Crystallography Open Database

Information card for entry 7151653

Preview

Coordinates	7151653.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H45 N2 O11 Tb Zn
Calculated formula	C53 H45 N2 O11 Tb Zn
Title of publication	A novel synthesis of oxazolidine-2,4-diones via an efficient fixation of CO2 with 3-aryl-2-alkynamides.
Authors of publication	Chen, Guofei; Fu, Chunling; Ma, Shengming
Journal of publication	Organic & biomolecular chemistry
Year of publication	2011
Journal volume	9
Journal issue	1
Pages of publication	105 - 110
a	13.028 ± 0.003 Å
b	13.163 ± 0.003 Å
c	15.397 ± 0.003 Å
α	75.58 ± 0.03°
β	82.38 ± 0.03°
γ	83.32 ± 0.03°
Cell volume	2525.1 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0586
Residual factor for significantly intense reflections	0.0406
Weighted residual factors for significantly intense reflections	0.0955
Weighted residual factors for all reflections included in the refinement	0.0992
Goodness-of-fit parameter for all reflections included in the refinement	0.986
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180302 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/16.	7151653.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7151653.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7151653.cif
14975	2011-03-12	../uploads/cif-deposit/cod/cif Adding structures of 7151651, 7151652, 7151653, 7151654, 7151655 via cif-deposit CGI script.	7151653.cif