Crystallography Open Database

Information card for entry 7156728

Preview

Coordinates	7156728.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H22 N4
Calculated formula	C24 H22 N4
Title of publication	Iodine-mediated oxidative N-N coupling of secondary amines to hydrazines.
Authors of publication	Ren, Linning; Wang, Manman; Fang, Benyao; Yu, Wenquan; Chang, Junbiao
Journal of publication	Organic & biomolecular chemistry
Year of publication	2019
Journal volume	17
Journal issue	13
Pages of publication	3446 - 3450
a	9.8651 ± 0.0004 Å
b	18.4812 ± 0.0009 Å
c	11.3374 ± 0.0006 Å
α	90°
β	107.506 ± 0.005°
γ	90°
Cell volume	1971.29 ± 0.17 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0649
Residual factor for significantly intense reflections	0.0487
Weighted residual factors for significantly intense reflections	0.1316
Weighted residual factors for all reflections included in the refinement	0.1474
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
225199 (current)	2019-11-08	cif/ Updating files of 7156728 Original log message: Adding full bibliography for 7156728.cif.	7156728.cif
214104	2019-03-13	cif/ Adding structures of 7156728 via cif-deposit CGI script.	7156728.cif