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Information card for entry 7151764
Preview
| Coordinates | 7151764.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | ChemSpider |
| Formula | C19 H23 N O4 |
|---|---|
| Calculated formula | C19 H23 N O4 |
| SMILES | O1COc2cc3[C@@H]4[C@H]5OC(O[C@H]5C[C@H]5CCN(Cc3cc12)[C@@H]45)(C)C |
| Title of publication | Total synthesis of the Amaryllidaceae alkaloid clivonine. |
| Authors of publication | Haning, Helmut; Giró-Mañas, Carles; Paddock, Victoria L.; Bochet, Christian G.; White, Andrew J. P.; Bernardinelli, Gerald; Mann, Inderjit; Oppolzer, Wolfang; Spivey, Alan C. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 8 |
| Pages of publication | 2809 - 2820 |
| a | 10.695 ± 0.001 Å |
| b | 10.695 ± 0.001 Å |
| c | 25.134 ± 0.004 Å |
| α | 90° |
| β | 90° |
| γ | 120° |
| Cell volume | 2489.7 ± 0.5 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 169 |
| Hermann-Mauguin space group symbol | P 61 |
| Hall space group symbol | P 61 |
| Residual factor for all reflections | 0.1136 |
| Residual factor for significantly intense reflections | 0.0446 |
| Weighted residual factors for significantly intense reflections | 0.0727 |
| Weighted residual factors for all reflections included in the refinement | 0.0846 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.959 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 202017 (current) | 2017-10-14 | cif/ Marking COD entries in range 7 that are known to be related to ChemSpider entries using the _cod_related_entry data loop. |
7151764.cif |
| 180303 | 2016-03-26 | cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/17. |
7151764.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7151764.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7151764.cif |
| 21258 | 2011-06-22 | ../uploads/cif-deposit/cod/cif Adding structures of 7151762, 7151763, 7151764, 7151765 via cif-deposit CGI script. |
7151764.cif |
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Users of the data should acknowledge the original authors of the
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