Crystallography Open Database

Information card for entry 7153252

Preview

Coordinates	7153252.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	04srv178 - HY/5/35-Fr50-r
Formula	C23 H34 O5 P2
Calculated formula	C23 H34 O5 P2
Title of publication	A synthesis of oligomeric alpha-hydroxy phenylphosphinates and a study of the conformational preferences of the dimers.
Authors of publication	Afarinkia, Kamyar; Royappa, Martin; Scowen, Ian J.; Steed, Jonathan W.; Yu, Hiu-Wan
Journal of publication	Organic & biomolecular chemistry
Year of publication	2010
Journal volume	8
Journal issue	3
Pages of publication	600 - 606
a	20.3573 ± 0.0004 Å
b	20.3573 ± 0.0004 Å
c	31.9361 ± 0.0012 Å
α	90°
β	90°
γ	120°
Cell volume	11461.8 ± 0.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0637
Residual factor for significantly intense reflections	0.0455
Weighted residual factors for significantly intense reflections	0.101
Weighted residual factors for all reflections included in the refinement	0.1088
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180318 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/32.	7153252.cif
92525	2014-01-12	cif/ Adding structures of 7153250, 7153251, 7153252, 7153253 via cif-deposit CGI script.	7153252.cif