Crystallography Open Database

Information card for entry 7152006

7152005 << 7152006 >> 7152007

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Coordinates	7152006.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H34 N2 O12
Calculated formula	C28 H34 N2 O12
Title of publication	Palladium-catalyzed C-H acetoxylation of 2-methoxyimino-2-aryl-acetates and acetamides.
Authors of publication	Wang, Liang; Xia, Xu-Dong; Guo, Wei; Chen, Jia-Rong; Xiao, Wen-Jing
Journal of publication	Organic & biomolecular chemistry
Year of publication	2011
Journal volume	9
Journal issue	20
Pages of publication	6895 - 6898
a	7.6651 ± 0.0006 Å
b	13.1131 ± 0.0009 Å
c	29.874 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	3002.7 ± 0.4 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	4
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0485
Residual factor for significantly intense reflections	0.0418
Weighted residual factors for significantly intense reflections	0.1173
Weighted residual factors for all reflections included in the refinement	0.1216
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180306 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/20.	7152006.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7152006.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7152006.cif
28168	2011-10-13	../uploads/cif-deposit/cod/cif Adding structures of 7152006 via cif-deposit CGI script.	7152006.cif