Crystallography Open Database

Information card for entry 7156003

Preview

Coordinates	7156003.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C17 H28 O4 Si
Calculated formula	C17 H28 O4 Si
Title of publication	Synthesis of the natural product descurainolide and cyclic peptides from lignin-derived aromatics.
Authors of publication	Ojo, O. Stephen; Nardone, Brunello; Musolino, Stefania F.; Neal, Andrew R.; Wilson, Liam; Lebl, Tomas; Slawin, Alexandra M. Z.; Cordes, David B.; Taylor, James E.; Naismith, James H.; Smith, Andrew D.; Westwood, Nicholas J.
Journal of publication	Organic & biomolecular chemistry
Year of publication	2018
Journal volume	16
Journal issue	2
Pages of publication	266 - 273
a	7.2037 ± 0.0011 Å
b	10.9197 ± 0.0017 Å
c	23.762 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	1869.2 ± 0.5 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0542
Residual factor for significantly intense reflections	0.0533
Weighted residual factors for significantly intense reflections	0.1337
Weighted residual factors for all reflections included in the refinement	0.1349
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	1.54187 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
230715 (current)	2019-11-17	cif/ Updating files of 7156003, 7156004, 7156005, 7156006, 7156007 Original log message: Adding full bibliography for 7156003--7156007.cif.	7156003.cif
203884	2017-12-02	cif/ Adding structures of 7156003, 7156004, 7156005, 7156006, 7156007 via cif-deposit CGI script.	7156003.cif