Crystallography Open Database

Information card for entry 7151896

Preview

Coordinates	7151896.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H25 N O Si
Calculated formula	C16 H25 N O Si
Title of publication	Conia-ene annulation of the α-cyano β-TMS-capped alkynyl cycloalkanone system and its synthetic application
Authors of publication	Chin, Chih-Lung; Liao, Cheng-Feng; Liu, Hsing-Jang; Wong, Ying-Chieh; Hsieh, Ming-Tsang; Amancha, Prashanth K.; Chang, Chun-Ping; Shia, Kak-Shan
Journal of publication	Organic & Biomolecular Chemistry
Year of publication	2011
Journal volume	9
Journal issue	13
Pages of publication	4778
a	11.914 ± 0.004 Å
b	11.74 ± 0.004 Å
c	12.726 ± 0.004 Å
α	90°
β	106.442 ± 0.005°
γ	90°
Cell volume	1707.2 ± 1 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1534
Residual factor for significantly intense reflections	0.0567
Weighted residual factors for significantly intense reflections	0.1344
Weighted residual factors for all reflections included in the refinement	0.1603
Goodness-of-fit parameter for all reflections included in the refinement	0.802
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180304 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/18.	7151896.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7151896.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7151896.cif
21444	2011-06-22	../uploads/cif-deposit/cod/cif Adding structures of 7151896, 7151897, 7151898 via cif-deposit CGI script.	7151896.cif