 P15 C125 C126 -38.9(12) . . . . ?
C127 P15 C125 C126 -144.8(11) . . . . ?
Pt8 P15 C125 C126 87.6(11) . . . . ?
C129 P15 C127 C128 -171.7(10) . . . . ?
C125 P15 C127 C128 -64.5(11) . . . . ?
Pt8 P15 C127 C128 66.0(11) . . . . ?
C127 P15 C129 C130 -67.0(13) . . . . ?
C125 P15 C129 C130 -172.9(11) . . . . ?
Pt8 P15 C129 C130 56.6(12) . . . . ?
C135 P16 C131 C132 55(3) . . . . ?
C133 P16 C131 C132 166(2) . . . . ?
Pt8 P16 C131 C132 -75(2) . . . . ?
C135 P16 C131 C232 89(3) . . . . ?
C133 P16 C131 C232 -160(3) . . . . ?
Pt8 P16 C131 C232 -41(3) . . . . ?
C135 P16 C133 C134 -71.2(13) . . . . ?
C131 P16 C133 C134 179.5(13) . . . . ?
Pt8 P16 C133 C134 57.7(13) . . . . ?
C131 P16 C135 C136 55.1(15) . . . . ?
C133 P16 C135 C136 -52.0(15) . . . . ?
Pt8 P16 C135 C136 -177.2(11) . . . . ?
C139 P17 C137 C138 -161.1(10) . . . . ?
C141 P17 C137 C138 -50.9(12) . . . . ?
Pt9 P17 C137 C138 72.4(11) . . . . ?
C137 P17 C139 C140 -75.8(12) . . . . ?
C141 P17 C139 C140 174.6(11) . . . . ?
Pt9 P17 C139 C140 55.4(12) . . . . ?
C139 P17 C141 C142 54.1(15) . . . . ?
C137 P17 C141 C142 -53.6(15) . . . . ?
Pt9 P17 C141 C142 175.9(12) . . . . ?
C147 P18 C143 C144 -52.4(14) . . . . ?
C145 P18 C143 C144 54.7(13) . . . . ?
Pt9 P18 C143 C144 175.0(11) . . . . ?
C147 P18 C145 C146 -73.9(11) . . . . ?
C143 P18 C145 C146 177.1(10) . . . . ?
Pt9 P18 C145 C146 56.4(11) . . . . ?
C143 P18 C147 C148 -58.5(11) . . . . ?
C145 P18 C147 C148 -166.8(10) . . . . ?
Pt9 P18 C147 C148 68.9(11) . . . . ?
C151 P19 C149 C150 -44.2(13) . . . . ?
C153 P19 C149 C150 65.6(13) . . . . ?
Pt10 P19 C149 C150 -172.5(9) . . . . ?
C153 P19 C151 C152 -172.4(11) . . . . ?
C149 P19 C151 C152 -66.0(12) . . . . ?
Pt10 P19 C151 C152 70.1(12) . . . . ?
C151 P19 C153 C154 -172.9(10) . . . . ?
C149 P19 C153 C154 79.0(11) . . . . ?
Pt10 P19 C153 C154 -53.6(11) . . . . ?
C159 P20 C155 C156 -56.9(15) . . . . ?
C157 P20 C155 C156 51.8(15) . . . . ?
Pt10 P20 C155 C156 178.0(12) . . . . ?
C159 P20 C157 C158 170.6(13) . . . . ?
C155 P20 C157 C158 62.5(14) . . . . ?
Pt10 P20 C157 C158 -64.7(13) . . . . ?
C155 P20 C159 C160 -58.7(14) . . . . ?
C157 P20 C159 C160 -166.9(12) . . . . ?
Pt10 P20 C159 C160 68.0(13) . . . . ?
